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Wyświetlanie 1-15 z 25
Tytuł:
Mössbauer spectroscopy study of 60P2O5-40Fe2O3 glass crystallization
Autorzy:
Stoch, P.
Stoch, A.
Powiązania:
https://bibliotekanauki.pl/articles/146169.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
crystallization
iron phosphate glass
Mössbauer spectroscopy
nuclear waste
waste glass
Opis:
60P2O5-40Fe2O3 glass was synthesized and 57Fe Mössbauer spectroscopy study was presented. The main goal of the research was to investigate structural changes of local environment of iron ions during gradual crystallization of the glass. It was observed that some changes were evidenced at temperature of heat treatment higher than 400°C, above which content of tetrahedrally coordinated Fe3+ was increased in cost of octahedral sites. This led to formation of areas of nucleation of α-FePO4. Crystallization of α-Fe3(P2O7)2 and Fe2P2O7 was also observed.
Źródło:
Nukleonika; 2015, 60, 1; 133-136
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hyperfine interactions in x-Bi0.95Dy0.05FeO3-(1-x)-Pb(Fe2/3W1/3)O3 multiferroics
Autorzy:
Zachariasz, P.
Stoch, A.
Stoch, P.
Maurin, J.
Powiązania:
https://bibliotekanauki.pl/articles/147354.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
multiferroics
multifunctional materials
Néel temperature
Opis:
The complex perovskite system xźBi0.95Dy0.05FeO3-(1 - x)źPb(Fe2/3W1/3)O3 was synthesized by the solid-state reaction method and was studied by means of Mössbauer spectroscopy. For different Dy-doped bismuth ferrite (BDF) contents (x = 0.1, 0.3, 0.5, 0.7) the formation of single-phase sinters was confirmed using an X-ray diffraction technique. The random distributions of Fe/W cations in crystallographic structures have been proved. A monotonically, saturation- like increase of Néel temperatures with growing BDF contribution was confirmed, and a straightforward dependence between TN temperatures and the mean hyperfine magnetic fields at Fe nuclei was shown.
Źródło:
Nukleonika; 2013, 58, 1; 53-56
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Integration platform as central service of data replication in distributed medical system
Platforma integracyjna jako centralny system replikacji danych w sieciowym systemie medycznym
Autorzy:
Wajs, W.
Rączka, K.
Stoch, P.
Kruczek, P.
Powiązania:
https://bibliotekanauki.pl/articles/305696.pdf
Data publikacji:
2007
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:
systemy medyczne
replikacja danych
architektura rozproszona
diagram encji
XML
Java
medical system
data replication
distributed architecture
entity relationship diagram
ERD
Opis:
The paper presents the application of Java Integration Platform (JIP) to data replication in the distributed medical system. After an introductory part on the medical system's architecture, the focus shifts to a comparison of different approaches that exist with regard to transferring data between the system's components. A description is given of the historical data processing and of the whole area of the JIP application to the medical system.
Artykuł prezentuje wykorzystanie platformy integracyjnej JIP (Java Integration Platform) do realizacji replikacji danych w sieciowym systemie medycznym. Przedstawiono architekturę systemu medycznego, a następnie porównano różne podejścia do przesyłania danych pomiędzy komponentami systemu. Omówiono również przetwarzanie danych historycznych oraz pełny obszar wykorzystania platformy JIP w systemie medycznym.
Źródło:
Computer Science; 2007, 8, Spec. Ed; 135-142
1508-2806
2300-7036
Pojawia się w:
Computer Science
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and Mössbauer effect studies of Dy(Fe0.4Co0.6-x Alx)2 intermetallics
Autorzy:
Stoch, P.
Pszczoła, J.
Suwalski, J.
Pańta, A.
Powiązania:
https://bibliotekanauki.pl/articles/148809.pdf
Data publikacji:
2003
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
crystal structure
hyperfine interactions
Mössbauer spectroscopy
rare earth
Slater-Pauling curve
transition
Opis:
The magnetic hyperfine fields observed at the 57Fe nuclei (77 K) in the Dy(Mn1-xFex)2 and Dy(Fe1-xCox)2 intermetallics form a Slater-Pauling curve. In order to study the effect of cobalt atoms on crystal structure and hyperfine interactions, the new Co/Al substituted series Dy(Fe0.4Co0.6-xAlx)2 was prepared and data of X-ray powder analysis are presented (300 K). From the 57Fe Mössbauer measurements at 77 K the hyperfine parameters were obtained. The magnetic hyperfine fields form a branch of the Slater-Pauling curve.
Źródło:
Nukleonika; 2003, 48,suppl.1; 75-77
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and Mössbauer Effect Studies of $0.5Bi_{0.95}Dy_{0.05}FeO_{3}-$$0.5Pb(Fe_{2//3}W_{1//3})O_{3}$ Multiferroic
Autorzy:
Stoch, A.
Zachariasz, P.
Stoch, P.
Kulawik, J.
Maurin, J.
Powiązania:
https://bibliotekanauki.pl/articles/1506596.pdf
Data publikacji:
2011-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
61.66.Fn
75.50.Ee
77.84.Lf
Opis:
A polycrystalline ceramic of $0.5Bi_{0.95}Dy_{0.05}FeO_{3}-$ $0.5Pb(Fe_{2//3}W_{1//3})O_{3}$ was synthesized from a solid-state reaction method. At room temperature material exhibits both magnetic and electric dipolar properties simultaneously. Detailed X-ray diffraction analysis and Mössbauer effect studies have been done to determine the crystallographic structure and magnetic properties of $0.5Bi_{0.95}Dy_{0.05}FeO_{3}-$ $0.5Pb(Fe_{2//3}W_{1//3})O_{3}$. $T_{N}$ temperature was estimated at around 600 K.
Źródło:
Acta Physica Polonica A; 2011, 119, 1; 59-61
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural, Electrical and Mössbauer Effect Studies of 0.5Bi $rm_{0.95}Dy_{0.05}FeO_3-0.5Pb(Fe_{0.5}Nb_{0.5})O_3$ Multiferroics
Autorzy:
Stoch, A.
Kulawik, J.
Stoch, P.
Maurin, J.
Zachariasz, P.
Powiązania:
https://bibliotekanauki.pl/articles/1811599.pdf
Data publikacji:
2008-12
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
76.80.+y
77.22.-d
Opis:
$0.5Bi_{0.95}Dy_{0.05}FeO_3-0.5Pb(Fe_{0.5}Nb_{0.5})O_3$ is a multiferroic material which exhibits ferroelectric and antiferromagnetic ordering. (The synthesis of such compounds is rather difficult.) In this paper the way of the synthesis of $0.5Bi_{0.95}Dy_{0.05}FeO_3-0.5Pb(Fe_{0.5}Nb_{0.5})O_3$ is presented. The detailed X-ray and Mössbauer effect studies were done and crystal and hyperfine interaction parameters were obtained. To measure electrical properties of the compound the impedance spectroscopy measurements were performed. The obtained impedance spectra were fitted using a proposed equivalent electrical circuit and the results were discussed in the scope of the brick layer model without easy paths.
Źródło:
Acta Physica Polonica A; 2008, 114, 6; 1585-1590
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Crystal structure and Mössbauer effect in multiferroic 0.5BiFeO3-0.5Pb(Fe0.5Ta0.5)O3 solid solution
Autorzy:
Stoch, A.
Maurin, J.
Stoch, P.
Kulawik, J.
Szwagierczak, D.
Powiązania:
https://bibliotekanauki.pl/articles/146870.pdf
Data publikacji:
2017
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
BiFeO3
crystal structure
hyperfine interactions
multiferroics
solid solution
Opis:
Multiferroic 0.5BiFeO3-0.5Pb(Fe0.5Ta0.5)O3 solid solution is a material that exhibits ferroelectric and antiferromagnetic orderings in ambient temperature. The solid solution was obtained as a result of a conventional reaction in a solid state. The obtained material is a dense, fine-grained sinter whose surface was observed by scanning electron microscopy (SEM) and stoichiometry was confirmed by energy dispersive X-ray spectroscopic (EDS) analysis. According to the X-ray powder diffraction (XRD) measurements, the main phase is R3c space group with admixture of Pm-3m regular phase. Small contribution of pyrochlore-like phase was also observed. Mössbauer spectroscopy suggested random distribution of Fe3+/Ta5+ cations in the B sites of ABO3 compound. Reduction of the magnetic hyperfine field with an increase in the substitution of Ta5+ in Fe3+ neighbourhood was also observed.
Źródło:
Nukleonika; 2017, 62, 2; 177-181
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Magnetoelectric Properties of $0.3Bi_{0.95}Dy_{0.05}FeO_3-0.7Pb(Fe_{2//3}W_{1//3})O_3$ Multiferroic
Autorzy:
Stoch, A.
Stoch, P.
Kulawik, J.
Zieliński, P.
Maurin, J.
Powiązania:
https://bibliotekanauki.pl/articles/1490931.pdf
Data publikacji:
2012-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
75.85.+t
77.22.-d
77.55.Nv
77.80.-e
77.80.Jk
Opis:
Pb-based complex perovskites with $Fe^{3+}$ like $Pb(Fe_{2//3}W_{1//3})O_3$ were found to be interesting because of their unique properties such as relaxor and magnetoelectric behavior. $Pb(Fe_{2//3}W_{1//3})O_3$ is ferroelectric with ferroelectric Curie temperature $T_{C}$ between 150 and 200 K and at the same time is antiferromagnetic with magnetic Néel temperature about 400 K. $BiFeO_3$ is a well known perovskite compound which exhibits ferroelectric ($T_{C}$ = 1103 K) and antiferromagnetic ($T_{N}$ = 643 K) ordering simultaneously. The polycrystalline sample of $0.3Bi_{0.95}Dy_{0.05}FeO_3-0.7Pb(Fe_{2//3}W_{1//3})O_3$ were synthesized using standard sintering procedure. Magnetization vs. magnetic field (at 4.2 K) curves were measured. Magnetoelectric properties of the sample were obtained.
Źródło:
Acta Physica Polonica A; 2012, 121, 1; 128-130
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural and Mössbauer Effect Studies of $0.7Bi_{0.95}Dy_{0.05}FeO_3-$$0.3Pb(Fe_{0.5}Nb_{0.5})O_3$ Multiferroic
Autorzy:
Stoch, A.
Kulawik, J.
Stoch, P.
Maurin, J.
Zachariasz, P.
Powiązania:
https://bibliotekanauki.pl/articles/1506595.pdf
Data publikacji:
2011-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.05.cp
61.66.Fn
75.50.Ee
76.08.+y
77.84.Lf
Opis:
$0.7Bi_{0.95}Dy_{0.05}FeO_{3}-$ $0.3Pb(Fe_{0.5}Nb_{0.5})O_{3}$ is a multiferroic material which exhibits ferroelectric and antiferromagnetic ordering. In this paper the way of the synthesis of $0.7Bi_{0.95}Dy_{0.05}FeO_{3}-$ $0.3Pb(Fe_{0.5}Nb_{0.5})O_{3}$ is presented. The detailed X-ray and Mössbauer effect studies were done and crystal and hyperfine interaction parameters were obtained.
Źródło:
Acta Physica Polonica A; 2011, 119, 1; 56-58
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The role and position of iron in 0.8CaZrO3-0.2CaFe2O4
Autorzy:
Szczerba, J.
Śnieżek, E.
Stoch, P.
Prorok, R.
Jastrzębska, I.
Powiązania:
https://bibliotekanauki.pl/articles/146129.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
calcium ferrite
calcium zirconate
Mössbauer spectroscopy
perovskite
spinel
Opis:
The aim of the study was to characterize the 0.8CaZrO3-0.2CaFe2O4 composite structure with particular emphasis on the role and position of iron in the function of sintering temperature. The paper presents the results of 57Fe Mössbauer effect at room temperature. It was found that the increase of sintering temperature causes an increase in the amount of incorporated iron ions in the CaZrO3-crystal structure. Based on Mössbauer spectroscopy analysis, it was found that three different environments of Fe3+ ions were observed in the obtained materials. Two of them corresponded to CaFe2O4 phase and one was associated with the substitution of Zr4+ by Fe3+ in the CaZrO3 structure.
Źródło:
Nukleonika; 2015, 60, 1; 147-150
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Position of Fe ions in MgO crystalline structure
Autorzy:
Szczerba, J.
Prorok, R.
Stoch, P.
Śnieżek, E.
Jastrzębska, I.
Powiązania:
https://bibliotekanauki.pl/articles/146372.pdf
Data publikacji:
2015
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
Mössbauer spectroscopy
MgO
Fe ions
crystal structure
Opis:
Magnesium oxide (MgO) is one of the most important raw materials in many branches of industry. Magnesium oxide is a popular refractory raw material because of its high refractoriness and high resistance to basic slags and environment. In many cases, use of MgO is limited by its properties, especially the presence of secondary phases like iron oxides. The amount and distribution of iron oxides can strongly infl uence the technological properties of MgO and depend on the manufacturing method, particularly the heat-treatment process. The aim of the study was to evaluate the infl uence of the heat-treatment process on amount and distribution of iron ions in a magnesium oxide lattice. The 57Fe Mössbauer effect measurements of fused and sintered magnesium oxide samples doped by the iron oxide were conducted. Investigation reveals in both cases the presence of Fe2+ as well as Fe3+ ions. Fe2+ ions occupy Mg2+ octahedral sites in the MgO lattice, whereas the Fe3+ ions are located in highly distorted octahedral coordination. The amount of Fe2+ varies from around 66% for fused samples to 30% for sintered samples.
Źródło:
Nukleonika; 2015, 60, 1; 143-145
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mössbauer spectroscopy study of 60P2O5-40Fe2O3 glass
Autorzy:
Stoch, P.
Ciecińska, M.
Zachariasz, P.
Suwalski, J.
Górski, L.
Wójcik, T.
Powiązania:
https://bibliotekanauki.pl/articles/147350.pdf
Data publikacji:
2013
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
iron phosphate glass
Mössbauer spectroscopy
nuclear waste
waste glass
Opis:
A 57Fe Mössbauer spectroscopy study is presented. The main goal of the research was to investigate the structural information of the glass-like the coordination numbers and redox ratio of the iron. Most of the iron, about 80%, is present in the glass as Fe3+, which is composed of tetrahedral (57%) and octahedral (23%) coordinated iron. The rest of the iron, about 20%, is in the oxidation state Fe2+. This iron could be mostly present as VIFe2+, but five-fold coordinated iron is also possible. Finally, the structural model of the synthesized 60P2O5-40Fe2O3 glass was proposed.
Źródło:
Nukleonika; 2013, 58, 1; 63-66
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hyperfine interactions in Ho(Fe1-xCox)2 compounds at 295 K
Autorzy:
Bednarski, M.
Stoch, P.
Bodnar, W.
Zachariasz, P.
Pszczoła, J.
Suwalski, J.
Powiązania:
https://bibliotekanauki.pl/articles/148624.pdf
Data publikacji:
2010
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
intermetallics
crystal structure
Laves phase
Mössbauer effect
hyperfine interaction
Slater-Pauling dependence
Opis:
Synthesis of Ho(Fe1–xCox)2 intermetallic compounds, studies of their crystal structure and 57Fe Mössbauer effect analysis were carried out at 295 K. X-ray measurements evidence a pure cubic Fd3m, C15, MgCu2-type Laves phase. The unit cell parameter decreases non-linearly with composition parameter x. Mössbauer effect spectra for the Ho(Fe1–xCox)2 series were composed of a number of locally originated subspectra due to random Fe/Co nearest neighbourhoods. Hyperfine interaction parameters, i.e. isomer shift, the magnetic hyperfine field and a quadrupole interaction parameter were determined from the fitting procedure of the spectra, for both the individual nearest neighbourhoods, and for the sample as bulk. As a consequence of Fe/Co substitution a Slater-Pauling type curve for the average magnetic hyperfine field vs. x is observed. The correlation between the local magnetic hyperfine fields and the average magnetic hyperfine fields is related to weak and strong ferromagnetism of the transition metal sublattice.
Źródło:
Nukleonika; 2010, 55, 3; 279-284
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mössbauer effect studies of Dy(Fe0.7-xNixCo0.3)2 intermetallics
Autorzy:
Jabłońska, A.
Suwalski, J.
Pszczoła, J.
Guzdek, P.
Stoch, P.
Pańta, A.
Powiązania:
https://bibliotekanauki.pl/articles/147231.pdf
Data publikacji:
2004
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
intermetallics
crystal structure
57Fe Mössbauer effect
hyperfine interactions
Slater-Pauling curve
band structure
Opis:
Abstract A consequence of the Fe/Ni substitution in the series of Dy(Fe0.7 xNixCo0.3)2 was studied in the presented paper. The synthesis and X-ray analysis (300 K) of the Dy(Fe0.7 xNixCo0.3)2 system were performed. The cubic, MgCu2-type, Fd3m crystal structure was evidenced for this solid solution. 57Fe Mössbauer effect measurements for the system were carried out at 77 K. The obtained crystallographic lattice parameters and the hyperfine interaction data are presented. The magnetic hyperfine field values form a separate branch of the Slater-Pauling curve situated above the branch corresponding to the Dy(Fe1 xCox)2 intermetallics.
Źródło:
Nukleonika; 2004, 49,suppl.3; 85-88
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural properties of Mn-substituted hercynite
Autorzy:
Jastrzębska, I.
Bodnar, W.
Witte, K.
Burkel, E.
Stoch, P.
Szczerba, J.
Powiązania:
https://bibliotekanauki.pl/articles/147826.pdf
Data publikacji:
2017
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
FeAl2O4
MnAl2O4
hercynite
spinel
galaxite
Mössbauer spectroscopy
Opis:
In this work spinel series with the general formula Fe1–xMnxAl2O4 (where x = 0, 0.3, 0.5 and 0.7) were synthesized and characterized with respect to their structure and microstructure. X-ray diffractometry (XRD) was used to identify the phase composition that revealed a single phase spinel material. Rietveld refinements of the XRD patterns were carried out in order to determine the lattice and oxygen positional parameters of the spinel compounds. Mössbauer effect measurements were performed at room temperature to determine the local chemical environment of the Fe ions, their valences, and degrees of spinels inversion. It was shown that an increase in the Mn content led to a decrease in the ratio of Fe2+ to Fe3+. The results obtained from Mössbauer spectroscopy (MS) were used to establish the chemical formulas of the synthesized spinels. Finally, the microstructure that was observed using scanning electron microscopy (SEM) showed a compact microstructure with an octahedral crystal habit.
Źródło:
Nukleonika; 2017, 62, 2; 95-100
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 25

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