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    Tytuł:
    Study of Ammonium Perchlorate-based Molecular Perovskite (H2DABCO)[NH4(ClO4)3]/Graphene Energetic Composite with Insensitive Performance
    Autorzy:
    Liu, Yang
    Hu, Li-shuang
    Gong, Shida
    Guang, Chunyu
    Li, Lianqiang
    Hu, Shuangqi
    Deng, Peng
    Powiązania:
    https://bibliotekanauki.pl/articles/1063027.pdf
    Data publikacji:
    2020
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    ammonium perchlorate
    molecular perovskite
    graphene
    energetic composites
    composite desensitization
    Opis:
    In order to improve the safety properties of molecular perovskite energetic materials, ammonium perchlorate-based molecular perovskite ((H2DABCO)[NH4(ClO4)3], DAP)/graphene composite was prepared and characterized. Molecular perovskite DAP was prepared via a molecular assembly strategy by the facile one-pot reaction of triethylenediamine (TEDA, DABCO), perchloric acid, and ammonium perchlorate, and the DAP/graphene composite was fabricated by mechanical mixing with 10 wt.% graphene. The results demonstrated that impact sensitivity (>120 cm), friction sensitivity (25%) and electrostatic spark sensitivity (7.04 J) of the DAP/graphene composite was less sensitive than raw DAP (impact, friction and electrostatic spark sensitivity: 112.3 cm, 45%, and 5.39 J, respectively), due to the composite desensitization mechanism of graphene. This work may offer new ideas for the design and fabrication of insensitive molecular perovskite-based energetic composites.
    Źródło:
    Central European Journal of Energetic Materials; 2020, 17, 3; 451-469
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study of Molecular Perovskite (H2dabco)[NH4(ClO4)3]/Carbon Nanotubes Energetic Composite
    Autorzy:
    Hu, Li-shuang
    Liu, Yang
    He, Dan
    Yang, Yajun
    Gong, Shida
    Guang, Chunyu
    Deng, Peng
    Hu, Shuangqi
    Powiązania:
    https://bibliotekanauki.pl/articles/27788083.pdf
    Data publikacji:
    2022
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    ammonium perchlorate
    (H2dabco)[NH4(ClO4)3]
    carbon nanotubes
    mechanical sensitivity
    thermal stability
    Opis:
    An ammonium perchlorate (AP, NH4(ClO4)3)-based molecular perovskite energetic material (H2dabco)[NH4(ClO4)3]/carbon nanotubes (DAP/CNTs) composite was prepared and characterized. Molecular perovskite DAP samples were synthesized by a facile one-pot reaction of triethylenediamine, perchloric acid (PCA, HClO4), and AP via a molecular assembly strategy. The results showed that the mechanical sensitivity (impact and friction sensitivities: >120 cm and 20%) and electrostatic spark sensitivity (8.90 J) of the DAP/CNTs energetic composite with 10 wt.% CNTs exhibited less sensitivity than that of DAP (impact, friction and electrostatic spark sensitivities: 112.3 cm, 45%, and 5.39 J, respectively), because of the mixing desensitization mechanism of CNTs. Compared with the pure DAP, the DAP/CNTs energetic composite has better performance with respect to thermal stability, exothermic capacity, and excellent continuous combustion properties. The DAP/CNTs energetic composite has potential application in a weapons system.
    Źródło:
    Central European Journal of Energetic Materials; 2022, 19, 1; 91--105
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Green Fabrication of Nanoscale Energetic Molecular Perovskite (H2dabco)[Na(ClO4)3] with Reduced Mechanical Sensitivity
    Autorzy:
    Hu, Li-shuang
    Du, Zelin
    Liu, Yang
    Gong, Shida
    Guang, Chunyu
    Li, Xin
    Yang, Zhi
    Jia, Qi
    Liang, Kaili
    Powiązania:
    https://bibliotekanauki.pl/articles/27787996.pdf
    Data publikacji:
    2021
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    molecular perovskite
    (H2dabco)[Na(ClO4)3]
    ball milling
    thermal decomposition
    mechanical sensitivity
    Opis:
    High-energy-density molecular perovskite energetic materials with high detonation performance have attracted much attention, but poor safety performance has limited their potential applications. In this paper, nano sodium perchlorate-based molecular perovskite (H2dabco)[Na(ClO4)3] (nano DAP-1) was fabricated by green ball-milling technology. The structure and morphology of the samples were characterized and the results showed that nano DAP-1 with nearly spherical morphology has a narrow particle size distribution, < 1 μm. The thermal decomposition properties were investigated by differential scanning calorimetry (DSC). The exothermic peak of nano DAP-1 thermal decomposition was 330.0 °C, a decrease of 51.7 °C compared with that of raw DAP (381.7 °C). The apparent activation energy (Ea) of nano DAP-1 was calculated to be 160.9 kJ·mol–1, which is lower than that of raw DAP-1 (168.6 kJ·mol–1). Mechanical sensitivity studies showed that nano DAP-1 (H50: 64 cm) exhibited a lower impact sensitivity than that of the raw DAP-1 (H50: 51 cm). This work provides a simple and effective way for improving the thermal decomposition properties and safety performance of molecular perovskite energetic materials.
    Źródło:
    Central European Journal of Energetic Materials; 2021, 18, 3; 369--384
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-3 z 3

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