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    Wyświetlanie 1-13 z 13
    Tytuł:
    Identification of three species commonly known as“daqingye” by internal leaf anatomy and high-performance liquid chromatography analyses
    Autorzy:
    Zhang, Y.
    Zhu, Y.
    Chen, J.
    Xia, C.
    Deng, J.
    Li, H.
    Li, Y.
    Li, J.
    Liu, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/59301.pdf
    Data publikacji:
    2018
    Wydawca:
    Polskie Towarzystwo Botaniczne
    Opis:
    The macroscopic and microscopic morphologies and indigo and indirubin concentration of the traditional Chinese medicine herbs Isatis indigotica Fort., Polygonum tinctorium Ait., and Baphicacanthus cusia (Nees) Bremek, all commonly known as “daqingye”, were determined and compared. The morphological analyses indicated that I. indigotica has leaves with winged petioles and no glandular hairs or crystals, P. tinctorium has leaves with membranous ocrea and clusters of calcium oxalate, and B. cusia has palisade cells in the mesophyll running over the main vein and single cells containing calcium carbonate crystals. Indigo and indirubin are chemical constituents that have been previously isolated from daqingye and were selected in this study as identification markers for high-performance liquid chromatography analysis due to their pharmacological activities. The chromatographic results showed that indigo and indirubin concentration varied significantly among the three species: high concentration of both indigo and indirubin were observed in I. indigotica, the highest concentration among the three daqingye plants was found in P. tinctorium but with low levels of indirubin, and the concentration of indigo and indirubin was quite low in B. cusia. In summary, three different species commonly known as daqingye were accurately distinguished by morphological observation, internal leaf anatomy analysis, and chromatographic analysis.
    Źródło:
    Acta Societatis Botanicorum Poloniae; 2018, 87, 1
    0001-6977
    2083-9480
    Pojawia się w:
    Acta Societatis Botanicorum Poloniae
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Stability analysis and H∞ control of discrete T–S fuzzy hyperbolic systems
    Autorzy:
    Duan, R.
    Li, J.
    Zhang, Y.
    Yang, Y.
    Chen, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/331173.pdf
    Data publikacji:
    2016
    Wydawca:
    Uniwersytet Zielonogórski. Oficyna Wydawnicza
    Tematy:
    discrete T–S fuzzy hyperbolic model
    parallel distributed compensation
    positive diagonally dominant matrices
    robust stability
    model Takagi-Sugeno
    kompensacja rozproszona
    sterowanie odporne
    Opis:
    This paper focuses on the problem of constraint control for a class of discrete-time nonlinear systems. Firstly, a new discrete T–S fuzzy hyperbolic model is proposed to represent a class of discrete-time nonlinear systems. By means of the parallel distributed compensation (PDC) method, a novel asymptotic stabilizing control law with the “soft” constraint property is designed. The main advantage is that the proposed control method may achieve a small control amplitude. Secondly, for an uncertain discrete T–S fuzzy hyperbolic system with external disturbances, by the proposed control method, the robust stability and H∞ performance are developed by using a Lyapunov function, and some sufficient conditions are established through seeking feasible solutions of some linear matrix inequalities (LMIs) to obtain several positive diagonally dominant (PDD) matrices. Finally, the validity and feasibility of the proposed schemes are demonstrated by a numerical example and a Van de Vusse one, and some comparisons of the discrete T–S fuzzy hyperbolic model with the discrete T–S fuzzy linear one are also given to illustrate the advantage of our approach.
    Źródło:
    International Journal of Applied Mathematics and Computer Science; 2016, 26, 1; 133-145
    1641-876X
    2083-8492
    Pojawia się w:
    International Journal of Applied Mathematics and Computer Science
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Flotation behavior of hard-to-separate and high-ash fine coal
    Autorzy:
    Xing, Y.
    Gui, X.
    Liu, J.
    Cao, Y.
    Zhang, Y.
    Li, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/110585.pdf
    Data publikacji:
    2016
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    flotation behavior
    fine coal
    Fuerstenau upgrading curve
    energy input
    selectivity
    Opis:
    The flotation behavior of hard-to-separate and high-ash fine coal was investigated using conventional flotation with constant power input. A new flotation process, based on energy input and distribution, was designed to lower the ash content of concentrate. The results obtained using Fourier transform infrared (FTIR) analysis show that the coal samples have good floatability because of many hydrophobic and few hydrophilic functional groups. Under a constant power input, a large number of ash-forming materials floated into a froth product at the start of flotation. Based on the Fuerstenau upgrading curves, it was determined that the 0.25-0.074 mm size fraction range showed the worst selectivity when compared with 0.50-0.25 mm and -0.074 mm size fractions. The desired concentrate with an ash content of 13.98%, 27.59% of ash recovery, and 80.01% combustible matter recovery could be obtained by transferring the excess energy of the flotation-conditioning stage to the pre-conditioning stage and increasing the power input step-by-step in the flotation-conditioning stage at equal total energy consumption.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2016, 52, 2; 703-717
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    New compensation scheme of magneto-optical current sensor for temperature stability improvement
    Autorzy:
    Chen, J.
    Li, H.
    Zhang, M.
    Zhang, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/221874.pdf
    Data publikacji:
    2012
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    magneto-optical current sensor
    normalization
    Verdet constant
    birefringence
    Opis:
    A novel magneto-optical current sensor (MOCS) with two sensing arms is proposed to improve the temperature stability. One of the arms, with a highly stable permanent magnet attached and orthogonal to the other one, is designed to provide a reference that follows the temperature characteristics of the sensing material. By a normalization operation between two arms, the temperature drift is compensated adaptively and a sensing output proportional to the measured current can be reached. A dual-input and dual-output structure is specially designed for the reference sensing arm to demodulate the DC Faraday rotation angle. This scheme compensates simultaneously two main temperature influence factors, the Verdet constant and linear birefringence. Validation tests were carried out and are discussed.
    Źródło:
    Metrology and Measurement Systems; 2012, 19, 3; 611-616
    0860-8229
    Pojawia się w:
    Metrology and Measurement Systems
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Modification Mechanism and Growth Process of Al3(Sc, Zr) Particles in As-cast Al-Si-Mg-Cu-Zr-Sc Alloy
    Autorzy:
    Li, Y.
    Du, X.
    Fu, J.
    Zhang, Y.
    Zhang, Z.
    Zhou, S.
    Wu, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/382672.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    solidification process
    Al3(Sc, Zr)
    three-dimensional morphology
    eutectic growth
    krzepnięcie stopu
    morfologia trójwymiarowa
    wzrost eutektyczny
    Opis:
    In this study, the modification mechanism and growth process of Al3(Sc, Zr) particles in as-cast Al-Si-Mg-Cu based alloy with addition of Sc and Zr were systematically investigated. It was found that 0.57 wt-%Sc addition caused a significant refinement in the average grain size of the investigated alloy, which brought about a remarkable transformation in as-cast microstructure, from thick dendritic shape to fine equiaxed structure. A large amount of primary Al3(Sc, Zr) particles with the dimension of around 5-6 μm were also observed within the equiaxed grain. Due to the identical orientation and similar crystal structure between primary Al3(Sc, Zr) particles and α-Al matrix, the primary particles always served as heterogeneous nucleus for the α-Al matrix. In addition, these cusped cubic primary Al3(Sc, Zr) particles showed triangle, star, rhomboid morphologies are generated from sectioning the particle in (111), (100) and (110) planes, respectively. Particularly, the typical eutectic structure which contained odd number-layer (Al3(Sc, Zr)+α-Al+ ... +Al3(Sc, Zr)) was observed within the investigated particles.
    Źródło:
    Archives of Foundry Engineering; 2018, 18, 2; 51-56
    1897-3310
    2299-2944
    Pojawia się w:
    Archives of Foundry Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    An improved Otsu method for oil spill detection from SAR images
    Autorzy:
    Yu, F.
    Sun, W.
    Li, J.
    Zhao, Y.
    Zhang, Y.
    Chen, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/47553.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Instytut Oceanologii PAN
    Tematy:
    remote sensing
    oil spill
    detection
    Otsu's method
    accident
    marine transport
    synthetic aperture radar
    Opis:
    In recent years, oil spill accidents have become increasingly frequent due to the development of marine transportation and massive oil exploitation. At present, satellite remote sensing is the principal method used to monitor oil spills. Extracting the locations and extent of oil spill spots accurately in remote sensing images reaps significant benefits in terms of risk assessment and clean-up work. Nowadays the method of edge detection combined with threshold segmenta- tion (EDCTS) to extract oil information is becoming increasingly popular. However, the current method has some limitations in terms of accurately extracting oil spills in synthetic aperture radar (SAR) images, where heterogeneous background noise exists. In this study, we propose an adaptive mechanism based on Otsu method, which applies region growing combined with both edge detection and threshold segmentation (RGEDOM) to extract oil spills. Remote sensing images from the Bohai Sea on June 11, 2011 and the Gulf of Dalian on July 17, 2010 are utilized to validate the accuracy of our algorithm and the reliability of extraction results. In addition, results according to EDCTS are used as a comparator to further explore validity. The comparison with results according to EDCTS using the same dataset demonstrates that the proposed self-adapting algorithm is more robust and boasts high-accuracy. The accuracy computing by the adaptive algorithm is significantly improved compared with EDCTS and threshold method.
    Źródło:
    Oceanologia; 2017, 59, 3
    0078-3234
    Pojawia się w:
    Oceanologia
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study on optimization simulation of SCR denitration system for marine diesel engine
    Autorzy:
    Du, J.
    Li, R. N.
    Wu, X.
    Zhang, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/259646.pdf
    Data publikacji:
    2018
    Wydawca:
    Politechnika Gdańska. Wydział Inżynierii Mechanicznej i Okrętownictwa
    Tematy:
    marine diesel engine
    SCR system
    flue gas
    flow deflector
    Opis:
    With the rapid development of shipbuilding industry exhaust world is also very harmful one kind of environmental issues, and the ship marine diesel engine exhaust gas is mainly produced, so in recent years it has developed a diesel engine SCR system. SCR system can control emissions of nitrogen oxides in the exhaust of vessel, furthermore air pollution can be reduced. The main goal of article was using fluent software to correct SCR system selection and flue gas flow under different size best deflector arrangement is simulated. Next goal is further optimize the structure of the SCR system.
    Źródło:
    Polish Maritime Research; 2018, S 3; 13-21
    1233-2585
    Pojawia się w:
    Polish Maritime Research
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Reliability analysis of the products subject to competing failure processes with unbalanced data
    Oparta na niezbilansowanych danych analiza niezawodności produktów podlegających procesom powstawania uszkodzeń konkurujących
    Autorzy:
    Li, J.
    Zhang, Y.
    Wang, Z.
    Fu, H.
    Xiao, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/1365849.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Polskie Naukowo-Techniczne Towarzystwo Eksploatacyjne PAN
    Tematy:
    reliability evaluation
    competing failure model
    unbalanced data
    interval statistics
    ocena niezawodności
    model uszkodzeń konkurujących
    dane niezbilansowane
    statystyki przedziałowe
    Opis:
    Considering the degradation and catastrophic failure modes simultaneously, a general reliability analysis model was presented for the competing failure processes with unbalanced data. For the degradation process with highly unbalanced data, we developed a linear random-effects degradation model. The model parameters can be estimated based on a simple least square method. Furthermore, to fully utilize the degradation information, we considered the last measured times of the degradation units that had only one or two measured time points as zero-failure data or right-censored data of the catastrophic failure mode. Then the incomplete data set was composed of zero-failure data and catastrophic failure data. To analyze the incomplete data, the definition of the interval statistics was firstly given. The best linear unbiased parameter estimators of catastrophic failure were obtained based on the Gauss-Markov theorem. Then, the reliability function of the competing failure processes was given. The corresponding two-sided confidence intervals of the reliability were obtained based on a bootstrap procedure. Finally, a practical application case was examined by applying the proposed method and the results demonstrated its validity and reasonability.
    W pracy przedstawiono ogólny model analizy niezawodności procesów związanych z powstawaniem uszkodzeń konkurujących, który pozwala na wykorzystanie danych niezbilansowanych oraz umożliwia jednoczesne uwzględnienie uszkodzeń wynikających z obniżenia charakterystyk i uszkodzeń katastroficznych. Opracowano liniowy model efektów losowych dla procesu degradacji o wysoce niezbilansowanych danych. Parametry tego modelu można określić na podstawie prostej metody najmniejszych kwadratów. Ponadto, aby w pełni wykorzystać informacje dotyczące obniżenia charakterystyk, dane pochodzące z ostatniego pomiaru jednostek podlegających degradacji, dla których przeprowadzono tylko jeden lub dwa pomiary, rozpatrywano jako dane o zerowym uszkodzeniu lub jako ucięte prawostronnie dane dotyczące uszkodzenia katastroficznego. W ten sposób otrzymano zbiór niepełnych danych składający się z danych o uszkodzeniach zerowych oraz danych o uszkodzeniach katastroficznych. Aby móc przeanalizować uzyskane niepełne dane, podano definicję statystyki przedziałowej. Najefektywniejszy nieobciążony estymator liniowy (BLUE) parametrów uszkodzeń katastroficznych uzyskano na podstawie twierdzenia Gaussa-Markowa. Następnie, podano wzór funkcji niezawodności procesów związanych z powstawaniem uszkodzeń konkurujących. Odpowiednie dwustronne przedziały ufności dla oszacowanej niezawodności uzyskano metodą bootstrapową. Na koniec, przedstawiono przypadek praktycznego zastosowania proponowanej metody, którego wyniki wykazały jej trafność i zasadność.
    Źródło:
    Eksploatacja i Niezawodność; 2016, 18, 1; 98-109
    1507-2711
    Pojawia się w:
    Eksploatacja i Niezawodność
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Interaction of Water with Glycine: A Combined Inelastic Neutron Scattering and Raman Spectra Studies
    Autorzy:
    Zhang, P.
    Zhang, Y.
    Han, S.
    Yan, Q.
    Li, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/2044762.pdf
    Data publikacji:
    2006-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    36.20.Ng
    87.64.Je
    25.40.Fq
    82.30.Rs
    Opis:
    The vibrational dynamics of water around glycine was investigated by using Raman spectroscopy and inelastic neutron scattering. Experiments of deuterated glycine versus deuterium were performed as comparison. The study shows that for glycine, the exchange of proton-deuteron on the active NH$\text{}_{3}^{+}$ side was easy, whereas there was hardly exchange on the CH$\text{}_{2}$ side. Comparing different proportion of glycine vs. water molecules we obtained that the presence of water hardly changes the main features of glycine illustrating its hydrophobic character. The intralayer hydrogen bonds of glycine crystal are difficult to be replaced due to its stronger bond than water.
    Źródło:
    Acta Physica Polonica A; 2006, 109, 3; 399-404
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Experimental and numerical study of the uniaxial compressive stress-strain relationship of a rock mass with two parallel joints
    Autorzy:
    Xiong, L. X.
    Yuan, H. Y.
    Zhang, Y.
    Zhang, K. F.
    Li, J. B.
    Powiązania:
    https://bibliotekanauki.pl/articles/231076.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    masa skalna łączona
    złącze równoległe
    siła szczytowa
    jointed rock mass
    parallel joint
    peak strength
    Opis:
    A “rock bridge”, defined as the closest distance between two joints in a rock mass, is an important feature affecting the jointed rock mass strength. Artificial jointed rock specimens with two parallel joint fractures were tested under uniaxial compression and numerical simulations were carried out to study the effects of the inclination of the rock bridge, the dip angle of the joint, rock bridge length, and the length of joints on the strength of the jointed rock mass. Research results show: (1) When the length of the joint fracture, the length of the rock bridge, and the inclination of the rock bridge stay unchanged, the uniaxial compressive strength of the specimen gradually increases as the inclination of the joint fracture increases from 0° to 90°. (2) When the length of the joint fracture, the length of the rock bridge, and the inclination of the joint fracture stay unchanged, the uniaxial compressive strength of the specimen shows variations in trends with the inclination of the rock bridge increasing from 30° to 150° (3). In the case when the joint is angled from the vertical loading direction, when the dip angle of the joint fracture, the inclination of the rock bridge, and the length of the rock bridge stay unchanged, the uniaxial compressive strength of the specimen gradually decreases with an increasing length of joint fracture. When the dip angle of the joint fracture, the inclination of the rock bridge, and the length of the joint fracture stay unchanged, the uniaxial compressive strength of the specimen does not show a clear trend with an increase of the length of the rock bridge.
    Źródło:
    Archives of Civil Engineering; 2019, 65, 2; 67-80
    1230-2945
    Pojawia się w:
    Archives of Civil Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A novel Wiener process model with measurement errors for degradation analysis
    Analiza degradacji z zastosowa niem nowego modelu procesu Wienera uwzględniającego błędy pomiarowe
    Autorzy:
    Wang, Z.
    Li, J.
    Zhang, Y.
    Fu, H.
    Liu, C.
    Krishnaswamy, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/301209.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Polskie Naukowo-Techniczne Towarzystwo Eksploatacyjne PAN
    Tematy:
    performance degradation
    independent increment process
    Wiener process model
    linear mean function
    linear standard deviation function
    measurement error
    obniżenie charakterystyk
    proces o przyrostach niezależnych
    model procesu Wienera
    funkcja średniej liniowej
    funkcja liniowego odchylenia standardowego
    błąd pomiaru
    Opis:
    Degradation analysis can be used to assess reliability for complex systems and highly reliable products, because few or even no failures are expected in a reasonable life test span. In order to further our study on degradation analysis, an independent increment random process method with linear mean and standard deviation functions is presented to model practical degradation procedures. It is essentially a Wiener process method. Since measurement errors are often created by imperfect instruments, procedures and environments during degradation investigation, the measurement error is incorporated into the independent increment random process. Furthermore, statistical inferences of this model are discussed, and close forms of a product’s median life and percentile of the failure time distribution (FTD) are also derived. The proposed method is illustrated and verified in a comprehensive simulation study and two practice applications for storage disks and Infrared light-emitting diodes. Meanwhile, the time-transformed Wiener process model with measurement error is considered as a reference method. Comparisons show that the proposed model can provide reasonable results, even in considerably small sample size circumstance.
    Analizę degradacji można stosować do oceny niezawodności wysoce niezawodnych złożonych systemów i produktów, ponieważ w ich przypadku istnieje bardzo niskie lub zerowe prawdopodobieństwo wystąpienia uszkodzenia w trakcie badania trwałości w przyjętym okresie eksploatacji. W artykule przedstawiono nowo opracowane podejście do modelowania procesu degradacji wykorzystujące metodę procesu o przyrostach niezależnych oraz pojęcia funkcji średniej liniowej i funkcji liniowego odchylenia standardowego. Zasadniczo jest to metoda oparta na procesie Wienera. Ponieważ badania degradacji często wiążą się z błędami pomiarowymi wynikającymi z niedoskonałości stosowanych narzędzi, procedur i warunków badawczych, opisywany proces o przyrostach niezależnych uwzględnia błędy pomiaru. Ponadto, w pracy omówiono wnioski statystyczne, jakie można wyciągnąć na podstawie przedstawionego modelu oraz wyprowadzono wzory ogólne na średnią długość życia produktu oraz na percentyl rozkładu czasu do uszkodzenia. Proponowaną metodę zilustrowano i zweryfikowano na podstawie kompleksowego badania symulacyjnego oraz przykładów praktycznego zastosowania modelu w odniesieniu do dysków pamięci masowej oraz diod podczerwieni. W artykule przedstawiono także model procesu Wienera z transformowanym czasem uwzględniający błąd pomiaru, który posłużył za model referencyjny. Porównania pokazują, że proponowany model może dawać poprawne wyniki, nawet przy bardzo małej liczebności próby.
    Źródło:
    Eksploatacja i Niezawodność; 2016, 18, 3; 396-405
    1507-2711
    Pojawia się w:
    Eksploatacja i Niezawodność
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Modulation of virulence genes by the two-component system PhoP - PhoQ in avian pathogenic Escherichia coli
    Autorzy:
    Tu, J.
    Huang, B.
    Zhang, Y.
    Xue, T.
    Li, S.
    Qi, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/30418.pdf
    Data publikacji:
    2016
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Opis:
    Avian pathogenic Escherichia coli (APEC) infections are a very important problem in the poultry industry. PhoP-PhoQ is a two-component system that regulates virulence genes in APEC. In this study, we constructed strains that lacked the PhoP or PhoQ genes to assess regulation of APEC pathogenicity by the PhoP-PhoQ two-component system. The PhoP mutant strain AE18, PhoQ mutant strain AE19, and PhoP/PhoQ mutant strain AE20 were constructed by the Red homologous recombination method. Swim plates were used to evaluate the motility of the APEC strains, viable bacteria counting was used to assess adhesion and invasion of chick embryo fibroblasts, and Real-Time PCR was used to measure mRNA expression of virulence genes. We first confirmed that AE18, AE19, and AE20 were successfully constructed from the wild-type AE17 strain. AE18, AE19, and AE20 showed significant decreases in motility of 70.97%, 83.87%, and 37.1%, respectively, in comparison with AE17. Moreover, in comparison with AE17, AE18, AE19, and AE20 showed significant decreases of 63.11%, 65.42%, and 30.26%, respectively, in CEF cell adhesion, and significant decreases of 59.83%, 57.82%, and 37.90%, respectively, in CEF cell invasion. In comparison with AE17, transcript levels of sodA, polA, and iss were significantly decreased in AE18, while transcript levels of fimC and iss were significantly decreased in AE19. Our results demonstrate that deletion of PhoP or PhoQ inhibits invasion and adhesion of APEC to CEF cells and significantly reduces APEC virulence by regulating transcription of virulence genes.
    Źródło:
    Polish Journal of Veterinary Sciences; 2016, 19, 1
    1505-1773
    Pojawia się w:
    Polish Journal of Veterinary Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation and Characterization of Ultrafine HMX/TATB Explosive Co-crystals
    Autorzy:
    An, C.
    Li, H.
    Zhang, Y.
    Ye, B.
    Xu, C.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358105.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    HMX
    TATB
    ultrafine co-crystals
    ball milling
    mechanical sensitivity
    Opis:
    An explosive co-crystal of 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane (HMX) and 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) was prepared by the ball milling method. The raw materials and co-crystals were characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and Raman spectroscopy. Impact and friction sensitivity of the co-crystals were tested and analyzed. The results showed that the HMX/TATB co-crystals are spherical in shape and 100-300 nm in size. The co-crystals are different from anintimate mixture of HMX/TATB and they exhibit a new co-crystal structure. HMX/TATB co-crystals are formed by N-O···H hydrogen bonding between −NO2 (HMX) and −NH2 (TATB). The drop height of ultrafine HMX/TATB explosive co-crystals is 12.7 cm higher than that of ultrafine HMX, whilst the explosion probability of friction is 20% lower than that of ultrafine HMX. Ultrafine HMX/TATB explosive co-crystals are difficult to initiate under impact and friction conditions.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 4; 876-887
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-13 z 13

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