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    Wyświetlanie 1-6 z 6
    Tytuł:
    Preparation, characterization and rheological behavior of chitosan nanocapsule emulsion encapsulated tuberose fragrance
    Autorzy:
    Xiao, Z.
    Wang, E.
    Zhu, G.
    Zhou, R.
    Niu, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/778241.pdf
    Data publikacji:
    2016
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    chitosan nanocapsules
    encapsulation
    rheological
    viscoelasticity
    particle size
    Opis:
    In this paper, ionic gelation method was adopted to produce nanocapsules (CNs) encapsulated tuberose fragrance with chitosan (CS) and sodium tripolyphosphate (TPP) as wall materials. The effects of CS/TPP mass ratio, pH value of CS solution, molecular mass of CS and tuberose fragrance (TF) concentration on particle size and particle size distribution (PDI) of chitosan nanocapsules encapsulated tuberose fragrance (CNTs) were investigated systematically. CNTs were characterized by dynamic light scattering (DLS), scanning electron microscopy (SEM), Fourier transforms infrared spectroscopy (FTIR), X-ray diffraction (XRD), thermogravimetric analyzer (TGA) and differential scanning calorimetry (DSC). The results showed that CNTs were successfully prepared. The optimum preparation conditions were as follows: CS/TPP mass ratio 5:1, pH of CS solution 4.0, and molecular mass of CS 150 kda. CNTs emulsions were also systematically investigated by steady-state shear and oscillatory shear measurements respectively. The rheological behaviors of CNTs were obtained.
    Źródło:
    Polish Journal of Chemical Technology; 2016, 18, 2; 1-8
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Pyrolysis characteristics and kinetics of β-cyclodextrin and its two derivatives
    Autorzy:
    Zhu, G.
    Xiao, Z.
    Zhou, R.
    Niu, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/779364.pdf
    Data publikacji:
    2015
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    Pyrolysis characteristics
    kinetics
    β-cyclodextrin
    Hydroxypropyl-β-cyclodextrin
    Monochlorotriazinyl-β-cyclodextrin
    Opis:
    β-cyclodextrin (β-CD) and its derivatives have been widely used to prepare inclusion complexes. However, systematic research on their thermal stabilities, pyrolysis characteristics and kinetics has rarely been reported. In this paper, thermogravimetric analysis was employed to investigate β-cyclodextrin and its two derivatives, 2-Hydroxypropyl-β-cyclodextrin (HP-β-CD) and monochlorotriazinyl-β-cyclodextrin (MCT-β-CD). The pyrolysis characteristics and kinetic parameters were obtained. The results show that three stages can be distinguished during the heating process of the above three samples. The temperature of initial decomposition of HP-β-CD (309.5°C is higher than that of β-CD (297.8°C), while the temperature of initial decomposition of MCT-β-CD (231.4°C) is lower than that of β-CD. For the three cyclodextrins, the thermal stability in descending order is HP-β-CD, β-CD and MCT-HP-β-CD. The activation energy values are 350.6, 303.3 and 113.9 KJ/mol, and the pre-exponential factor values are 1.11×1031, 1.37×1026 and 1.39×1010 for β-CD, HP-β-CD and MCT-β-CD respectively.
    Źródło:
    Polish Journal of Chemical Technology; 2015, 17, 4; 1-4
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation of micro-encapsulated strawberry fragrance and its application in the aromatic wallpaper
    Autorzy:
    Xiao, Z.
    Zhang, Y.
    Zhu, G.
    Niu, Y.
    Xue, Z.
    Zhu, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/778533.pdf
    Data publikacji:
    2017
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    micro-encapsulation
    fragrance
    wallpaper
    controlled release
    Opis:
    Micro-encapsulated strawberry fragrance was successfully prepared with wall materials including maltodextrin, sodium octenylsuccinate and gum Arabic. The micro-capsule was added to wallpaper and aromatic wallpaper with strawberry characteristics was obtained. The particle distribution, surface morphology, chemical structure, thermal property and controlled release performance of micro-encapsulated fragrance and aromatic wallpaper were investigated using laser particle size analyzer, scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FT-TR), thermal gravity analysis (TGA) and chromatography-mass spectrometer (GC-MS). The results showed that the average diameter of micro-capsule was 2 μm and the particles mainly distributed in the tissues of wallpaper. The result of TGA showed that the micro-capsule had a good stability. Meanwhile, the aromatic wallpaper had strawberry aroma more than 3 months and took on excellent controlled release performance.
    Źródło:
    Polish Journal of Chemical Technology; 2017, 19, 1; 89-94
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Encapsulation of l-menthol in hydroxypropyl-β-cyclodextrin and release characteristics of the inclusion complex
    Autorzy:
    Zhu, G.
    Xiao, Z.
    Zhou, R.
    Niu, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/778623.pdf
    Data publikacji:
    2016
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    l-menthol
    inclusion complex
    release characteristics
    binding energy
    release kinetics
    Opis:
    l-menthol has been widely used in flavour, food and pharmaceuticals. Because of its high volatility and whisker growth, l-menthol-hydroxypropyl-β-cyclodextrin inclusion complex was produced to improve shelf-life, provide protection, and enhance the stability of l-menthol. The inclusion complex was characterized by Fourier transform infrared spectroscopy, X-ray diffraction. The results show that l-menthol was successfully encapsulated in hydroxypropyl-β-cyclodextrin. l-menthol loading capacity is about 8.44%. Geometries and binding energies of l-menthol-hydroxypropyl-β-cyclodextrin inclusion complexes were investigated using molecular mechanics calculations. The shape and orientation of the most stable complex, and the minimum binding energy were determined. L-menthol release from complex was determined by thermogravimetric analysis. Two l-menthol release rate peaks were observed at 69.3 and 279.1°C. The l-menthol release reaction order, release activation energy and the preexponential factor were obtained.
    Źródło:
    Polish Journal of Chemical Technology; 2016, 18, 3; 110-116
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Modelling and Calculation of the Initial Ignition Gas Pressure Flow through a Rigid Porous Medium in a 100 mm Ignition Simulator
    Autorzy:
    Xiao, Z.
    Ying, S.
    He, W.
    Xu, F.
    Powiązania:
    https://bibliotekanauki.pl/articles/358563.pdf
    Data publikacji:
    2014
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    ignition
    ignition simulator
    porous media
    propellant
    modelling
    simulation
    Opis:
    To acquire a better understanding of the early ignition phenomena in a 100 mm ignition simulator loaded with a packed propellant bed, a theoretical model of the ignition gas flow through the rigid porous medium was developed. Three pressure gauges were installed in the lateral side of the ignition simulator for post ignition measurement of the chamber pressure. The pseudo-propellant loaded into the chamber was similar in size to the standard 13/19 single-base cylindrical propellant. It was composed of a rigid ceramic composite with low thermal conductivity. It was assumed that the pseudo-propellant bed was rigid in contrast to the assumption of an elastic porous medium. The calculated pressure values were well verified by the experimental data at a low loading density of the pseudo-propellant bed of 0.18 g•cm-3. However, there was still error between the experimental and the calculated results in the early pressure peak position closest to the ignition primer when the loading density of the pseudo-propellant bed was increased to 0.73 and 1.06 g•cm-3. This error is attributed to the change in local permeability of the pseudo-propellant bed at high loading densities, which is assumed, for ease of modelling, to be constant in the model. These calculations may enable a better understanding of the physical processes of ignition gas flow in an ignition simulator loaded with a pseudo-propellant bed.
    Źródło:
    Central European Journal of Energetic Materials; 2014, 11, 4; 475-489
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects of Holding Conditions on Microstructure of Al-5Ti-1B and Its Refining Efficiency on Al-Cu Alloy
    Autorzy:
    Huang, Y.
    Shao, H.
    Xiao, Z.
    Ren, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/353764.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-5Ti-1B
    holding condition
    microstructure
    refining efficiency
    Opis:
    A series of Al-5Ti-1B master alloys were obtained via fluoride salt process by holding them between 780°C and 880°C for 10-90 min. The influence of holding temperature and time during preparation on the microstructure and its refining performance were investigated by X-ray diffractometer, optical microscopy and scanning electron microscopy equipped with energy dispersive X-ray spectroscopy. The results indicated both the morphology and the distribution of TiB22and Al3Ti were seriously affected by holding conditions. Inadequate TiB2 particles were generated when holding time was short. However, Fe-containing impurity particles that aggregated along the matrix grain boundaries were found after the prolonged holding time. The refining and microhardness test results revealed that Al-5Ti-1B, the one held at 820°C for 30 min showed the optimum refining efficiency on Al-Cu alloy.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 2; 647-652
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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