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    Wyświetlanie 1-6 z 6
    Tytuł:
    Microstructure And Thermoelectric Properties Of TAGS-90 Compounds Fabricated By Mechanical Milling Process
    Mikrostruktura i właściwości termoelektryczne związków TAGS-90 wytworzonych przez mielenie
    Autorzy:
    Kim, H.-S.
    Babu, M.
    Hong, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/353404.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    TAGS-90
    thermoelectric properties
    high-energy milling
    SPS
    właściwości termoelektryczne
    mielenie wysokoenergetyczne
    Opis:
    TAGS-90 compound powder was directly prepared from the elements by high-energy ball milling (HEBM) and subsequently consolidated by a spark plasma sintering (SPS). Effect of milling time on the microstructure and thermoelectric properties of the samples were investigated. The particle size of fabricated powders were decreased with increasing milling time, finally fine particles with ~1μm size was obtained at 90 min. The SPS samples exhibited higher relative densities (>99%) with fine grain size. X-ray diffraction analysis (XRD) and energy dispersion analysis (EDS) results revealed that all the samples were single phase of GeTe with exact composition. The electrical conductivity of samples were decreased with milling time, whereas Seebeck coefficient increased over the temperature range of RT~450°C. The highest power factor was 1.12×10-3 W/mK2 obtained for the sample with 90 min milling at 450°C.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1231-1234
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication Of Zn4Sb3 Alloys By A Combination Of Gas-Atomization And Spark Plasma Sintering Processes
    Wytwarzanie i konsolidacja proszków stopowych zn4sb3 przez kombinację procesów atomizacji gazowej i spiekania
    Autorzy:
    Dharmaiah, P.
    Kim, H.-S.
    Lee, L. H.
    Hong, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/355894.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    gas atomization
    microstructure
    spark plasma sintering (SPS)
    X-ray diffraction
    atomizacja gazowa
    mikrostruktura
    SPS
    spiekanie plazmowe
    analiza rentgenowska (XRD)
    Opis:
    In this study, single phase polycrystalline Zn4Sb3 as well as 11 at.% Zn-rich Zn4Sb3 alloy having ε-Zn4Sb3 (majority phase) and Zn (minority phase) phases bulk samples produced by gas-atomization and subsequently consolidated by spark plasma sintering (SPS) process. The crystal structures were analyzed by X-ray diffraction (XRD) and cross-sectional microstructure were observed by the scanning electron microscopy (SEM). The internal grain microstructure of 11at.% Zn-rich Zn4Sb3 powders shows lamellar structure. Relative density, Vickers hardness and crack lengths were measured to investigate the effect of sintering temperature of Zn4Sb3 samples which are sintered at 653, 673 and 693 K. Relative density of the single phase bulk Zn4Sb3 sample reached to 99.2% of its theoretical density. The micro Vickers hardness of three different sintering temperatures were found around 2.17 – 2.236 GPa.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1417-1421
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Formation of Tungsten/Ammonium Perchlorate Composites and Their Reaction Kinetics
    Autorzy:
    Shim, H.-M.
    Lee, E.-A.
    Kim, J.-K.
    Kim, H.-S.
    Koo, K.-K.
    Powiązania:
    https://bibliotekanauki.pl/articles/358373.pdf
    Data publikacji:
    2015
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    ammonium perchlorate
    composite
    thermal decomposition
    Opis:
    The reaction kinetics of tungsten nanoparticles/ammonium perchlorate (W/AP) composites, produced by a spray drying technique, were analyzed and compared with those of neat AP particles and aluminum nanoparticles/AP (Al/AP) composites. The W was found to raise the onset temperature of the thermal decomposition of AP by increasing the activation energy, whereas Al conversely lowered the onset temperature of AP due to the decreased activation energy. From the master plots of kinetic models with the experimental data, the Prout-Tompkins model and the 1-D diffusion controlled model were found to describe the low-temperature decomposition (LTD) and high-temperature decomposition (HTD), respectively, giving remarkable agreement with experimental curves for all heating rates. The presence of W was found to increase the HTD zone width compared with that of neat AP particles and Al/AP composites. Analysis of the average activation energy and pre-exponential factor showed that W increases the energy barrier and the frequency of occurrence of the reaction compared with that of neat AP particles at the LTD state, whereas W decreases both of them at the HTD state. The effect of Al was also shown to be similar to that of W, but the magnitudes of the variation in activation energy and the pre-exponential factor were relatively small.
    Źródło:
    Central European Journal of Energetic Materials; 2015, 12, 4; 703-722
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of Cu and Ni Nano-Fluids Synthesized by Pulsed Wire Evaporation Method
    Autorzy:
    Kim, H.-S.
    Yilmaz, F.
    Dharmaiah, P.
    Lee, D.-J
    Lee, T.-H.
    Hong, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/356475.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    pulsed wire evaporation
    nanofluid
    Cu
    Ni
    suspension stability
    dispersibility
    Opis:
    In the present work, Cu and Ni nanofluids were synthesized using the pulsed wire evaporation (PWE) method in the different aqueous medias, namely (ethanol and ethylene glycol), and the effects of the aqueous media on the dispersion state, stability, and particle size of nanoparticles were studied. The size and morphology of synthesized nano-particles were investigated by transmission electron microscopy (TEM). Also, the dispersion stability of the nanofluids was evaluated by turbiscan analysis. The TEM results showed that the nano-particles were spherical in shape, and the average particle size was below 100 nm. The average particle size of the Cu nano-particles was smaller than that of Ni, which was attributed to a difference in the specific sublimation energy of the elements. Moreover, ethylene glycol (EG) exhibited higher suspension stability than ethanol. Finally, the dispersion stability of Cu@EG displayed the highest value due to lower particle size and greater viscosity.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 999-1004
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of Different Mechanical Milling Processes On Morphology And Microstructural Changes Of Nano And Micron Al-Powders
    Wpływ różnych procesów mielenia na morfologię i mikrostrukturę nanometrycznych i mikronowych proszków Al
    Autorzy:
    Kim, H.-S.
    Madavali, B.
    Eom, T.-J.
    Kim, C.- M.
    Koo, J.-M.
    Lee, T. H.
    Hong, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/355715.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al alloys
    high-energy ball milling
    low energy ball milling
    plastic deformation
    stopy Al
    wysokoenergetyczne mielenie kulkowe
    mielenie energooszczędne
    odkształcenia plastyczne
    Opis:
    In this research, effect of the various mechanical milling process on morphology and microstructural changes of nano and micron Al-powders was studied. The milling of Al-powders was performed by both high energy and low energy ball milling process. The influence of milling (pulverizing) energy on the structural changes of Al-powders was studied. Al-nanoparticles were agglomerated during the MA and its size was increased with increasing milling while micron Al-powder gets flattened shape during high energy ball milling due to severe plastic deformation. Meanwhile, structural evolution during high energy ball milling of the nano powder occurred faster than that of the micron powder. A slight shift in the position of X-ray diffraction peaks was observed in nano Al-powders but it was un-altered in macro Al-powders. The variation in lattice parameters was observed only for nano Al powders during the high energy ball milling due to lattice distortion.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1235-1239
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Acid Dissolution Conditions on Recovery of Valuable Metals from Used Plasma Display Panel Scrap
    Autorzy:
    Kim, C.- M.
    Dharmaiah, P.
    Kim, H.-S.
    Koo, J.-M.
    Yoon, J.-S.
    Hong, S.-H.
    Hong, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/355713.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    high energy ball milling
    waste plasma display panels
    dissolution
    recovery
    Opis:
    The objective of this particular study was to recover valuable metals from waste plasma display panels using high energy ball milling with subsequent acid dissolution. Dissolution of milled (PDP) powder was studied in HCl, HNO3, and H2SO4 acidic solutions. The effects of dissolution acid, temperature, time, and PDP scrap powder to acid ratio on the leaching process were investigated and the most favorable conditions were found: (1) valuable metals (In, Ag, Mg) were recovered from PDP powder in a mixture of concentrated hydrochloric acid (HCl:H2O = 50:50); (2) the optimal dissolution temperature and time for the valuable metals were found to be 60°C and 30 min, respectively; (3) the ideal PDP scrap powder to acid solution ratio was found to be 1:10. The proposed method was applied to the recovery of magnesium, silver, and indium with satisfactory results.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1173-1177
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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