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Wyświetlanie 1-3 z 3
Tytuł:
Synthesis of hydroxyapatite in the presence of anionic surfactant
Autorzy:
Kolodziejczak-Radzimska, A.
Samuel, M.
Paukszta, D.
Piasecki, A.
Jesionowski, T.
Powiązania:
https://bibliotekanauki.pl/articles/110560.pdf
Data publikacji:
2014
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
hydroxyapatite
precipitation
anionic surfactant
Opis:
Hydroxyapatite was synthesized by precipitation method using an anionic surfactant (SDS) template, at ambient temperature and normal pressure. Phosphoric acid and disodium phosphate were used as a precursor of phosphorous, whereas calcium hydroxide and chloride were used as a precursor of calcium. The obtained hydroxyapatite was subjected to a wide range of physicochemical analysis using various measurement techniques. In order to get information about the properties of the obtained products, the following analysis of characteristics was performed: dispersion (NIBS), morphological (SEM), adsorptive (BET) and structural (XRD). Energy-dispersive X-ray spectroscopy and elemental analysis were also applied.
Źródło:
Physicochemical Problems of Mineral Processing; 2014, 50, 1; 225-236
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and characterization of hydroxyapatite/chitosan composites
Autorzy:
Szatkowski, T.
Kołodziejczak-Radzimska, A.
Zdarta, J.
Szwarc-Rzepka, K.
Paukszta, D.
Wysokowski, M.
Ehrlich, H.
Jesionowski, T.
Powiązania:
https://bibliotekanauki.pl/articles/109806.pdf
Data publikacji:
2015
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
hydroxyapatite
chitosan
composite
one-step co-precipitation
Opis:
Hydroxyapatite (HAp)/chitosan (CS) composites were synthesized via a one-step co-precipitation method from aqueous solution, with the use of calcium chloride (CaCl2) and disodium hydrogen phosphate (Na2HPO4). CS was obtained via partial deacetylation of chitin with the use of strong sodium hydroxide solution. Composites were prepared with various HAp/CS ratios (30/70, 50/50, 70/30, 85/15) for comprehensive comparison of their properties. Fourier Transform Infrared Spectroscopy (FT-IR) analysis showed that hydrogen bonds were formed between the organic matrix and the mineral compound, confirming a successful phase interconnection. X-ray diffraction patterns were obtained, enabling examination of the crystalline properties of the composites, including HAp identification. The porous structure parameters of the composites were investigated, and morphological analysis (SEM) was performed. Differential Thermal Gravimetry (DTG) analysis of the composites indicated that the material is thermally stable up to 200 oC. Additionally, Energy Dispersive Spectroscopy (EDS) analysis of the mineral was carried out to check the Ca/P ratio, and confirmed its similarity to pure HAp.
Źródło:
Physicochemical Problems of Mineral Processing; 2015, 51, 2; 575-585
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hydroxyapatite as a support in protease immobilization process
Autorzy:
Zdarta, J.
Budzinska, K.
Kolodziejczak-Radzimska, A.
Klapiszewski, Ł.
Siwinska-Stefanska, K.
Bartczak, P.
Piasecki, A.
Maciejewski, H.
Jesionowski, T.
Powiązania:
https://bibliotekanauki.pl/articles/110452.pdf
Data publikacji:
2015
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
hydroxyapatite
enzyme immobilization
protease
physicochemical characteristic
Opis:
Hydroxyapatite is used as a matrix for immobilization of protease from Aspergillus oryzae by a process of adsorption. The matrix obtained has the surface area of 26 m2/g and particles in the shape of flakes of diameters no greater than 650 nm. The efficiency of the proposed method was confirmed by the Fourier transform infrared spectroscopy, elemental analysis and by analysis of parameters of the pore structure of matrix and products after immobilization. On the basis of the Bradford method it was found that the greatest amount of enzyme (132 mg/g) was immobilized from a solution of initial enzyme concentration of 7 mg/cm3 after 24 h of the process.
Źródło:
Physicochemical Problems of Mineral Processing; 2015, 51, 2; 633-646
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-3 z 3

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