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Wyświetlanie 1-15 z 18
Tytuł:
Separation of HCl from the mixture of KCl and HCl using membrane distillation
Autorzy:
Tomaszewska, M.
Mientka, A.
Powiązania:
https://bibliotekanauki.pl/articles/779695.pdf
Data publikacji:
2008
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
wydzielanie HCl
destylacja membranowa
HCl separation
membrane distillation
Opis:
Membrane distillation (MD) was applied for the concentration of solutions containing hydrochloric acid and potassium chloride. The studies of the concentration and separation of HCl through the hydrophobic membrane were performed. In the investigations plate and frame or capillary modules, equipped with membranes from polytetrafluoroethylene and polypropylene were applied, respectively. The feed temperature amounted to 333 K or 343 K and permeate 293 K at the inlet of the module. Under the MD operation conditions the transfer of water vapour and hydrogen chloride from potassium chloride and hydrochloric acid solutions through the hydrophobic membranes took place, whereas the potassium chloride as a nonvolatile component underwent concentration in the feed. The influence of acid concentration and salt presence in the feed on the HCl molar flux through the membrane was systematically studied. The increase of the temperature and salt concentration in the feed caused higher partial pressure volatile of HCl and the resultant HCl Flux through a membrane was higher. During MD for the initial concentration in the feed equal 50 g KCl/dm3 and 40g HCl/dm3, at the feed temperature 343K, the permeate flux decreased from 353 dm3/m2d to 289 dm3/m2d, whereas the HCl flux increased to 6 mol/m2d for the capillary module. At higher KCl concentration in the feed, amounting to 100g KCl/dm3 and under the same operation conditions, the permeate flux decreased to 285 dm3/m2d, but the molar flux HCl increased to 18 mol/m2d. The results were compared with the data obtained for the plate and frame module.
Źródło:
Polish Journal of Chemical Technology; 2008, 10, 2; 27-32
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of foam separation in production of β-glucanase in Pichia
Autorzy:
Yuhang, Qin
Yuqing, Chen
Yajuan, Peng
Wenyao, Shao
Powiązania:
https://bibliotekanauki.pl/articles/2174820.pdf
Data publikacji:
2022
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
Foam separation
β-glucanase
recovery rate
enrichment ratio
Opis:
β-glucanase is widely used in many fields and has great economic value and development space, but it faces the difficulties of separation and nutrient destruction in the process of industrial production. Foam separation is a simple, mild and efficient adsorption separation technique that enables efficient separation and extraction of β-glucanase. In this study, five single factors(loading volume, pH, separation gas velocity, fermentation loading concentration, surfactant concentration) of foam separation and harvest of β-glucanase produced by Pichia pastoris were studied. The best univariate condition was: 600 mL/min separation gas velocity, loading volume of 200 mL, initial enzyme concentration of 100 g/mL, surfactant concentration of 0.3 mg/mL and pH of 5. Based on the best univariate condition, the optimal separation conditions of β-glucanase were further explored, and the five-factor four-level orthogonal test was designed. From the experimental results, the best separation condition was: 600 mL/min, loading volume of 200 mL, initial enzyme concentration of 100 μg/mL, surfactant concentration of 0.5 mg/mL and pH of 5. Under this separation condition, the enrichment ratio (E) was 0.56 and the recovery rate (R) was 96.01%.
Źródło:
Polish Journal of Chemical Technology; 2022, 24, 3; 1--7
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The separation of microscale HA in aqueous solution by foam separation technique
Autorzy:
Wenyao, Shao
Xiao, Gong
Shuming, Cui
Ying, Lin
Yinghua, Lu
Yuqing, Chen
Powiązania:
https://bibliotekanauki.pl/articles/949357.pdf
Data publikacji:
2019
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
Foam Separation
Hyaluronic Acid
Enrichment Ratio
Recovery Rate
Opis:
Hyaluronic acid (HA) has important applications in fields of health care products, cosmetics and clinical medical. However, the unique physiological properties of HA make cost of its traditional separation and extraction process relatively high. Foam separation technique has simple, gentle and efficient advantages on the separation of substances with surface activity by using bubbles as the separation medium. In this paper, natural surfactant CocamideBetaine (CAPB) was used as a foaming agent to explore the technology of microscale HA in aqueous solution by foam separation. The optimum process conditions were determined based on the recovery rate and enrichment ratio of HA by single factor and orthogonal experiment: at room temperature, pH = 7, separating air velocity (v) = 350 mL/min, HA concentration (CHA) = 50 mg/L, adding liquid volume (V) = 200 mL, collecting time (tcol) = 10 min, CAPB concentration (CCAPB) = 0.035 g/L. Under these conditions, HA enrichment ratio (E) equals 6.821 and HA recovery rate (R) equals 66.425%.
Źródło:
Polish Journal of Chemical Technology; 2019, 21, 4; 66-71
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Two-step treatment of harmful industrial wastewater: an analysis of microbial reactor with integrated membrane retention for benzene and toluene removal
Autorzy:
Trusek-Holownia, A.
Noworyta, A.
Powiązania:
https://bibliotekanauki.pl/articles/778406.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
bioremoval
benzene
toluene
MBR
mathematical model
membrane separation
Opis:
Standards for highly toxic and carcinogenic pollutants impose strict guidelines, requiring values close to zero, regarding the degradation of such pollutants in industrial streams. In many cases, classic bioremoval processes fail. Therefore, we proposed a stream leaving the microbial membrane bioreactor (MBR) that is directed to an additional membrane separation mode (NF/RO). Under certain conditions, the integrated process not only benefits the environment but may also increase the profitability of the bioreactor operation. An appropriate model was developed and tested in which the bioremoval of benzene and toluene by Pseudomonas fluorescens was used as an example. This paper presents equations for selecting the operation parameters of the integrated system to achieve the expected degree of industrial wastewater purification.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 4; 15-22
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Batch electrodialysis of lactic acid obtained from LAB fermentation
Autorzy:
Lech, M.
Trusek, A.
Powiązania:
https://bibliotekanauki.pl/articles/778573.pdf
Data publikacji:
2018
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
lactic acid
membrane separation
Lactobacillus rhamnosus
whey
lactose
Opis:
The aim of this work was to develop the method of lactic acid (LA) separation from fermented whey. CMI-7000 Cation Exchange Membrane and AMI-7001 Anion Exchange Membrane were employed in electrodialysis process. Experiments showed that the selected membranes separated organic acids effectively (including LA) from other organic ingredients present in medium. Selecting an appropriate volume of a receiving chamber could lead to LA concentration. Moreover, membrane fouling during separation was investigated. This phenomenon is negligible which is the main advantage of this process. As it was shown during batch processes, with the voltage increase, the rate of electrodialysis increases as well. It prompts to a reduction of residence time in electrodialyzer during a continuous separation.
Źródło:
Polish Journal of Chemical Technology; 2018, 20, 3; 81-86
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Non-alcoholic beer production – an overview
Autorzy:
Jackowski, M.
Trusek, A.
Powiązania:
https://bibliotekanauki.pl/articles/779911.pdf
Data publikacji:
2018
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
non-alcoholic beer
fermentation
membrane separation
dealcoholisation
evaporation
Opis:
Through years beer became one of the best known alcoholic beverages in the world. For some reason e.g. healthy lifestyle, medical reasons, driver’s duties, etc. there is a need for soft drink with similar organoleptic properties as standard beer. There are two major approaches to obtain such product. First is to interfere with biological aspects of beer production technology like changes in mashing regime or to perform fermentation in conditions that promote lower alcohol production or using special (often genetic modified) microorganism. Second approach is to remove alcohol from standard beer. It is mainly possible due to evaporation techniques and membrane ones. All these approaches are presented in the paper.
Źródło:
Polish Journal of Chemical Technology; 2018, 20, 4; 32-38
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A novel approach for calculating packed column height based on new correlation of mass transfer coefficient
Autorzy:
Rahbar-Kelishami, A.
Bahmanyar, H.
Hajamini, Z.
Powiązania:
https://bibliotekanauki.pl/articles/778168.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
separation
liquid-liquid extraction
packed column
mass transfer
column design
diffusion
Opis:
The calculation of column’s height plays an important role in packed columns precise design. This research is based on experimentally measurement of mass transfer coefficients in different heights of packed column to predict its height. The objective of presented work is to introduce a novel conceptual method to predict column height via new correlation for mass transfer coefficient. As the mass transfer coefficient is decreased with increase of column height, the HTU’s are not constant figures along the column so this new approach is called increasing HTU’s. The results of the proposed idea were compared with other correlations and the conventional method i.e. constant HTU’s. Since the results are in very good agreement with experimental data comparing to conventional method, it seems this approach can be a turning point in design of all differential columns like packed columns. Making use of this method is suggested for design of differential columns.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 1; 48-54
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The effect of hydrotropes on the solubility and mass transfer coefficient of 2-nitrobenzoic acid
Autorzy:
Thenesh-Kumar, S.
Gnana-Prakash, D.
Nagendra-Gandhi, N.
Powiązania:
https://bibliotekanauki.pl/articles/779314.pdf
Data publikacji:
2009
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
hydrotrop
solubilizacja
współczynnik wymiany masy
separacja
hydrotropy
solubilization
mass transfer coefficient
separation
Opis:
A comprehensive investigation on the solubility and mass transfer coefficient enhancement of 2-nitrobenzoic acid through hydrotropy, has been undertaken. The solubility and mass transfer coefficient studies were carried out using hydrotropes such as sodium acetate, citric acid and nicotinamide under a wide range of hydrotrope concentrations (0 to 3.0 mol/L) and different system temperatures (303 to 333 K). It was found that the solubility and mass transfer coefficient of 2-nitrobenzoic acid increases with an increase in hydrotrope concentration and also with system temperature. All hydrotropes used in this work showed an enhancement in the solubility and mass transfer coefficient to different degrees. The maximum enhancement factor value has been determined for both the solubility and mass transfer coefficient. The effectiveness of hydrotropes was measured in terms of Setschnew constant Ks and reported for all the hydrotropes used in this study.
Źródło:
Polish Journal of Chemical Technology; 2009, 11, 2; 55-59
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of mares colostrum and milk sample for 2-DE separation without acetone precipitation
Przygotowanie próbek siary i mleka klaczy do rozdziału 2-DE, z pominięciem precypitacji acetonem
Autorzy:
Cichy, A.
Dratwa-Chałupnik, A.
Medeńska, W.
Ożgo, M.
Pikuła, R.
Powiązania:
https://bibliotekanauki.pl/articles/2621587.pdf
Data publikacji:
2020
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
electrophoretic separation
colostrum
mare milk
proteomic analysis
precipitation
acetone
2-D electrophoresis
Źródło:
Acta Scientiarum Polonorum. Zootechnica; 2020, 19, 3; 71-77
1644-0714
Pojawia się w:
Acta Scientiarum Polonorum. Zootechnica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization and components separation of corn stover by alkali and hydrogen peroxide treatments
Autorzy:
Cong, L.
Li, Z.
Guanqun, Z.
Jianguo, X.
Long, .
Powiązania:
https://bibliotekanauki.pl/articles/778467.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
Corn stover
lignin
hemicellulose
cellulose
Component separation
NaOH-H2O2
Opis:
The dissolution of corn stover in alkaline solvent system composed of NaOH-H2O2 was reported and the separation of its ingredients combined with acid precipitation, ethanol extraction was proposed. It is proven that the residual after alkali solvent was cellulose, the filtrate by the acid precipitation of the liquor was lignin, the solid by the ethanol extraction of the liquor was hemicellulose. The optimum dissolution conditions were determined by single-factor experiment as follows: the concentration of H2O2 5.0%, pH 11.5, dissolution temperature 60°C, dissolution time 3.0 h, the ratio of liquid to solid 30 mL/g. And chemical analysis were employed to determine the purity of the components separated. The structure of the components separated were identifi ed by FT-IR, SEM, XRD and NMR. The cellulose recovery yield can achieve to 84.2% and lignin recovery yield is 86.6%, the hemicellulose recovery yield is 96.7%. After recycling the solvent 3 times, the recovery yield of cellulose, lignin and hemicellulose were 82.7, 87.6 and 97.4%, and the purity of cellulose, lignin and hemicellulose were 98.0, 96.5 and 98.7%, respectively.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 2; 89-95
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Air Separation Units (ASUs) Simulation Using Aspen Hysys® at Oxinor I of Air Liquid Chile S.A Plant
Autorzy:
Leiva, C.A
Poblete, D.A.
Aguilera, T.L.
Acuña, C.A.
Quintero, F.J.
Powiązania:
https://bibliotekanauki.pl/articles/778527.pdf
Data publikacji:
2020
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
Simulation
Oxygen plant
Aspen Hysys
Air separation units (ASUs)
Air Liquide S.A.
Opis:
The method used to extract copper from its ores depends on the nature of the ore. The main process currently to separate copper from sulphide ores is the smelting process. The concentrated ore is heated strongly with silicon dioxide (silica), calcium carbonate and oxygen enriched air in a furnace or series of furnaces which is carried out using the injection of the air for oxidation the Fe and Si present in the raw material. Oxygen can be produced using several different methods. One of these methods is Air separation process, which separates atmospheric air into its primary components, typically nitrogen and oxygen, and sometimes also argon and other rare inert gases by cryogenic distillation. In this paper, simulation of air separation units (ASUs) was studied using Aspen Hysys®. The obtained simulation and model was validated with the operational data from the Oxinor I of Air Liquide S.A Plant. The ASU was divided into subsystems to perform the simulations. Each subsystem was validated separately and later on integrated into a single simulation. An absolute error of 1% and 1.5% was achieved between the simulated and observed the process variables(s). This indicated that Aspen Hysys®  has the thermodynamic packages and required tools to perform simulations in cryogenic processes at industrial scale.
Źródło:
Polish Journal of Chemical Technology; 2020, 22, 1; 10-17
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Reverse osmosis as one-step wastewater treatment: a case study on groundwater pollution
Autorzy:
Ali, W.
Rehman, W. U.
Younas, M.
Ahmad, M. I.
Gul, S.
Powiązania:
https://bibliotekanauki.pl/articles/779416.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
reverse osmosis (RO)
membrane separation
Total Dissolved Solids (TDS)
Total Coliform
E. Coli
Opis:
The present case study is focused on performance evaluation of a Reverse Osmosis (RO) membrane based pilot plant to treat the ground/surface drinking water sources polluted by flood, rivers and/or canals. The RO plant was designed, fabricated and then operated with polluted water. Two feed water samples having a TDS of 2.000 mg · L−1 and 10.000 mg · L−1 respectively, were taken and analyzed for physical, chemical and microbiological contaminants. The RO plant was run once through over a span of 100 hrs at an operating pressure of 15 bar. TDS rejections were found to be more than 94% while permeate flux was measured to be 25.82 L · m−2 · hr−1 to 40.55 L · m−2 · hr−1. Results show that RO plant has a potential to remove physical, chemical and microbiological contaminants like Total Coliform and E. Coli in one step.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 4; 42-48
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Separation of matrine and oxymatrine from Sophora flavescens extract through cation exchange resin coupled with macroporous absorption resin
Autorzy:
Chen, H.
Luo, S.
Zheng, X.
Fan, H.
Powiązania:
https://bibliotekanauki.pl/articles/778382.pdf
Data publikacji:
2016
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
Sophora flavescens
BS-65 macroporous resin
001×732 cation exchange resin
separation
alkaloids
Opis:
A simple method for separation of matrine and oxymatrine from Sophora flavescens was developed with cation exchange resin coupled with macroporous resin. Based on the adsorption characteristics of matrine and oxymatrine, 001×732 cation exchange resin was used to absorb target alkaloids for removing most of the foreign matter, while BS-65 macroporous resin was chosen to purify these alkaloids. The result showed that the equilibrium adsorption data of matrine and oxymatrine on 001×732 resin and BS-65 resin at 30°C was fitted to Langmuir isotherm and Freundlich isotherm, respectively. The contents of matrine and oxymatrine were increased from 0.73% and 2.2% in the crude extract of the root of Sophora flavescens to 67.2% and 66.8% in the final eluent products with the recoveries of 90.3% and 86.9%, respectively.
Źródło:
Polish Journal of Chemical Technology; 2016, 18, 2; 31-39
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, characterization and analytical applications of chelating resin containing orcinol
Autorzy:
Shah, B. A.
Shah, A. V.
Patel, N. B
Shah, M.
Powiązania:
https://bibliotekanauki.pl/articles/779773.pdf
Data publikacji:
2012
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
separacja analityczna
żywice chelatujące
kopolimery
wymiana
analytical separation
chelating resin
column operation
copolymer
exchange capacity
Opis:
A chelating resin based on Salicylic acid-Formaldehyde copolymer, containing Orcinol (SFO), has been synthesized and characterized on the basis of Elemental Analysis, Particle Size Distribution, FT-IR Analysis, XRD, SEM and Optical Photographs. The Physico-Chemical properties have been studied. This resin is highly stable in acidic and alkaline solutions and has been studied as a chelating sorbent for heavy metal ions and transition metal ions. The Exchange capacity order is Ni(II) > Cu(II) > Zn(II) > Cd(II) > Pb(II). The effect of nature and concentration of different electrolytes on distribution coefficient (Kd) for metal ions have been investigated. Separation of synthetic mixtures containing Cu(II)-Pb(II), Ni(II)-Cd(II) and Brass constituents has been carried out using a column prepared from the synthesized chelating resin. The developed procedure was also tested for the removal of Cd(II) and Pb(II) from natural water of Purna River near by Navsari, Gujarat, India. Keywords
Źródło:
Polish Journal of Chemical Technology; 2012, 14, 2; 88-96
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Pressure swing absorption of carbon dioxide in n-methyl-2-pyrrolidone solutions
Autorzy:
Kierzkowska-Pawlak, H.
Powiązania:
https://bibliotekanauki.pl/articles/779872.pdf
Data publikacji:
2007
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
oddzielanie CO2
separacja CO2
desorpcja pęcherzy gazowych
przesycenie
CO2 separation
bubbling desorption
supersaturation ratio
Opis:
The mass transfer rates during CO2 absorption and desorption from N-methyl-2-pyrrolidone solutions were measured at 293.15 K in a baffled agitated reactor with a flat gas-liquid interface. Based on the measured values of pressure changes, the desorption rate was determined and compared to the absorption rate at the same driving force. Two distinct mechanisms of desorption were observed. The transition from bubbling to the diffusive desorption is found to be a function of the supersaturation ratio, pressure and the stirring speed.
Źródło:
Polish Journal of Chemical Technology; 2007, 9, 2; 106-109
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 18

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