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Wyszukujesz frazę "mechanical milling" wg kryterium: Temat


Wyświetlanie 1-2 z 2
Tytuł:
Preparation and Characterization of Ultrafine HMX/TATB Explosive Co-crystals
Autorzy:
An, C.
Li, H.
Zhang, Y.
Ye, B.
Xu, C.
Wang, J.
Powiązania:
https://bibliotekanauki.pl/articles/358105.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
HMX
TATB
ultrafine co-crystals
ball milling
mechanical sensitivity
Opis:
An explosive co-crystal of 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane (HMX) and 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) was prepared by the ball milling method. The raw materials and co-crystals were characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and Raman spectroscopy. Impact and friction sensitivity of the co-crystals were tested and analyzed. The results showed that the HMX/TATB co-crystals are spherical in shape and 100-300 nm in size. The co-crystals are different from anintimate mixture of HMX/TATB and they exhibit a new co-crystal structure. HMX/TATB co-crystals are formed by N-O···H hydrogen bonding between −NO2 (HMX) and −NH2 (TATB). The drop height of ultrafine HMX/TATB explosive co-crystals is 12.7 cm higher than that of ultrafine HMX, whilst the explosion probability of friction is 20% lower than that of ultrafine HMX. Ultrafine HMX/TATB explosive co-crystals are difficult to initiate under impact and friction conditions.
Źródło:
Central European Journal of Energetic Materials; 2017, 14, 4; 876-887
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Green Fabrication of Nanoscale Energetic Molecular Perovskite (H2dabco)[Na(ClO4)3] with Reduced Mechanical Sensitivity
Autorzy:
Hu, Li-shuang
Du, Zelin
Liu, Yang
Gong, Shida
Guang, Chunyu
Li, Xin
Yang, Zhi
Jia, Qi
Liang, Kaili
Powiązania:
https://bibliotekanauki.pl/articles/27787996.pdf
Data publikacji:
2021
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
molecular perovskite
(H2dabco)[Na(ClO4)3]
ball milling
thermal decomposition
mechanical sensitivity
Opis:
High-energy-density molecular perovskite energetic materials with high detonation performance have attracted much attention, but poor safety performance has limited their potential applications. In this paper, nano sodium perchlorate-based molecular perovskite (H2dabco)[Na(ClO4)3] (nano DAP-1) was fabricated by green ball-milling technology. The structure and morphology of the samples were characterized and the results showed that nano DAP-1 with nearly spherical morphology has a narrow particle size distribution, < 1 μm. The thermal decomposition properties were investigated by differential scanning calorimetry (DSC). The exothermic peak of nano DAP-1 thermal decomposition was 330.0 °C, a decrease of 51.7 °C compared with that of raw DAP (381.7 °C). The apparent activation energy (Ea) of nano DAP-1 was calculated to be 160.9 kJ·mol–1, which is lower than that of raw DAP-1 (168.6 kJ·mol–1). Mechanical sensitivity studies showed that nano DAP-1 (H50: 64 cm) exhibited a lower impact sensitivity than that of the raw DAP-1 (H50: 51 cm). This work provides a simple and effective way for improving the thermal decomposition properties and safety performance of molecular perovskite energetic materials.
Źródło:
Central European Journal of Energetic Materials; 2021, 18, 3; 369--384
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-2 z 2

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