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    Wyświetlanie 1-11 z 11
    Tytuł:
    Process Optimization and Characterization of an HMX/Viton Nanocomposite
    Autorzy:
    Shi, X.
    Wang, C.
    Wang, J.
    Li, X.
    An, C.
    Ji, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/358667.pdf
    Data publikacji:
    2015
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    HMX
    spray drying
    processing parameters
    optimization
    impact sensitivity
    nanoparticles
    Opis:
    HMX/Viton A nanocomposites were prepared by a spray drying process using different processing parameters, which included the dry gas inlet temperature, the air flow rate, and the solution feed flow rate. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used to characterize the nanocomposites. The effects of the processing parameters on the morphology of the samples were investigated and are discussed. The thermal decomposition behaviour and impact sensitivity of the raw HMX and HMX/Viton A nanocomposites were also measured and compared. Optimal morphology and dispersion of the coated samples was achieved when the dry gas inlet temperature and the air and solution feed flow rates were 55 °C, 660 L/h and 1.5 mL/min, respectively. Under these optimal processing conditions, the nanocomposites were spherical in shape, ranged from 0.2-2 μm in size, and were composed of many tiny particles of 50-100 nm in size. The crystal phase of the nanocomposites was the same as that of raw HMX. Compared with those of raw HMX, the melting point and impact sensitivity of the nanocomposites were lower and the thermal decomposition rate was slightly higher.
    Źródło:
    Central European Journal of Energetic Materials; 2015, 12, 3; 487-495
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Detonation Reaction Characteristics for CL-20 and CL-20-based Aluminized Mixed Explosives
    Autorzy:
    Liu, D.
    Chen, L.
    Wang, C.
    Wu, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358308.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    detonation reaction zone
    aluminum reaction
    interfacial particle velocity
    interferometry
    Opis:
    The interfacial particle velocities for CL-20 and CL-20-based aluminized mixed explosives were measured by interferometry in order to analyze the aluminum reactions in the latter. The reaction characteristics were obtained, as well as a better understanding of the effects of aluminum powder on the detonation reaction zone length. Two functions were used to fit the particle velocity-time profiles, and their intersection was the corresponding Chapman-Jouget (CJ) point. From these profiles, the detonation reaction zone length and the aluminum reaction were then analyzed. CL-20-based explosives have a short reaction time (48 ns for a high CL-20 content), while the reaction time of CL-20/Al explosives increased with the aluminum content and particle size. Micron-scale aluminum particles barely reacted in the CL-20 detonation reaction zone, but instead reacted with the detonation products after the CJ point. This reduced the detonation pressure; however, the aluminum reaction can slow down the decrease in particle velocities. The start times of small-particle aluminum reactions were earlier than those of the larger particles. The 2-3-μm aluminum particles start to react within 1 μs after the CJ point, while the 200-nm particles may start to react in the reaction zone.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 3; 573-588
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    GAP/DNTF Based PBX Explosives: a Novel Formula Used in Small Sized Explosive Circuits
    Autorzy:
    An, C.
    Wen, X.
    Wang, J.
    Wu, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/358581.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    explosive circuits
    GAP/DNTF based PBX explosives
    thermal stability
    mechanical sensitivity
    propagation reliability
    detonation velocity
    Opis:
    With 3,4-dinitrofurazanofuroxan (DNTF) and glycidyl azide polymer (GAP) as the main explosive and binder respectively, GAP/DNTF based PBX explosives were designed, prepared and used to fill the small groove of some explosive circuits. The formulation was: DNTF 85 wt.%, GAP 11 wt.%, 2,4-toluene diisocyanate (TDI) and other additives making up the final 4 wt.%. After the uncured slurry mixture was prepared by uniform mixing, a squeezing device was used to charge the circuit groove (dimensions less than 1 mm × 1 mm). Scanning electron microscope (SEM) results showed a fine charging effect. Differential Scanning Calorimetry (DSC) was used to determine the energy of activation (Ea) and the pre-factor (A) of GAP/DNTF and these were compared with those for raw DNTF. The influences and causes of it have been investigated. The experimental results for propagation reliability showed that when the dimensions of the linear groove were 0.8 mm × 0.8 mm, 0.7 mm × 0.7 mm, 0.6 mm × 0.6 mm or 0.5 mm × 0.5 mm, GAP/DNTF based PBX explosives can propagate explosion successfully. Furthermore, the H50 and friction sensitivity of GAP/DNTF based PBX explosives were obtained using the following mechanical sensitivity experiments. These properties are vital if GAP/DNTF based PBX explosives are to be applied in complex explosive circuits.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 2; 397-410
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study on the rheological properties of CL-20/HTPB casting explosives
    Autorzy:
    Li, H.-X..
    Wang, J-Y.
    An, C.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/358310.pdf
    Data publikacji:
    2014
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    casting explosive
    particle gradation
    rheological properties
    plasticizer
    Opis:
    The rheological properties of ε-2,4,6,8,10,12-hexanitro-2,4,6,8,10,12hexaazaisowurtzitane (CL-20)/hydroxy-terminated polybutadiene (HTPB) casting explosives with different formulations were tested and analyzed. The effects of both the weight percentage (wt.%) of CL-20 and its particle size, as well as the type and content of plasticizers, on the rheological properties of CL-20/HTPB casting explosives were investigated in detail. The results show that the viscosity and pseudoplasticity of CL-20/HTPB casting explosives increase with increasing wt.% of CL-20 and decreasing particle size. The gradation of CL-20 particle size also affects the rheological properties of the casting explosives. When the mixing ratio of 30 μm to 2 μm particles is 3:1, the viscosity reaches its lowest value and the non-Newtonian index reaches the maximum value of 0.5698. The viscosity, non-Newtonian index and impact sensitivity of the samples studied are clearly decreased by the addition of dioctyl adipate (DOA), dioctyl sebacate (DOS) or dibutyl phthalate (DBP). However, the three plasticizers do not appear to affect the thermal decomposition of CL-20/HTPB casting explosives. With respect to the rheological properties, mechanical properties and sensitivity, DOA is the optimum plasticizer to use in CL-20/HTPB casting explosives.
    Źródło:
    Central European Journal of Energetic Materials; 2014, 11, 2; 237-255
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation and Characterization of Ultrafine HMX/TATB Explosive Co-crystals
    Autorzy:
    An, C.
    Li, H.
    Zhang, Y.
    Ye, B.
    Xu, C.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358105.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    HMX
    TATB
    ultrafine co-crystals
    ball milling
    mechanical sensitivity
    Opis:
    An explosive co-crystal of 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane (HMX) and 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) was prepared by the ball milling method. The raw materials and co-crystals were characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and Raman spectroscopy. Impact and friction sensitivity of the co-crystals were tested and analyzed. The results showed that the HMX/TATB co-crystals are spherical in shape and 100-300 nm in size. The co-crystals are different from anintimate mixture of HMX/TATB and they exhibit a new co-crystal structure. HMX/TATB co-crystals are formed by N-O···H hydrogen bonding between −NO2 (HMX) and −NH2 (TATB). The drop height of ultrafine HMX/TATB explosive co-crystals is 12.7 cm higher than that of ultrafine HMX, whilst the explosion probability of friction is 20% lower than that of ultrafine HMX. Ultrafine HMX/TATB explosive co-crystals are difficult to initiate under impact and friction conditions.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 4; 876-887
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication and Characterization of PMMA/HMX-based Microcapsules via in situ Polymerization
    Autorzy:
    Jia, X.
    Hou, C.
    Tan, Y.
    Wang, J.
    Ye, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/358134.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    fabrication
    characterization
    HMX
    PMMA
    microcapsules
    Opis:
    Microcapsule technology was applied with nitramine explosives to improve their performance. Polymethyl Methacrylate (PMMA) was selected for the fabrication of 1,3,5,7-tetranitro-1,3,5,7-tetrazocane (HMX) based microcapsules. The PMMA/HMX-based microcapsules were prepared via a facile in situ polymerization of PMMA on the surface of the HMX crystals. Structural characterization of the PMMA/HMX microcapsules was studied systematically by scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier-transform infrared (FT-IR) spectroscopy, and their thermal durability as well as their mechanical sensitivities were measured. The results indicated that spherical microcapsules were formed, with PMMA as the capsule wall and HMX as the core material. The SEM results showed that the grains of the PMMA/HMX microcapsules were spherical and that the particle distribution was homogeneous. XRD and FT-IR analyses indicated that the HMX polymorph was preserved in the optimal β-form during the whole preparative process. The DSC results showed that the PMMA/HMX microcapsules had better thermal decomposition performance, and that the apparent activation energy of the microcapsules had increased by 47.3 kJ/mol compared to the recrystallized HMX, and its thermal stability had greatly improved. In addition, the drop height (H50) had increased from 30.45 cm to 58.49 cm, an increase of 65.81%. Thus, microcapsule technology will have a very wide range of applications in reducing the sensitivity of high energy materials in the future.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 3; 559-572
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    An Insensitive Booster Explosive: DAAF Surface-coated with Viton A
    Autorzy:
    Li, X.
    Wu, B.
    Liu, S.
    An, C.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358841.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    DAAF
    refinement
    surface-coated
    thermal analysis
    impact sensitivity
    Opis:
    3,3’-Diamino-4,4’-azoxyfurazan (DAAF) is the principal component of an insensitive booster explosive; refined DAAF and DAAF surface-coated with Viton A were prepared. Scanning electron microscopy (SEM), X-ray diffraction (XRD), and differential scanning calorimetry (DSC) were employed to characterize the morphology, composition, and thermal decomposition of these samples. The impact sensitivity and theoretical detonation velocity of DAAF-based composites were also measured and analyzed. The results showed that DAAF surface-coated with Viton A was successfully obtained, and the impact sensitivity of DAAF/Viton A composites was much lower than that of crude DAAF. In addition, DAAF/Viton A composites exhibited better thermal stability compared to crude DAAF and refined DAAF. The theoretical detonation velocity of DAAF/Viton A composites and TATB/Viton A composites are roughly the same. Therefore, there is still great potential for DAAF to be used as the main explosive component of a booster explosive.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 3; 445-455
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation of Al Nanoparticles and Their Influence on the Thermal Decomposition of RDX
    Autorzy:
    Hou, C.
    Geng, X.
    An, Ch.
    Wang, J.
    Xu, W.
    Li, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358260.pdf
    Data publikacji:
    2013
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    Al nanoparticles
    properties
    RDX
    thermal decomposition
    Opis:
    Aluminum (Al) nanoparticles were prepared by the DC arc plasma method in order to study the influence of Al nanoparticles on the thermal decomposition of cyclotrimethylenetrinitramine (RDX). The Al powder was characterized by TEM, BET, XRD, and LSA, and the thermal decomposition of RDX and RDX/nanometer Al were examined by DSC. Based on the DSC curves, the thermal decomposition parameters of the samples were calculated and compared. The results showed that the particles of Al are homogeneous and fine, and that the surface is smooth. The TEM results showed that the nanoparticles are spherical, with an average diameter of approximately 60 nm. The peak temperature of RDX decomposition decreased by 4.36 K at the heating rates of 5, 10, and 20 K/min after the addition of nano-Al powder, and the activation energy for decomposition decreased by about 11 kJ/mol. Furthermore, the critical explosion temperature was also reduced. These observable changes indicate that Al nanoparticles act as catalysts for the thermal decomposition of RDX.
    Źródło:
    Central European Journal of Energetic Materials; 2013, 10, 1; 123-133
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis and Characterization of Four Energetic Transition Metal Complexes of 3,4-Diamino-1,2,4-triazole
    Autorzy:
    Yin, X.
    Jin, X.
    Xu, C.-X.
    He, P.
    Wang, K.
    Zhang, J.-G.
    Powiązania:
    https://bibliotekanauki.pl/articles/358716.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    3,4-diamino-1,2,4-triazole
    theoretic study
    crystal structure
    thermal stability
    sensitivity
    Opis:
    Four complexes with the formula of [M5(DATr)12~14(H2O)6](ClO4)10 (M = Mn (1), Co (2), Ni (3), Zn (4)) about their synthesis, structures and some energetic properties (such as sensitivities tests) have been described, where the DATr here denotes 3,4-diamino-1,2,4-triazole. These four compounds are all light metallic complexes with good thermal stability. The structures of 2-4 were determined by single-crystal X-ray diffraction, and the crystal structures mainly consist of penta-nuclear units. All the structures have a common interesting property in which DATr plays a role of bi-dentate ligand. Besides, it is observed from the crystal structure of 4 that DATr can be also act as a mono-dentate ligand. Thermodynamic studies of their decomposition properties and kinetic parameters show that the four complexes have high thermal stabilities. Furthermore, tests of their impact and friction sensitivities show that complexes (2) and (3) can be potential candidates as primary explosives to replace toxic lead azide.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 2; 301-320
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermally induced damage in hexanitrohexaazaisowurtzitane
    Autorzy:
    Tian, Q.
    Yan, G.
    Sun, G.
    Huang, C.
    Xie, L.
    Chen, B.
    Huang, M.
    Li, H.
    Liu, X.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358735.pdf
    Data publikacji:
    2013
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    CL-20
    SAXS
    AFM
    thermal effects
    voids
    Opis:
    The evolution of the microstructure of hexanitrohexaazaisowurtzitane (CL-20) after a thermal stimulus plays a key role in the performance of CL-20. In the current work, microstructural variations of CL-20 caused by thermal treatment were investigated by X-ray diffraction, in situ variable-temperature optical microscopy, atom force microscopy, and small-angle X-ray scattering. A wave-like process, an abrupt volume expansion, movement, and fragmentation of CL-20 particles during phase transition were observed. After the phase transition (160 °C) the CL-20 sample acquired a very rough surface with numerous dimple depressions, and during the thermal decomposition stage (200 °C) a large number of voids were produced in both the bulk and the surface of the CL-20.
    Źródło:
    Central European Journal of Energetic Materials; 2013, 10, 3; 359-369
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Microstructural Evolution in HMX Based Plastic-bonded Explosive During Heating and Cooling Process: an in situ Small-angle Scattering Study
    Autorzy:
    Yan, G.
    Tian, Q.
    Liu, J.
    Fan, Z.
    Sun, G.
    Zhang, C.
    Wang, Y.
    Chen, B.
    Gong, J.
    Zhou, X.
    Yang, Z.
    Nie, F.
    Li, J.
    Li, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358618.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    SANS
    SAXS
    HMX-PBX
    thermal damages
    phase transition
    Opis:
    The thermal damage in octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) based plastic-bonded explosive (PBX) was investigated using in situ small-angle neutron and X-ray scattering techniques. The microstructural evolution was quantitatively characterized by the model fitting parameters of total interfacial surface area (Sv) and void volume distribution. The Sv of HMX-PBX decreased markedly above 100 °C, indicating the movement of binder into the voids. After subsequent cooling to room temperature, the scattering intensity increased significantly with increasing storage time, and a new population of voids with average diameter of 20 nm was observed, accompanied by the gradual phase transition of HMX from δ- to β-phase. The experimental results implied that serious damage within the HMX-PBX was developed during storage after heating.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 916-926
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-11 z 11

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