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    Wyświetlanie 1-14 z 14
    Tytuł:
    Pre-formulation Compatibility Studies of 5-Amino-1H-tetrazole Nitrate with Several Typical Materials by Thermal and Non-thermal Techniques
    Autorzy:
    Guo, W.
    Han, Z.
    Lin, Q.
    Wang, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/358375.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    5-ATN
    compatibility
    energetic materials
    Opis:
    The aim of the present study was to assess the physicochemical compatibility of a promising energetic salt, 5-amino-1H-tetrazole nitrate (5-ATN), with some typical materials. Thermal techniques (differential scanning calorimetry (DSC) and vacuum stability test (VST)) and non-thermal techniques (X-ray diffractometry (XRD) and Fourier Transform Infrared Spectroscopy (FTIR)) were applied. Five energetic materials (TNT, RDX, HMX, CL-20 and AP) and three common additives (Al, DOS and F2604-2) were tested to evaluate their compatibility with 5-ATN. Based on the DSC results, except for AP that was only partially compatible with 5-ATN, all of the selected materials exhibited good compatible with 5-ATN. The VST test further confirmed the compatibility of the 5-ATN/AP mixtures. Combined with the thermal methods, the FTIR results agreed with the DSC findings. The XRD results showed some differences.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 1; 100-114
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Compatibility Study of 2,6-Diamino-3,5-dinitropyridine-1-oxide with Some Energetic Materials
    Autorzy:
    Li, X.
    Wang, B.-L,
    Lin, Q.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/358871.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    compatibility
    energetic materials
    ANPyO
    Opis:
    For the application of 2,6-diamino-3,5-dinitropyridine-1-oxide (ANPyO) in composite explosives, the compatibility of ANPyO with some energetic materials was studied by the use of differential scanning calorimetry (DSC), where the energetic materials were cyclotrimethylenetrinitramine (RDX), cyclotetramethylenetetranitramine (HMX), 3,4-dinitrofurazanfuroxan (DNTF), hexanitrohexazaisowurtzitane (CL-20), 2,4,6-trinitrotoluene (TNT), 2,4,6-triamino-1,3,5-trinitrobenzene (TATB), 3-nitro-1,2,4-triazol-5-one (NTO), 2,6-diamino-3,5-dinitropyrazine-1-oxide (LLM-105), 5-amino-1H-tetrazole nitrate (5-ATEZN), ammonium perchlorate (AP), potassium perchlorate (KP), aluminum powder (Al), boron powder (B), magnesium hydride (MgH2) and magnesium borohydride (Mg(BH4)2). The results showed that the binary systems of ANPyO/CL-20, ANPyO/NTO, ANPyO/5-ATEZN, ANPyO/Al, ANPyO/B, ANPyO/MgH2 and ANPyO/Mg(BH4)2 are compatible, and that the systems of ANPyO with RDX, LLM-105, HMX, AP and KP are sensitive, and with DNTF, TNT and TATB are incompatible.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 978-988
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparative Theoretical Investigation on Energetic Substituted Furazanyl Ethers
    Autorzy:
    Liu, N.
    Wang, K.
    Shu, Y.
    Zeman, S.
    Wang, B.
    Wang, W.
    Powiązania:
    https://bibliotekanauki.pl/articles/358622.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    furazanyl ethers
    heats of formation
    bond dissociation energy
    detonation performance
    melting point
    Opis:
    Furazanyl ether has great potential to be an important candidate as a casting explosive and energetic plasticizer. The density functional theory (DFT) method was used to investigate the heats of formation (HOFs), molecular stability, detonation performance and melting point of a series of substituted furazanyl ethers at B3LYP/6-311G(d,p) level. The results show that the introduction of –N3 or –N(O)=N– groups significantly improves the HOFs values of the derivatives. The bond dissociation energies (BDEs) were analyzed, showing that the N–O bond in the furazan ring is the weakest for most compounds and the ring is vulnerable to cleavage in thermal decomposition. The calculation of density, detonation velocities and detonation pressures suggests that the substitution of –NF2, –CF(NO2)2, furoxan or –N(O)=N– group is an effective method for enhancing their detonation performance. The melting points were determined according to the variation of specific heat capacity, and good estimates were obtained in comparison with the available experimental data. Taking into account the detonation performance and melting point, four compounds are favoured for application in melt cast explosive or energetic plasticizers.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 1; 47-71
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis and Property of 1,4-Diamino-3,6- dinitropyrazolo[4,3-c]pyrazole and Its Derivatives
    Autorzy:
    Li, Y.-N.
    Wang, B.-Z.
    Shu, Y.-J.
    Zhang, S.-Y.
    Lian, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/358674.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    3,6-dinitropyrazolo[4,3-c]pyrazole (DNPP)
    1,4-diamino-3,6- dinitropyrazolo[4,3-c]pyrazole (DADNP)
    4,4’-(triaz-1-ene-1,3-diyl)bis(1- amine-3,6-dinitropyrazolo[4,3-c]pyrazole) (TBADNP)
    N-amination reaction
    synthesis
    property
    Opis:
    A synthetic procedure has been developed for the synthesis of 1,4-diamino- 3,6-dinitropyrazolo[4,3-c]pyrazole (DADNP) via N-amination reaction. Its derivatives, 4,4’-(triaz-1-ene-1,3-diyl)bis(1-amine-3,6-dinitropyrazolo[4,3-c] pyrazole) (TBADNP) and 1,4-dinitramino-3,6-dinitropyrazolo[4,3-c]pyrazole (DNADNP), were first designed and synthesized by the diazotization and nitrification of amino group, and their structures were characterized by IR, 1H NMR, 13C NMR, elementary analysis and MS. The thermal properties of target compounds were studied by means of differential scanning calorimetry (DSC) and thermogravimetry (TG). The thermal decomposition peak temperatures of DADNP, TBADNP and DNADNP are 227, 236 and 288 °C, respectively. Results show that the derivatives of 1,4-diamino-3,6-dinitropyrazolo[4,3-c]pyrazole have better thermal stability.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 2; 321-331
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis, Structure and Energetic Properties of a Catenated N6, Polynitro Compound: 1,1’-Azobis(3,5-dinitropyrazole)
    Autorzy:
    Li, Y.-N.
    Shu, Y.-J.
    Wang, Y.-L.
    Wang, B.-Z.
    Zhang, S.-Y.
    Bi, F.-Q.
    Powiązania:
    https://bibliotekanauki.pl/articles/358573.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    energetic compound
    1,1’-azobis(3,5-dinitropyrazole)
    synthesis
    energetic properties
    Opis:
    A nitrogen-rich, polynitro energetic compound with an N,N-azo linkage, 1,1’-azobis(3,5-dinitropyrazole) (ABDNP), has been synthesized by an oxidative coupling reaction of 1-amino-3,5-dinitropyrazole with different oxidizing agents. The target compound was characterized by IR spectroscopy, 1H and 13C nuclear magnetic resonance spectroscopy, elemental analysis, mass spectra, X-ray diffraction and differential scanning calorimetry (DSC). The DSC results show that 1,1’-azobis(3,5-dinitropyrazole) decomposes at a relatively high onset temperature (202.9 °C), which indicates that 1,1’-azobis(3,5-dinitropyrazole) has acceptable thermal stability. The energetic properties were obtained, with a measured density and heat of formation matched by theoretically computed values based on the B3LYP method.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 2; 321-335
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    GAP/DNTF Based PBX Explosives: a Novel Formula Used in Small Sized Explosive Circuits
    Autorzy:
    An, C.
    Wen, X.
    Wang, J.
    Wu, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/358581.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    explosive circuits
    GAP/DNTF based PBX explosives
    thermal stability
    mechanical sensitivity
    propagation reliability
    detonation velocity
    Opis:
    With 3,4-dinitrofurazanofuroxan (DNTF) and glycidyl azide polymer (GAP) as the main explosive and binder respectively, GAP/DNTF based PBX explosives were designed, prepared and used to fill the small groove of some explosive circuits. The formulation was: DNTF 85 wt.%, GAP 11 wt.%, 2,4-toluene diisocyanate (TDI) and other additives making up the final 4 wt.%. After the uncured slurry mixture was prepared by uniform mixing, a squeezing device was used to charge the circuit groove (dimensions less than 1 mm × 1 mm). Scanning electron microscope (SEM) results showed a fine charging effect. Differential Scanning Calorimetry (DSC) was used to determine the energy of activation (Ea) and the pre-factor (A) of GAP/DNTF and these were compared with those for raw DNTF. The influences and causes of it have been investigated. The experimental results for propagation reliability showed that when the dimensions of the linear groove were 0.8 mm × 0.8 mm, 0.7 mm × 0.7 mm, 0.6 mm × 0.6 mm or 0.5 mm × 0.5 mm, GAP/DNTF based PBX explosives can propagate explosion successfully. Furthermore, the H50 and friction sensitivity of GAP/DNTF based PBX explosives were obtained using the following mechanical sensitivity experiments. These properties are vital if GAP/DNTF based PBX explosives are to be applied in complex explosive circuits.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 2; 397-410
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication and Characterization of PMMA/HMX-based Microcapsules via in situ Polymerization
    Autorzy:
    Jia, X.
    Hou, C.
    Tan, Y.
    Wang, J.
    Ye, B.
    Powiązania:
    https://bibliotekanauki.pl/articles/358134.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    fabrication
    characterization
    HMX
    PMMA
    microcapsules
    Opis:
    Microcapsule technology was applied with nitramine explosives to improve their performance. Polymethyl Methacrylate (PMMA) was selected for the fabrication of 1,3,5,7-tetranitro-1,3,5,7-tetrazocane (HMX) based microcapsules. The PMMA/HMX-based microcapsules were prepared via a facile in situ polymerization of PMMA on the surface of the HMX crystals. Structural characterization of the PMMA/HMX microcapsules was studied systematically by scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier-transform infrared (FT-IR) spectroscopy, and their thermal durability as well as their mechanical sensitivities were measured. The results indicated that spherical microcapsules were formed, with PMMA as the capsule wall and HMX as the core material. The SEM results showed that the grains of the PMMA/HMX microcapsules were spherical and that the particle distribution was homogeneous. XRD and FT-IR analyses indicated that the HMX polymorph was preserved in the optimal β-form during the whole preparative process. The DSC results showed that the PMMA/HMX microcapsules had better thermal decomposition performance, and that the apparent activation energy of the microcapsules had increased by 47.3 kJ/mol compared to the recrystallized HMX, and its thermal stability had greatly improved. In addition, the drop height (H50) had increased from 30.45 cm to 58.49 cm, an increase of 65.81%. Thus, microcapsule technology will have a very wide range of applications in reducing the sensitivity of high energy materials in the future.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 3; 559-572
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Unravelling the Effect of Anthraquinone Metal Salts as Wide-range Plateau Catalysts to Enhance the Combustion Properties of Solid Propellants
    Autorzy:
    Wang, Y.
    Yan, Q.-L.
    An, T.
    Chen, B.
    Ji, Y.-P.
    Wang, W.
    Zhao, F.
    Powiązania:
    https://bibliotekanauki.pl/articles/358042.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    solid propellants
    burning rate catalysts
    anthraquinone metal salts
    wide-range plateau combustion
    Opis:
    Novel lead and copper salts based on anthraquinone, including 1,8-dihydroxyanthraquinone,1,4,5,8-tetrahydroxyanthraquinone and 1,8-dihydroxy-4,5-dinitroanthraquinone, were prepared and characterized by Fourier transform infrared spectroscopy (FTIR), elemental analysis (EA), and X-ray fluorescence (XRF). The catalytic effects of these compounds on the decomposition of nitrocellulose (NC) and on the combustion properties of double-base (DB) and composite modified double-base (CMDB) propellants were comprehensively investigated. The results demonstrated that the burning rate is significantly increased (by 200%) in the lower pressure range (2-6 MPa) as compared to the control systems without added anthraquinone-based salts. Concurrently, the pressure exponents (n) were obviously lower, exhibiting a “wide-range plateau” combustion phenomenon in the middle-pressure region. Specifically, for the DB propellants such a plateau region extended from 10 MPa to 16 MPa for n equal to 0.10, from 10 MPa to 18 MPa for n equal to 0.11 and from 8 MPa to 18 MPa when n is 0.05. In the case of RDX-CMDB propellants, the plateau was found to be in the range 6-18 MPa, with n in the range 0.16-0.27, depending on the type of catalyst, in contrast to the reference CMDB sample, which was characterized by n equal to 0.7 for the same pressure range.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 2; 376-390
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    An Insensitive Booster Explosive: DAAF Surface-coated with Viton A
    Autorzy:
    Li, X.
    Wu, B.
    Liu, S.
    An, C.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358841.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    DAAF
    refinement
    surface-coated
    thermal analysis
    impact sensitivity
    Opis:
    3,3’-Diamino-4,4’-azoxyfurazan (DAAF) is the principal component of an insensitive booster explosive; refined DAAF and DAAF surface-coated with Viton A were prepared. Scanning electron microscopy (SEM), X-ray diffraction (XRD), and differential scanning calorimetry (DSC) were employed to characterize the morphology, composition, and thermal decomposition of these samples. The impact sensitivity and theoretical detonation velocity of DAAF-based composites were also measured and analyzed. The results showed that DAAF surface-coated with Viton A was successfully obtained, and the impact sensitivity of DAAF/Viton A composites was much lower than that of crude DAAF. In addition, DAAF/Viton A composites exhibited better thermal stability compared to crude DAAF and refined DAAF. The theoretical detonation velocity of DAAF/Viton A composites and TATB/Viton A composites are roughly the same. Therefore, there is still great potential for DAAF to be used as the main explosive component of a booster explosive.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 3; 445-455
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation and Characterization of Ultrafine HMX/TATB Explosive Co-crystals
    Autorzy:
    An, C.
    Li, H.
    Zhang, Y.
    Ye, B.
    Xu, C.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358105.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    HMX
    TATB
    ultrafine co-crystals
    ball milling
    mechanical sensitivity
    Opis:
    An explosive co-crystal of 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane (HMX) and 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) was prepared by the ball milling method. The raw materials and co-crystals were characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and Raman spectroscopy. Impact and friction sensitivity of the co-crystals were tested and analyzed. The results showed that the HMX/TATB co-crystals are spherical in shape and 100-300 nm in size. The co-crystals are different from anintimate mixture of HMX/TATB and they exhibit a new co-crystal structure. HMX/TATB co-crystals are formed by N-O···H hydrogen bonding between −NO2 (HMX) and −NH2 (TATB). The drop height of ultrafine HMX/TATB explosive co-crystals is 12.7 cm higher than that of ultrafine HMX, whilst the explosion probability of friction is 20% lower than that of ultrafine HMX. Ultrafine HMX/TATB explosive co-crystals are difficult to initiate under impact and friction conditions.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 4; 876-887
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of Processing Techniques on Mechanical Properties and Impact Initiation of an Al-PTFE Reactive Material
    Autorzy:
    Feng, B.
    Fang, X.
    Li, Y.-C.
    Wu, S.-Z.
    Mao, Y.-M.
    Wang, H.-X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358654.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    Al-PTFE
    reactive materials
    quasi-static compression
    impact initiation
    Opis:
    Reactive materials (RMs) or impact-initiated materials have received much attention as a class of energetic materials in recent years. To assess the influence of processing techniques on mechanical properties and impact initiation behaviors of an Al-PTFE reactive material, quasi -static compression tests and drop-weight tests were performed. Scanning electron microscopy (SEM) was used to identify the characteristics of the interior microstructures of the Al-PTFE samples. A sintering process was found to transform Al-PTFE from a brittle to a ductile material with an increased elasticity modulus (from 108-160 MPa to 256-336 MPa) and yield stress (from 12-16 MPa to 19-20 MPa). Increasing the molding pressure from 36 MPa to 182 MPa increased the elastic modulus of all Al-PTFE samples and also the yield stress of unsintered ones. Unsintered samples in general required less energy to initiate than sintered ones. As the molding pressure increased, the impact initiation energy for sintered Al-PTFE fell from 96 J to 68 J, whereas the initiation energy for unsintered Al-PTFE rose from 68 J to 85 J. PTFE nanofiber networks observed in sintered samples formed under the higher molding pressures could contribute to the opposite trends observed in the impact initiation energy of unsintered and sintered Al-PTFE samples.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 989-1004
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Microstructure, Mechanical and Detonation Properties of Elastomeric Micro/Ultrafine-rubber Modified TNT-based Molten Energetic Composites
    Autorzy:
    Ma, Q.
    Wang, P.-S.
    Luo, G.
    Wen, M.-P.
    Gao, D.-Y.
    Zheng, B.-H.
    Shu, Y.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358122.pdf
    Data publikacji:
    2015
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    micro and ultrafine rubber
    2,4,6-trinitrotoluene
    molten energetic composites
    mechanical properties
    detonation performance
    Opis:
    Elastomeric micro- and ultrafine-rubber are first considered as binders in melt-cast explosives for improving the mechanical properties. Acrylonitrile-butadiene rubber (NBR), in ultrafine fully vulcanized form (UF-NBR), carboxylated acrylonitrile-butadiene rubber (CNBR), in ultrafine fully vulcanized form (UF-CNBR), styrene-butadiene rubber (SBR), in ultrafine fully vulcanized form (UF-SBR), carboxylated styrene-butadiene rubber (CSBR), in ultrafine fully vulcanized form (UF-CSBR), acrylic rubber (ACM), in ultrafine fully vulcanized form (UF-ACM), room temperature vulcanized silicone rubber (RTV), in ultrafine fully vulcanized form (UF-RTV) and polytetrafluoroethene (PTFE) in micro-rubber form (PTFE-M) were utilized for modifying 2,4,6-trinitrotoluene (TNT) based melt-cast explosives. Based on their dispersity in TNT and RDX slurry, only UF-NBR, UF-CNBR and PTFE-M can be used. In the modification experiment, their influence on the mechanical and detonation performance of the matrixes were studied, as well as the impact sensitivity. Compared with PTFE-M and UF-CNBR, UF-NBR improved the tensile and compressive strength of the original formulation CYCLOTOL-65/35. The toughening mechanism was also explained through interfacial interactions and fracture energy analysis. The predicted detonation properties of the modified formulations (detonation pressure variations from 26 to 28 GPa, detonation velocity variations from 7900 to 8100 m/s) are at the same energy level as CYCLOTOL-65/35. In addition, the drop hammer impact testing results confirm that the formulation containing UF-NBR is more sensitive than the one with UF-CNBR, with the same amount of additive.
    Źródło:
    Central European Journal of Energetic Materials; 2015, 12, 4; 723-743
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermally induced damage in hexanitrohexaazaisowurtzitane
    Autorzy:
    Tian, Q.
    Yan, G.
    Sun, G.
    Huang, C.
    Xie, L.
    Chen, B.
    Huang, M.
    Li, H.
    Liu, X.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358735.pdf
    Data publikacji:
    2013
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    CL-20
    SAXS
    AFM
    thermal effects
    voids
    Opis:
    The evolution of the microstructure of hexanitrohexaazaisowurtzitane (CL-20) after a thermal stimulus plays a key role in the performance of CL-20. In the current work, microstructural variations of CL-20 caused by thermal treatment were investigated by X-ray diffraction, in situ variable-temperature optical microscopy, atom force microscopy, and small-angle X-ray scattering. A wave-like process, an abrupt volume expansion, movement, and fragmentation of CL-20 particles during phase transition were observed. After the phase transition (160 °C) the CL-20 sample acquired a very rough surface with numerous dimple depressions, and during the thermal decomposition stage (200 °C) a large number of voids were produced in both the bulk and the surface of the CL-20.
    Źródło:
    Central European Journal of Energetic Materials; 2013, 10, 3; 359-369
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Microstructural Evolution in HMX Based Plastic-bonded Explosive During Heating and Cooling Process: an in situ Small-angle Scattering Study
    Autorzy:
    Yan, G.
    Tian, Q.
    Liu, J.
    Fan, Z.
    Sun, G.
    Zhang, C.
    Wang, Y.
    Chen, B.
    Gong, J.
    Zhou, X.
    Yang, Z.
    Nie, F.
    Li, J.
    Li, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358618.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    SANS
    SAXS
    HMX-PBX
    thermal damages
    phase transition
    Opis:
    The thermal damage in octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) based plastic-bonded explosive (PBX) was investigated using in situ small-angle neutron and X-ray scattering techniques. The microstructural evolution was quantitatively characterized by the model fitting parameters of total interfacial surface area (Sv) and void volume distribution. The Sv of HMX-PBX decreased markedly above 100 °C, indicating the movement of binder into the voids. After subsequent cooling to room temperature, the scattering intensity increased significantly with increasing storage time, and a new population of voids with average diameter of 20 nm was observed, accompanied by the gradual phase transition of HMX from δ- to β-phase. The experimental results implied that serious damage within the HMX-PBX was developed during storage after heating.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 916-926
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-14 z 14

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