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    Wyświetlanie 1-7 z 7
    Tytuł:
    Enhanced Non-linear Viscoelastic Properties of Polymer Bonded Explosives Based on Graphene and a Neutral Polymeric Bonding Agent
    Autorzy:
    Lin, C.
    He, G.
    Liu, J.
    Pan, L.
    Liu, S.
    Powiązania:
    https://bibliotekanauki.pl/articles/358748.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    polymer bonded explosives
    graphene
    neutral polymeric bonding agent
    creep behaviour
    Opis:
    During their long-term storage and transport, polymer bonded explosives (PBXs) will be subjected to complex thermal physical environments with combined thermal and mechanical loads. The creep behaviour results in a change of physical and mechanical properties, which consequently influences the explosive performance. In this work, graphene and a neutral polymeric bonding agent (NPBA) were selected to improve the non-linear creep properties of 1,3,5-triamino-2,4,6-trinitrobenzene (TATB)-based PBXs. The results were compared with the creep response of the corresponding PBXs without additives and with graphene alone. It was observed that graphene and an NPBA exhibited a positive effect, improving the creep resistance of TATB-based PBXs. The compressive and tensile strength of 0.5 wt.% graphene-filled PBXs were improved by 5.1% and 29.2%, respectively, compared to raw TATB-based PBXs without additives. The performance of the PBXs was further enhanced by the addition of 0.1 wt.% NPBA. For a given stress and temperature, the TATB-based PBXs with graphene and NPBA deformed significantly less than the PBXs filled with graphene alone.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 4; 788-805
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Factors Affecting the Measurement of the Percentage of Gaseous Products from Boron-based Fuel-rich Propellants
    Autorzy:
    Liu, L.-L.
    He, G.-Q.
    Wang, Y.-H.
    Liu, P.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358720.pdf
    Data publikacji:
    2014
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    fuel-rich propellant
    percentage gaseous products
    combustion
    filter media
    Opis:
    Acid-washed asbestos, carbon fibre, and MgO with carbon fibre were used as the filter media in order to compare their filtering qualities in the estimation of the percentage of gaseous products (PGP) arising from the combustion of singlebase propellants, double-base propellants, and boron-based fuel-rich propellants. The comparison was based on an analysis of the experimentally registered influence of the propellant formulation, the propellant load, the maximum chamber pressure and the thickness of the MgO filter layer on the PGP from the fuel-rich propellant, and in particular on the PGP produced by combustion of boron-based fuel-rich propellant. The results showed that the experimental values of the PGP were closer to the theoretically predicted values when carbon fibre mixed with MgO powder was used as the filter medium. The PGP of boron-based fuel-rich propellant increased when the AP was in part replaced by HMX, when the AP content was increased and when boron was in part replaced by magnesium-aluminum alloy. In terms of the apparatus used in these experiments, the propellant loading density was found to have little correspondence with the PGP for boron-based fuel-rich propellant. The optimal propellant loading density for the chamber volume of 85 cm3 was found to be 2-2.5 g, in view of the reliability and safety of the experiment. It is emphasised that the thickness of the MgO filter layer is very important for the accuracy and reliability of the experiment, and that the optimum should be determined by experiment.
    Źródło:
    Central European Journal of Energetic Materials; 2014, 11, 1; 15-29
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Ignition and Combustion Performance of the Primary Condensed-phase Combustion Products from Boron-based Fuel-rich Propellants
    Autorzy:
    Liu, L.-L.
    He, G.-G.
    Wang, Y.-H.
    Hu, S.-G.
    Powiązania:
    https://bibliotekanauki.pl/articles/358859.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    boron-based fuel-rich propellant
    primary combustion products
    ignition
    combustion performance
    Opis:
    The primary condensed-phase combustion products of a boron-based fuel-rich propellant were ignited using a high-power CO2 laser in a pressurized and windowed combustion chamber under variable pressure. The ignition and combustion performances were characterized using an ultraviolet-visible spectrometer and a high-speed camera. The experimental results showed that the combustion of the condensed-phase combustion products originate from the combustion of carbon, and boron may not take any part in the combustion process because of the formation of a thick boron oxide coating and agglomeration after the primary combustion process. Both particle size and the ingredients play an important role in the combustion reaction of the condensed-phase products. It was observed that a lower particle size and a higher boron carbide content are beneficial for the combustion reaction of the products; higher primary and secondary combustion pressures clearly improved the secondary combustion efficiency of the propellant in the combustion reaction.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 2; 448-460
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Predicted Crystal Structures, Analysis, Impact Sensitivities and Morphology of Solid High-Energy Complexes: Alkaline-Earth Carbohydrazide Perchlorates
    Autorzy:
    Liu, Y.
    Zhang, R.
    Feng, C.-G.
    Yang, L.
    Zhang, T.-L.
    Powiązania:
    https://bibliotekanauki.pl/articles/358890.pdf
    Data publikacji:
    2015
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    crystal structure
    density of state
    thermodynamic property
    impact sensitivity
    crystal morphology
    Opis:
    The crystal structures, density of states, energy gap, thermodynamic properties, impact sensitivities and morphology of beryllium carbohydrazide perchlorate ([Be(CHZ)3](ClO4)2), magnesium carbohydrazide perchlorate ([Mg(CHZ)3](ClO4)2), calcium carbohydrazide perchlorate ([Ca(CHZ)3] (ClO4)2), strontium carbohydrazide perchlorate ([Sr(CHZ)3](ClO4)2) and barium carbohydrazide perchlorate ([Ba(CHZ)3](ClO4)2) were investigated using the density functional theory (DFT) and crystal morphology theory. The results show that all of the complexes have six-coordinated distorted octahedra, which is different from previous works. This was rationalised by consideration of the intermolecular interactions in the crystal structures. Hence the crystal structure is now more reliable. The chemical reactions of the whole molecule may be triggered by an electron transition of CHZ or ClO4 −. Furthermore the energy gaps were observed, and the values of the impact sensitivities were inferred to have the following sequence: [Be(CHZ)3](ClO4)2 > [Mg(CHZ)3](ClO4)2 > [Sr(CHZ)3](ClO4)2 > [Ca(CHZ)3](ClO4)2 > [Ba(CHZ)3](ClO4)2. In addition, the thermodynamic equations at 25-1000 K were obtained. The positive values of the standard molar free enthalpies shows that carbohydrazide perchlorates are stable at 298.15 K. The (1 0 -1) and (0 0 2) faces are the most important growth directions of the crystal morphologies, and have the minimum growth rates. From the cleaved main growth faces, it can be deduced that surface active agents with active hydrogen atoms in the functional groups could be used as crystal-control reagents to control the crystal morphology for alkaline-earth carbohydrazide perchlorates.
    Źródło:
    Central European Journal of Energetic Materials; 2015, 12, 2; 229-248
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermally induced damage in hexanitrohexaazaisowurtzitane
    Autorzy:
    Tian, Q.
    Yan, G.
    Sun, G.
    Huang, C.
    Xie, L.
    Chen, B.
    Huang, M.
    Li, H.
    Liu, X.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358735.pdf
    Data publikacji:
    2013
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    CL-20
    SAXS
    AFM
    thermal effects
    voids
    Opis:
    The evolution of the microstructure of hexanitrohexaazaisowurtzitane (CL-20) after a thermal stimulus plays a key role in the performance of CL-20. In the current work, microstructural variations of CL-20 caused by thermal treatment were investigated by X-ray diffraction, in situ variable-temperature optical microscopy, atom force microscopy, and small-angle X-ray scattering. A wave-like process, an abrupt volume expansion, movement, and fragmentation of CL-20 particles during phase transition were observed. After the phase transition (160 °C) the CL-20 sample acquired a very rough surface with numerous dimple depressions, and during the thermal decomposition stage (200 °C) a large number of voids were produced in both the bulk and the surface of the CL-20.
    Źródło:
    Central European Journal of Energetic Materials; 2013, 10, 3; 359-369
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Coating of LiBH4 and Its Effect on the Decomposition of RDX and AP
    Autorzy:
    Ding, X.
    Shu, Y.
    Chen, Z.
    Liu, N.
    Gou, B.
    Zhang, J.
    Wu, M.
    Xie, G.
    Dang, T.
    Powiązania:
    https://bibliotekanauki.pl/articles/358086.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    coating
    hydride
    additive
    hygroscopicity
    DSC
    Opis:
    The novel fuel additive LiBH4 was introduced as an energetic component for its outstanding hydrogen content, perfect burning performance and high reactivity. In order to limit the hygroscopicity and to improve the stability in the air, LiBH4 was coated on the surface with wax and polyester carbonate. The final product was characterized by scanning electron microscopy (SEM), X-ray photoelectron energy spectroscopy (XPS) and Raman spectroscopy, while the stability in air was investigated by regular checking of variations in weight. The results show that a uniform coating layer was formed on the surface of the LiBH4, and the coverage was estimated from the boron content as approximately 82%. A healing effect was confirmed on defective surfaces exposed to air; the coating layer improves the relative stability by 50.7%. Furthermore, LiBH4 as an additive to promote the thermal decomposition of 1,3,5-trinitro-1,3,5-trazinane (RDX) and ammonium perchlorate (AP) was explored by differential scanning calorimetry (DSC), in which the catalytic effects of pure LiBH4 and coated LiBH4 were compared, and indicated that the coating does not decrease the reactivity of LiBH4. It is suggested that surface coating with some inert materials is a simple and effective method for improving the storage and performance of LiBH4, while ensuring its reactivity.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 1; 134-151
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Microstructural Evolution in HMX Based Plastic-bonded Explosive During Heating and Cooling Process: an in situ Small-angle Scattering Study
    Autorzy:
    Yan, G.
    Tian, Q.
    Liu, J.
    Fan, Z.
    Sun, G.
    Zhang, C.
    Wang, Y.
    Chen, B.
    Gong, J.
    Zhou, X.
    Yang, Z.
    Nie, F.
    Li, J.
    Li, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358618.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    SANS
    SAXS
    HMX-PBX
    thermal damages
    phase transition
    Opis:
    The thermal damage in octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) based plastic-bonded explosive (PBX) was investigated using in situ small-angle neutron and X-ray scattering techniques. The microstructural evolution was quantitatively characterized by the model fitting parameters of total interfacial surface area (Sv) and void volume distribution. The Sv of HMX-PBX decreased markedly above 100 °C, indicating the movement of binder into the voids. After subsequent cooling to room temperature, the scattering intensity increased significantly with increasing storage time, and a new population of voids with average diameter of 20 nm was observed, accompanied by the gradual phase transition of HMX from δ- to β-phase. The experimental results implied that serious damage within the HMX-PBX was developed during storage after heating.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 916-926
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-7 z 7

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