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Tytuł:
Hydrogen Sensor Of TiO2-Based Nanomaterials
Sensor wodoru na bazie nanomateriałów TiO2
Autorzy:
Łysoń-Sypień, B.
Zakrzewska, K.
Gajewska, M.
Radecka, M.
Powiązania:
https://bibliotekanauki.pl/articles/354826.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2 nanomaterials
Cr dopant
hydrogen sensor
nanomateriały TiO2
domieszka chromu
sensor wodoru
Opis:
The aim of this research was to examine gas sensing properties of TiO2 based nanomaterials. Nanopowders of Cr doped TiO2 with constant Specific Surface Area, SSA, were obtained using Flame Spray Synthesis technique, FSS. Nanomaterials were characterized by Brunauer – Emmett – Teller adsorption isotherms, BET, X – ray diffraction, XRD, Transmission Electron Microscopy, TEM, optical spectrometry UV – vis with the use of an integrating sphere as well as impedance spectroscopy. Detection of hydrogen was carried out over the concentration range of 50 - 3000 ppm at the temperatures extending from 200 to 400°C and synthetic air working as a reference atmosphere. As a result of experiments it appeared that incorporation of 5 at.% of Cr into TiO2 improved hydrogen sensing features due to small crystallite size and predominance of rutile polymorphic phase.
Przedmiotem pracy są nanomateriały na bazie TiO2 do zastosowań sensorowych. Nanoproszki TiO2 domieszkowane chromem o stałej powierzchni właściwej SSA (ang. Specific Surface Area) otrzymano przy pomocy techniki syntezy w płomieniu FSS (ang. Flame Spray Synthesis). Materiały poddano charakteryzacji z wykorzystaniem: izoterm adsorpcyjnych Brunauer – Emmett – Teller, BET, dyfraktometrii rentgenowskiej, XRD, transmisyjnej mikroskopii elektronowej, TEM, spektroskopii optycznej UV – vis oraz spektroskopii impedancyjnej. Pomiar własności sensorowych został przeprowadzony dla koncentracji H2 w zakresie 50-3000 ppm w przedziale temperatur 200-400°C. Wykazano, że najlepiej na wodór odpowiada próbka TiO2: 5 at.% Cr charakteryzująca się małym rozmiarem krystalitów oraz przewagą fazy rutylu.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2A; 935-940
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Gas sensors based on nanostructures of semiconductors ZnO and TiO2
Autorzy:
Pustelny, T.
Procek, M.
Maciak, E.
Stolarczyk, A.
Drewniak, S.
Urbańczyk, M.
Setkiewicz, M.
Gut, K.
Opilski, Z.
Powiązania:
https://bibliotekanauki.pl/articles/201719.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gas sensors
nanostructures
TiO2
ZnO
Opis:
The paper presents a resistance structures with sensor layers based on nanostructures elaborated on the base of TiO2 and ZnO. The structures were tested concerning their sensitivities to the effects of nitrogen dioxide in the atmosphere of synthetic air. The TiO2 and ZnO nanostructures played the role of sensor layers. Investigations have proved that the elaborated resistance structures with TiO2 and ZnO layers are sensitive to the presence of NO2 in the atmosphere of synthetic air. The resistance of the structure amounted to about 20 in the case of ZnO structures and to about 200 in the case of TiO2 structures. The investigations confirmed that resistance structures with ZnO and TiO2, exposed to the effect of nitrogen dioxide in the atmosphere of synthetic air changes their resistances relatively fast. This indicates that such structures might be practically applied in sensors of nitrogen dioxide ensuring a short time of response.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2012, 60, 4; 853-859
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Simple synthesis of Black TiO2 Nanofibers Via Calcination in Inert Atmosphere
Autorzy:
Ji, Myeongjun
Kim, Eung Ryong
Park, Mi-Jeong
Jeon, Hee Yeon
Moon, Jaeyun
Byun, Jongmin
Lee, Young-In
Powiązania:
https://bibliotekanauki.pl/articles/2174573.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
black TiO2
nanofibers
electrospinning
calcination
atmosphere
Opis:
Black TiO2 nanofibers have recently emerged as a promising material that has both advantages of black metal oxide and one-dimensional nanostructure. However, current reduction-based synthesis approaches are not compatible with practical applications because these processes require high process costs, complicated processes, and sophisticated control. Therefore, it is still necessary to develop a simple and facile method that can easily introduce atomic defects during the synthesis process. This work suggests an electrospinning process with an antioxidant and subsequent calcination process for the facile synthesis of black TiO2 nanofibers. The synthesized black TiO2 nanofiber has an average diameter of 50.3 nm and a rutile structure. Moreover, this nanofiber represented a noticeable black color and a bandgap of 2.67 eV, clearly demonstrating the bandgap narrowing by the introduced atomic defects.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 4; 1481--1486
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Analysis Of Structure For The Multi-Layered Of Ge/TiO2 Films Prepared By The Differential Pressure Co-Sputtering
Analiza struktury wielowarstwowych filmów Ge/TiO2 wytwarzanych metodą różnicowo-ciśnieniowego współrozpylania jonowego
Autorzy:
Adachi, Y.
Abe, S.
Matsuda, K.
Nose, M.
Powiązania:
https://bibliotekanauki.pl/articles/354833.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2
solar cells
sputtering
ogniwa słoneczne
rozpylanie
Opis:
We tried to fabricate the Ge/TiO2 composite films with the differential pressure (pumping) co-sputtering (DPCS) apparatus in order to improve the optical properties. In the study, the micro structure of these thin films has been evaluated. TEM image revealed that the thin film was alternately layered with TiO2 and Ge, lattice fringes were observed both of Ge layer and TiO2 layer. There were portions that lattice fringe of Ge was disturbed near the interface of Ge and TiO2. X-ray photoelectron spectroscopy elucidated that there were few germanium oxides and a part with the thin film after annealed.
W pracy przedstawiono rezultaty badań mających na celu wytworzenie warstw kompozytowych Ge/TiO2 wykorzystując aparaturę do różnicowo-ciśnieniowego współrozpylania jonowego (DPCS) w celu poprawy właściwości optycznych. Mikrostruktura warstw została zbadana z zastosowaniem mikroskopii TEM. Analiza TEM wykazała, że cienki film składał się z naprzemiennie ułożonych warstw TiO2 oraz Ge, a dodatkowo zlokalizowano krawędzie sieci przestrzennych Ge i TiO2. Rentgenowska spektroskopia fotoelektronów wykazała niewielkie ilości tlenków germanu oraz występowanie cienkiego filmu po procesie wyżarzania.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2A; 963-964
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization of SnO2/TiO2 with the Addition of Polyethylene Glycol via Sol-Gel Method for Self-Cleaning Application
Autorzy:
Halin, Dewi Suriyani Che
Azliza, Azani
Razak, Kamrosni Abdul
Abdullah, Mohd Mustafa Al Bakri
Salleh, Mohd Arif Anuar Mohd
Wahab, Juyana A
Chobpattana, Varistha
Kaczmarek, Łukasz
Nabiałek, Marcin
Jeż, Bartłomiej
Powiązania:
https://bibliotekanauki.pl/articles/2203743.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2
SnO2
thin film
polyethylene glycol
self-cleaning
Opis:
TiO2 is one of the most widely used metal oxide semiconductors in the field of photocatalysis for the self-cleaning purpose to withdraw pollutants. Polyethylene glycol (PEG) is recommended as a stabilizer and booster during preparation of water-soluble TiO2. Preparation of SnO2/TiO2 thin film deposition on the surface of ceramic tile was carried out by the sol-gel spin coating method by adding different amount of PEG (0g, 0.2g, 0.4g, 0.6g, 0.8g) during the preparation of the sol precursor. The effects of PEG content and the annealing temperature on the phase composition, crystallite size and the hydrophilic properties of SnO2/TiO2 films were studied. The X-ray diffraction (XRD) spectra revealed different phases existed when the films were annealed at different annealing temperatures of 350°C, 550°C and 750°C with 0.4 g of PEG addition. The crystallite sizes of the films were measured using Scherrer equation. It shows crystallite size was dependent on crystal structure existed in the films. The films with mixed phases of brookite and rutile shows the smallest crystallite size. In order to measure the hydrophilicity properties of films, the water contact angles for each film with different content of PEG were measured. It can be observed that the water contact angle decreased with the increasing of the content of PEG. It shows the superhydrophilicity properties for the films with the 0.8 g of PEG annealed at 750°C. This demonstrates that the annealed temperature and the addition of PEG affect the phase composition and the hydrophilicity properties of the films.
Źródło:
Archives of Metallurgy and Materials; 2023, 68, 1; 243--248
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure of Al2O3-13TiO2 coatings deposited from nanoparticles by plasma spraying
Mikrostruktura powłok Al2O3-13TiO2 natryskanych plazmowo z nanocząstek
Autorzy:
Góral, A.
Lityńska-Dobrzyńska, L.
Żórawski, W.
Berent, K.
Wojewoda-Budka, J.
Powiązania:
https://bibliotekanauki.pl/articles/355112.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al2O3-13TiO2 coating
microstructura
plasma spraying process
powłoka Al2O3-13TiO2
mikrostruktura
proces natryskiwania plazmowego
Opis:
The aim of the study was to characterize nanostructured Al2O3-13TiO2 coatings deposited by plasma spraying on a grit blasted steel substrate. The Al2O3-13TiO2 coatings were characterized using scanning and transmission electron microscopy and X-ray diffraction techniques. Obtained coatings possessed a unique microstructure consisting of fully melted regions with the microstructure similar to a typical plasma sprayed lamellar morphology as the conventional coatings and areas comprising unmelted or partially melted nanosized particles. The analysis showed that most of the α-Al2O3 phase from the nanostructured powders transformed into γ-Al2O3 phase after plasma spraying process. Moreover, the presence of amorphous phase was also observed.
W pracy przedstawiono charakterystykę nanostrukturalnych powłok Al2O3-13TiO2 natryskiwanych plazmowo na podłożu stalowym. Powłoki scharakteryzowano za pomocą skaningowej i transmisyjnej mikroskopii elektronowej oraz technik dyfrakcji rentgenowskiej. Mikrostruktura uzyskanych powłok składała się z obszarów powstałych z całkowicie stopionych proszków, podobnych do mikrostruktury powłok wytworzonych z proszków o rozmiarach konwencjonalnych, jak również z obszarów zawierających niestopione lub częściowo stopione nanocząstki. Wykazano, ze większość fazy α-Al2O3 występującej w materiale proszkowym uległa przemianie w faze γ-Al2O3 w trakcie procesu natryskiwania plazmowego. Zidentyfikowano również obecność fazy amorficznej.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 2; 335-339
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
MHD Supported Electroreduction of Formate Nickel Complexes with Simultaneous Incorporation of TiO2 Particles
Autorzy:
Mech, K.
Powiązania:
https://bibliotekanauki.pl/articles/356370.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrodeposition
Ni-TiO2 composites
composite coatings
MHD effect
Opis:
The present work concerns analysis of the possibilities of synthesis of Ni-TiO2 composite coatings from electrolytes containing formate nickel complexes. A magnetic field was applied as an additional factor enabling modification of properties of the synthesized coatings through its influence on electrode processes. The presented data describes the effect of electrode potential, TiO2 concentration in the electrolyte as well as the value of the magnetic field induction vector on the deposition rate, composition, current efficiency, structure, surface states and morphology of synthesized coatings. The studies were preceded by thermodynamic analysis of the electrolyte. The obtained results indicated possibilities of synthesis of composites containing up to 0.97wt.% of TiO2. Depending on applied electrolysis conditions current efficiency amounted to from 61.2 to 75.1%.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 1; 219-227
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of nano TiO2/Micro (SiC/B4C) Reinforcement on the Mechanical, Wear and Corrosion Behaviour of A356 Metal Matrix Composite
Autorzy:
Paulraj, D.
Jeyakumar, Palanisamy D.
Rajamurugan, G.
Krishnasamy, Prabu
Powiązania:
https://bibliotekanauki.pl/articles/2049401.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nano TiO2
SiC
B4C
wear
corrosion
Opis:
This work investigates the distribution and the effect of synthesized nano TiO2, micro SiC and B4C particle on the aluminium (A356) metal matrix composites (AMMC). The consequences of this reinforcement on the mechanical, tribology and corrosion behaviour of the AMMC matrix are analyzed. The nano TiO2 is synthesized by wet chemistry sol-gel process, and the reinforcements are added with A-356 by stir casting method. The ASTM standard test specimens are characterized through mechanical, tribology, and corrosion tests for identifying their properties. The metallurgical characterization has been deliberated through XRD and SEM with EDS. in the tensile test results, the percentage of elongation is dropped drastically by 73% due to the enhanced volume % of nano TiO2, micro SiC, and B4C particles. The particle addition of the wear rate and weight loss are reduced at different volume percentages of the A356 matrix. The time plays a significant role in the corrosion rate. The test results also confirm that the corrosion rate is comparatively minimum in 24 hrs (592.35 mm/yr) duration than the 48 hrs (646.368 mm/yr) in both the solutions.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 3; 871-880
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis of Single Crystalline Titanium Oxide and Sodium Titanate Nanorods via Salt-Assisted Ultrasonic Spray Pyrolysis
Autorzy:
Hwangbo, Y.
Yoo, J.-H.
Lee, Y.-I.
Powiązania:
https://bibliotekanauki.pl/articles/352337.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2
nanorods
salt
Ultrasonic Spray Pyrolysis
optical properties
Opis:
The simple and continuous synthesis of single crystalline anatase titanium dioxide and sodium titanate nanorods by a saltassisted ultrasonic spray pyrolysis method is demonstrated. This method does not require expensive precursors, long reaction time, and physical templates or surfactant. In addition, its continuous nature makes it a suitable method for the large-scale preparation. Moreover, the effect of a salt concentration in a starting solution on material properties, including morphology and phase of the synthesized products was systematically investigated. The synthesized nanorods had one-dimensionality, a single crystalline and the average diameter of 12.3 nm with dual phases of titanium dioxide and sodium titanate by FE-SEM, XRD, HR-TEM as well as FFT-converted SAED pattern analysis.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1411-1414
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrochemical sensors based on TiO2–Fe2O3 coupled system
Autorzy:
Kusior, Anna
Karoń, Iwona
Radecka, Marta
Powiązania:
https://bibliotekanauki.pl/articles/220949.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
electrochemical sensor
cyclic voltammetry
hydrazine
TiO2
Fe2O3
Opis:
Recently, transition metal oxides, which exhibit favorable catalytic abilities, have also been investigated as a material for the detection of hydrazine (N2H4). It has been reported that mixed metal oxides usually offer a higher electrochemical activity than binary oxides. In this work, a TiO2-Fe2O3 coupled system is presented as an enhanced material with major applications in electrochemical detectors. The electrochemical behavior of glassy carbon electrodes modified with TiO2-Fe2O3 in the absence and presence of hydrazine was evaluated via cyclic voltammetry (CV). Experimental results also suggest that the formation of the TiO2-Fe2O3 coupled system enhances electrochemical catalytic performance in N2H4 detection. The modificationTiO2+2 mol% Fe2O3 provides good analytical performance of detection (0.13 mM) and quantification limits (0.39 mM). The presented coupled system provides the premise for a suitable material for a stable and sensitive N2H4 sensor.
Źródło:
Metrology and Measurement Systems; 2020, 27, 2; 301-311
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrophoretic deposition of nc-TiO2/chitosan composite coatings on X2CrNiMo17-12-2 stainless steel
Autorzy:
Ledwig, P.
Kot, M.
Moskalewicz, T.
Dubiel, B.
Powiązania:
https://bibliotekanauki.pl/articles/351827.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chitosan
TiO2
electrophoretic deposition
X2CrNiMo17-12-2 steel
Opis:
This paper presents the results of the optimization of electrophoretic deposition parameters for manufacturing of nc-TiO2/chitosan composite coatings on X2CrNiMo17-12-2 steel as well as characterization of their microstructure, electrochemical properties and adhesion to the substrate. The parameters of the deposition, such as composition, pH and zeta potential of suspensions as well as voltage and process time were investigated. The microstructure of the coatings was characterized using scanning and transmission electron microscopy. Obtained coatings were crack-free and uniform. The adhesion strength to the substrate was measured by scratch-test method. The deposited coatings improve corrosion resistance of steel, what was confirmed by the results of the potentiodynamic polarization test in Ringer’s solution.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 405-410
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Corrosion Resistance of Composite nc-TiO2/Ni Coating on 316L Steel
Autorzy:
Ledwig, P.
Dubiel, B.
Powiązania:
https://bibliotekanauki.pl/articles/353248.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nc-TiO2/Ni coatings
electrodeposition
nanocomposite
microstructure
corrosion resistance
Opis:
The aim of this work was to obtain composite of nc-TiO2/Ni coatings on 316L steel and to characterize their corrosion resistance. In order to investigate the influence of the addition of TiO2 nanoparticles, both pure Ni and composite nc-TiO2/Ni coatings were electrodeposited from nickel citrate baths. The microstructure of the coatings was examined by scanning and transmission electron microscopy. The nc-TiO2/Ni coatings were about 10 μm thick. Their microstructure consisted of TiO2 nanoparticles uniformly distributed in nanocrystalline Ni matrix. The corrosion resistance of the coatings was measured using impedance spectroscopy and polarization curves techniques in Ringer’s solution. It was determined that the addition of nano-TiO2 particles improved corrosion resistance and reduced corrosion rate of the coated steel.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 4; 2455-2460
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Flame Retardant and Processing Conditions on Selected Properties of Mouldings Made of ABS
Autorzy:
Trzaskalska, Milena
Powiązania:
https://bibliotekanauki.pl/articles/2174593.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
injection moulding
ABS
PS
TiO2
flame retardant
mechanical properties
Opis:
Thanks to dyeing of polymers, the possibilities of their use are constantly increasing. It is equally important to use additives that will have several functions. A perfect example is titanium dioxide used as an optical brightener and a flame retardant at the same time. Mostly it is used in the form of a powder. However, there are no studies where TiO2 is used as a colourbatch based on the different polymer matrix. The aim of the work was to investigate the effect of titanium white in the form of colourbatch on the flammability and selected properties of mouldings produced in various processing conditions. Colourbatch based on PS matrix, was used in the research. The variable processing parameters were: injection temperature Tw, volume flow rate Vw, residence time and the addition of a colourbatch. On the basis of the measurements, it was found that the processing conditions and the addition of the colourbatch have low effect on the hardness of the mouldings, which was in the range from 75.59° Sh D (Shore type D) to 81.95° Sh D. It was also noted that the addition of colourbatch with TiO2 and increasing injection temperature reduces impact strength even by several dozen percent. Moreover, it was found that use of TiO2 causes a delay in the ignitability of the samples in selected cases. It is difficult to determine whether the variable processing conditions or the addition of TiO2 on the PS matrix have a greater impact on the ignitability of the moulded parts.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 4; 1381-1386
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructural Studies of Ag/TiO2 Thin Film; Effect of Annealing Temperature
Autorzy:
Kamrosni, Abdul Razak
Dewi Suryani, Che Halin
Azliza, Azani
Mohd Mustafa Al Bakri, Abdullah
Mohd Arif Anuar, Mohd Salleh
Norsuria, Mahmed
Chobpattana, Varistha
Kaczmarek, L.
Jeż, Bartłomiej
Nabiałek, Marcin
Powiązania:
https://bibliotekanauki.pl/articles/2048839.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ag/TiO2
annealing temperature
microstructure
optical properties
thin film
Opis:
Microstructures are an important link between materials processing and performance, and microstructure control is essential for any materials processing route where the microstructure plays a major role in determining the properties. In this work, silverdoped titanium dioxide (Ag/TiO2) thin film was prepared by the sol-gel method through the hydrolysis of titanium tetra-isopropoxide and silver nitrate solution. The sol was spin coated on ITO glass substrate to get uniform film followed by annealing process for 2 hours. The obtained films were annealed at different annealing temperatures in the range of 300°C-600°C in order to observe the effect on crystalline state, microstructures and optical properties of Ag/TiO2 thin film. The thin films were characterized by X-Ray diffraction (XRD), scanning electron microscopy (SEM), and UV-Vis spectrophotometry. It is clearly seen, when the annealing temperature increases to 500°C, a peak at 2θ = 25.30° can be seen which refers to the structure of TiO2 tetragonal anatase. The structure of Ag/TiO2 thin film become denser, linked together, porous and uniformly distributed on the surface and displays the highest cut-off wavelength value which is 396 nm with the lowest band gap value, which is 3.10 eV.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 1; 241-245
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Impedance spectroscopy in H2 sensing with TiO2/SnO2 nanomaterials
Autorzy:
Szafraniak, Bartłomiej
Kusior, Anna
Radecka, Marta
Zakrzewska, Katarzyna
Powiązania:
https://bibliotekanauki.pl/articles/221225.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
impedance spectroscopy
TiO2
SnO2
hydrogen detection
resistive-type gas sensors
Opis:
Alternating current a.c. measurements enable to understand the physical and chemical processes occurring in semiconductor materials. Impedance spectroscopy has been successfully applied to study the responses of gas sensors based on metal oxides, such as TiO2, SnO2 and TiO2/SnO2 nanocomposites. This work is devoted to dynamic measurements of hydrogen sensor behaviour over the temperature range of 300-450°C. Frequency dependence of the impedance signal gives evidence that 50 mol% TiO2/50 mol% SnO2 nanocomposites should be treated as resistive-type sensors. Temporal evolution of the response to 500 ppm H2 at 320°C indicates a very short response time and much longer recovery.
Źródło:
Metrology and Measurement Systems; 2020, 27, 3; 417-425
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 33

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