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Tytuł:
Detonation deposited Fe-Al coatings Part III: Morphology of the Ni(Cr) and Ni(Al) interlayers and Fe-Al coating sprayed onto the 045 steel substrate
Powłoki Fe-Al osadzane detonacyjnie. Część III: budowa warstw pośrednich Ni(Cr) I Ni(Al) oraz powłoki Fe-Al na podłożu stali węglowej osadzanych detonacyjnie
Autorzy:
Pawłowski, A.
Senderowski, C.
Bojar, Z.
Bonarski, J.
Major, Ł.
Powiązania:
https://bibliotekanauki.pl/articles/351088.pdf
Data publikacji:
2011
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
powłoki międzymetaliczne
warstwy pośrednie Ni(Cr) i Ni(Al)
G-dun spraying
Fe-Al intermetallic coatings
Ni(Al) and Ni(Cr) interlayers
Opis:
The morphology of interlayars and the coating of Fe-Al phase detonation sprayed (DGS) on the substrate of 045 steel was analysed in the work. The Ni(Al) layer, first from the substrate side consisted of Ni with inclusions of Al oxide. The second deposited layer was Ni(Cr), which contained lamellas of Cr in the Ni matrix. The phases present in the transition layers and in the coating were identified with SEM, and EDX methods (linear and point changes of chemical composition). The identification was confirmed with the X-ray technique and TEM microstructure analysis. It was established that Al oxides and AlNiO phases appeared in the DGS process after partial melting and oxidation of Al particles, while in the not melted part of grains small grain morphology was observed. Using the X-ray method, the FeAl2O4, Fe3Al and FeAl phases were identified in the coating, the Cr and Cr2Ni3 phase in the Ni(Cr) interlayer as well as pure nickel and the NiAl phase in the Ni(Al) interlayer. The occurrence of brittle phases of Al oxide and AlNiO phases near the boundaries of layers might result in the increase of tendency to delamination. Hence the reduction of the Al content seems advantageous from the point of view of mechanical properties of the joint.
W pracy poddano analizie metodą skaningowej - SEM i transmisyjnej- TEM mikroskopii elektronowej, budowę warstw pośrednich i powłokę faz typu Fe-Al natryskiwanych detonacyjnie (DGS) na podłoże stali 045. Warstwa Ni(Al) pierwsza od podłoża składa się z niklu z wtrąceniami Al i tlenku glinu. Na niej osadzona jest warstwa druga Ni(Cr) składającą się z warstewek chromu w osnowie niklu. Metodami EDX, liniowej zmiany składu oraz punktowej analizy zidentyfikowano fazy w warstwach pośrednich i powłoce. Tą identyfikację potwierdzono techniką X-ray oraz analizą mikrostruktury TEM. Ustalono, że tlenki oraz AlNiO fazy powstały w procesie DGS po nadtopieniu i utlenieniu cząstek Al, zaś w nie nadtopionej części ziaren zaobserwowano drobnoziarnistą budowę. W powłoce zidentyfikowano metodą X-ray fazy: FeAl2O4, Fe3Al oraz FeAl, w warstwie pośredniej Ni(Cr) - chrom i fazę Cr2Ni3w osnowie niklu, zaś w warstwie Ni(Al) czysty nikiel i fazę NiAl. Występowanie faz tlenku glinu i faz AlNiO w pobliżu granic warstw pośrednich powodować może zwiększenie tendencji do delaminacji. Korzystnym byłoby zatem obniżenie ilości aluminium.
Źródło:
Archives of Metallurgy and Materials; 2011, 56, 2; 262-269
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Gaseous Nitriding of Binary Ni-Cr Alloys - Observation and Interpretation of Microstructural Features
Autorzy:
Kodentsov, A.
Cserháti, C.
Powiązania:
https://bibliotekanauki.pl/articles/2125547.pdf
Data publikacji:
2022
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nitridation
Ni-Cr-N system
diffusion
internal precipitation
microstructure
Opis:
Gaseous nitriding of binary Ni-Cr solid-solution alloys was studied at 1125ºC over the range 1 to 6000 bar of N2-pressure. At the specified temperature the nitriding response of the Ni-Cr alloys depends on the Cr-content in the initial alloy and activity (fugacity) of nitrogen at the gas/metal interface. Transition from cubic δ-CrN to hexagonal β-Cr2N precipitation occurs within the reaction zone after nitrogenization at 1125ºC under nitrogen pressure 100-6000 bar when chromium content in the initial alloy is 28 at. % or higher. It was found that a ternary phase, π (Cr12.8Ni7.2N4.0) is formed inside the Ni32Cr alloy upon cooling in nitrogen after nitriding at 1125ºC and 1 bar of N2. Experimental evidence is presented that π-phase is involved in peritectoid relations with β-Cr2N and γ-(Ni-Cr) solid solution. It was also demonstrated that nitriding behaviour of the Ni-Cr alloy can be rationalized using pertinent phase diagram information, but, in some cases, effect of mechanical stresses induced upon the internal precipitation can vitiate this prediction.
Źródło:
Archives of Metallurgy and Materials; 2022, 67, 3; 1007--1020
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Strut Thickness on Room and High Temperature Compressive Properties of Block-Type Ni-Cr-Al Powder Porous Metals
Autorzy:
Kang, B.-H.
Park, M.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/355591.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni-Cr-Al
powder porous metal
strut thickness
high temperature
compressive behavior
Opis:
This study investigated the effect of strut thickness on the room and high temperature compressive properties of block-type Ni-Cr-Al powder porous metals with ~3000 μm pore size manufactured using a new powder process. Two block-type Ni-Cr-Al porous metals with different strut thicknesses were manufactured. The strut thicknesses of two block foams were 340 μm (A) and 383 μm (B), respectively. Room temperature, 500°C, 650°C and 800°C compressive tests were performed. The compressive results identified typical elastic, plateau and densification regions of foam material in all temperature conditions. Regardless of the strut thickness, compressive strength (maximum peak stress) decreased as deformation temperature increased. In all deformation temperature ranges, the compressive strength measured higher in the porous metal with greater strut thickness (B). The high temperature deformation behavior of powder porous metal was confirmed to be affected by the structural factor and microstructural factor of the porous metal. With the findings described above, this study also discussed the high temperature deformation mechanism of the Ni-Cr-Al metal foam based on fracture surfaces after the high temperature compressions.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1329-1334
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cast steels for creep-resistant parts used in heat treatment plants
Autorzy:
Drotlew, A.
Garbiak, M.
Piekarski, B.
Powiązania:
https://bibliotekanauki.pl/articles/380318.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
innowacyjne technologie odlewnicze
innowacyjne materiały odlewnicze
staliwo austenityczne Ni-Cr
obróbka cieplna
innovative foundry technologies
innovative foundry materials
cast Ni-Cr austenitic steel
castings for heat treatment plants
Opis:
Creep-resistant parts of heat treatment furnaces are in most cases made from high-alloyed chromium-nickel and nickel-chromium iron alloys, both cast and wrought. This paper presents the types of casting alloys used for this particular purpose, since the majority of furnace components are made by the casting process. Standards were cited which give symbols of alloy grades used in technical specifications by the domestic industry. It has been indicated that castings made currently are based on a wider spectrum of the creep-resistant alloy grades than the number of alloys covered by the standards. Alloy grades recommended by the technical literature for individual parts of the furnace equipment were given. The recommendations reflect both the type of the technological process used and the technical tasks performed by individual parts of the furnace equipment. Comments were also made on the role of individual alloying elements in shaping the performance properties of castings.
Źródło:
Archives of Foundry Engineering; 2012, 12, 4; 31-38
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
DTA Thermal Analysis of Alloys from Nickel-Rich Part of Ni-Al-Cr System
Autorzy:
Maciąg, T.
Powiązania:
https://bibliotekanauki.pl/articles/351762.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni-Al-Cr system
order-disorder
DTA analysis
Opis:
Thermal analysis allows for determination of temperature specific for the beginning and the end of phase transitions occurring in studied samples. In this paper results obtained from DTA (Differential Thermal Analysis) of alloys of chemical composition referring to nickel-rich part of Ni-Al-Cr system, specifically from section Ni75Al25÷Ni65Cr35 are presented. Those alloys are based on intermetallic phase Ni3 Al. Referring to measurements obtained during heating and cooling, characteristic peaks related to occurrence of phase transition of order-disorder type were noted as well as melting and solidification temperature of alloys was determined. Results of thermal analysis DTA of studied range were compared with results obtained for section Ni75Al25÷Ni75Cr25 and Ni75Al25÷Ni87Cr13, additionally results of measurements performed on high-temperature solution calorimeter were collated. Both methods presented good compatibility.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 981-986
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and abrasive wear resistance of 18Cr-4Ni-2.5Mo cast steel
Autorzy:
Kalandyk, B.
Powiązania:
https://bibliotekanauki.pl/articles/380296.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stal wysokostopowa Cr-Ni
mikrostruktura
wykres CTPc
zużycie ścierne
highly alloyed Cr-Ni cast steel
microstructure
equivalent Cr and Ni
CCT diagrams
abrasive wear
Opis:
An influence of a decreased Cr content on the microstructure of the highly alloyed Cr-Ni cast steel, duplex type, melted under laboratory conditions, was characterized in the paper. The microstructure investigations were performed in the initial state and after the heat treatment (solution annealing) at 1060 C as well as the phase transformation kinetics at continuous cooling was measured. The wear resistance of the investigated cast steel was tested and compared with the 24%Cr-5%Ni-2.5%Mo cast steel. The Cr content decrease, in ferritic-austenitic cast steels (duplex), from 24-26%Cr to 18% leads to the changes of the castings microstructure and eliminating of a brittle \sigma phase. In dependence of the casting cooling rate, apart from ferrite and austenite, also fine martensite precipitates occur in the casting structure. It was shown that the investigated cast steel is characterised by a slightly lower wear resistance than the typical cast steel duplex grades.
Źródło:
Archives of Foundry Engineering; 2012, 12, 4; 81-84
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
DSC Analysis of Order–Disorder Transition in Ni3Al Based Alloys From Ni-Al-Cr System
Analiza DSC przemian typu porządek-nieporządek w stopach na osnowie Ni3Al z układu Ni-Al-Cr
Autorzy:
Maciąg, T.
Rzyman, K.
Przeliorz, R.
Powiązania:
https://bibliotekanauki.pl/articles/356471.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni-Al-Cr system
intermetallic phase Ni3Al
order-disorder
DSC analysis
system Ni-Al-Cr
faza międzymetaliczna Ni3Al
faza nieuporządkowana
analiza DSC
Opis:
Ni-Al-Cr system is significant for industrial alloys based on intermetallic phase Ni3Al, that crystallizes in crystal lattice L12. It is indicated as γ′, contrary to disordered phase γ which occurs with addition of chromium. DSC analysis was performed on alloys of chemical composition from Ni75Al25÷Ni75Cr25 range of Ni-rich part of Ni-Al-Cr system. In addition, few measurements were conducted using DTA method. Based on curves registered, it was possible to identify characteristic temperature during heating and cooling of the sample. It corresponds to existence of phase boundary γ′+γ / γ in examined alloys. Results of thermal analysis were compared with results obtained with other method performed by authors which is solution calorimetric method.
Układ Ni-Al-Cr jest ważnym układem dla przemysłowych stopów na osnowie fazy międzymetalicznej Ni3Al, która krystalizuje w uporządkowanej sieci L12. Oznacza się ją jako γ′ w odróżnieniu od fazy nieuporządkowanej γ, która pojawia się wraz z dodatkiem stopowym chromu. Wykonano serię stopów, których skład chemiczny leży na linii Ni75Al25÷Ni75Cr25 w bogatej w nikiel części układu Ni-Al-Cr i poddano je analizie DSC. Dodatkowo wykonano kilka pomiarów metodą DTA. Na podstawie zarejestrowanych krzywych udało się zidentyfikować charakterystyczne temperatury podczas nagrzewania i studzenia próbki. Odpowiadają one miejscom występowania granicy międzyfazowej γ′+γ / γ w stopach. Wyniki analiz termicznych zestawiono z wynikami innej metody zastosowanej przez autorów tj. kalorymetrycznej metody typu rozpuszczania.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 3A; 1871-1876
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Remelting of the Ni-22Cr-9Mo Alloy on its Microstructural and Electrochemical Properties
Autorzy:
Augustyn-Nadzieja, J.
Łukaszczyk, A.
Loch, J.
Powiązania:
https://bibliotekanauki.pl/articles/351218.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni-Cr-Mo alloys
metal prosthetics restorations
method melted models
artificial saliva solution
corrosion resistance
Opis:
The Ni-Cr-Mo alloys are used as the alternative for the cobalt alloys in the manufacture of metal prosthetic elements, i.e. crowns, bridges and frame prostheses. The article attempts at a materials science characterization of the nickel-based alloy of the commercial name Argeloy N.P Be-Free by Argen. Within the study, examinations were made on the commercial alloy as well as the alloy which was remelted and cast by the los mould (lost wax) method. Observations of the microstructure were performed with the use of optical and electron scanning microscopy. Also, X-ray structural tests were conducted as well as corrosion resistance tests in an artificial saliva solution (pH = 6,7). It was demonstrated that the examined Ni-22Cr-9Mo alloy characterized in a dendritic structure typical of the cast materials. The X-ray qualitative phase analysis revealed the phase γ'(Ni) in both examined materials, as well as the presence of Cr23C6 type carbides and Nb2C, Ta2C (commercial alloy) and NbC, Ta4C0,04 (cast alloy) phases. The effect of the alloy’s remelting and the morphology of the passive layer on the corrosion resistance of the Ni-Cr-Mo alloy was examined. The results of the electrochemical tests show that the process of re-casting only slightly affects the corrosion resistance and the microstructure of the considered alloy. The roles of recasting process and the passive film homogeneity on the corrosion resistance of Ni-Cr-Mo dental alloy were reviewed. The results the electrochemical study show that the dependence of corrosion resistance on the microstructure associated with the recasting process is marginal.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 411-418
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Determination of γ′+γ / γ Phase Boundary in Ni-Al-Cr System Using DTA Thermal Analysis
Autorzy:
Maciąg, T.
Rzyman, K.
Powiązania:
https://bibliotekanauki.pl/articles/354947.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
DTA thermal analysis
order-disorder transition
Ni3Al
Ni-Al-Cr
Opis:
Mechanical properties at elevated temperature, in modern alloys based on intermetallic phase Ni3Al are connected with phase composition, especially with proportion of ordered phase γ′ (L12) and disordered phase γ (A1). In this paper, analysis of one key systems for mentioned alloys - Ni-Al-Cr, is presented. A series of alloys with chemical composition originated from Ni-rich part of Ni-Al-Cr system was prepared. DTA thermal analysis was performed on all samples. Based on shape of obtained curves, characteristic for continuous order-disorder transition, places of course of phase boundaries γ′+γ / γ were determined. Moreover, temperature of melting and freezing of alloys were obtained. Results of DTA analysis concerning phase boundary γ′+γ / γ indicated agreement with results obtained by authors using calorimetric solution method.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 237-240
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wpływ żużli syntetycznych na proces odsiarczania niskostopowego staliwa Cr-Ni-Mo
The Influence of Synthetic Slags on Desulphurisation Process of Low Alloy Cr-Ni-Mo Cast Steel
Autorzy:
Balicki, M.
Sobula, S.
Kalandyk, B.
Powiązania:
https://bibliotekanauki.pl/articles/380598.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
obróbka pozapiecowa stali
żużel syntetyczny
staliwo Cr-Ni-Mo
secondary metallurgy
synthetic slag
Cr-Ni-Mo cast steel
Opis:
W artykule zaprezentowano wyniki obróbki pozapiecowej stali niskostopowej L70H2GNM przeznaczonej na masywne odlewy, pracujące w warunkach ścierania. Obróbka polegała na przedmuchiwaniu argonem stali w kadzi odlewniczej o pojemności 8,5 Mg, przy udziale trzech różnych żużli syntetycznych. Do badań wybrano żużle dostępne na rynku materiałów odlewniczych takie jak: LDSF LT firmy Kerneos, UZRA KP firmy ZM Ropczyce, który dodatkowo zmodyfikowano przez wprowadzenie aluminium. Czas przedmuchiwania kąpieli argonem wynosił 4 minuty dla każdego wytopu. Na podstawie przeprowadzonych badań uzyskano zmiany zawartości siarki w wytapianym staliwie w zależności od zastosowanych żużli syntetycznych. Stwierdzono, że zawartość siarki w staliwie zmniejszyła się po rafinacji w kadzi. Dodatkowo wykazano, że na zawartość siarki w badanym staliwie ma wpływ skład chemiczny zastosowanych żużli syntetycznych.
In this article, the results of secondary metallurgy of L70H2GNM cast steel has been shown. This grade of low alloy cast steel is popular in Poland for heavy castings which works in wear conditions e.g. in coal mills. The ladle refining process was composed of argon stirring in 8.5 Mg bottom pour ladle and treatment with synthetic slags. The three commercial slag mixtures available on casting materials market such as: LDSF of the Kerneos company, UZRA KP and UZRA KP+Al of the ZM Ropczyce company were chosen for examinations. The time of argon blowing through porous plug was 4 minutes for every melt. Experimental results have shown, that sulphur content in steel decreases after refining in ladle. Moreover, desulphurisation ratio during argon stirring have also been influenced by composition of slag mixtures.
Źródło:
Archives of Foundry Engineering; 2015, 15, 4 spec.; 11-14
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Laser Surface Melting on Microstructure of Cold Sprayed Ni20Cr Coatings
Autorzy:
Soboń, D.
Powiązania:
https://bibliotekanauki.pl/articles/2049393.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
cold spraying
Ni20Cr coating
laser modification
mechanical properties
Opis:
In this study, Ni20Cr coatings were obtained by cold spraying on an aluminum alloy 7075 substrate. The obtained coatings were characterized by a uniform microstructure and low porosity. The sprayed coating has the same phase composition as the powder used. Next, the cold sprayed coatings were heat treated using a TRUMPF TLF 6000 TURBO (4 kW) CO2 laser. The laser surface melting of the coatings resulted in the formation of a columnar structure and an improvement in their mechanical properties. The Ni20Cr cold sprayed coatings after additional laser melting showed lower porosity and an increase in microhardness and Young`s modulus.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 3; 853-860
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Corrosion Behavior of Hastelloy® C-2000® Ni-Cr-Mo-Fe Alloys in the Entrained-Flow Coal Gasification Syngas Plants
Autorzy:
Lee, Sungkyu
Kim, Min-Jung
Choi, Nuri
Hwang, Sang Yeon
Chung, Seok-Woo
Lee, Seung-Kong
Yun, Yongseung
Powiązania:
https://bibliotekanauki.pl/articles/352403.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
mixed oxidant corrosion
Hastelloy® C-2000® Ni-Cr-Mo-Fe alloy
coal gasification
high temperature halogencorrosion
hydrated chlorides
Opis:
A mechanistic exposure experiment was performed on the commercially available and welded Ni-Cr-Mo-Fe alloy samples used in the piping materials of the coal gasification pilot plant. Thermodynamic Ellingham-Pourbaix stability diagrams were constructed to provide insight into the mechanism of the observed corrosion behavior. The thermodynamic inference on the corrosion mechanism was supplemented with the morphological, compositional and microstructural analyses of the exposed samples using scanning electron microscopy, X-ray diffraction and energy-dispersive X-ray spectroscopy analyses. X-ray diffraction result revealed stable corrosion products of NiO, MoNi4 and Cr4.6 MoNi2.1 after accumulated total exposure duration of 139 h to the corrosive atmosphere. Scanning electron microscopy and energy-dispersive X-ray spectroscopy positively identified formation of rather continuous and adherent pre-oxidation corrosion products although extensively peeled-off oxides were finally observed as corrosion scales on the post-exposure alloy samples, which were attributed to the chlorination/oxidation into thin (spalled) oxides.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 869-878
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Compressive Properties of Open-Cell Ni-Mo-Cr (Hastelloy) Foams Manufactured by Electrostatic Powder Spraying
Autorzy:
Kang, Tae-Hoon
Kim, Kyu-Sik
Lee, Min-Jeong
Yun, Jung-Yeul
Lee, Kee-Ahn
Powiązania:
https://bibliotekanauki.pl/articles/356501.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metallic foam
electrostatic powder spraying
Ni-Mo-Cr alloy
sintering
compressive property
Opis:
An open-cell Ni-Mo-Cr foam was newly manufactured using electrostatic powder spraying process and its room-temperature compressive properties were investigated in this study. For manufacturing Ni-Mo-Cr foam, Ni-Mo-Cr powders were sprayed on the polyurethane pre-form by electrostatic powder spraying process. And then, Ni-Mo-Cr powder sprayed pre-forms were sintered at 1200°C, 1250°C, and 1300°C, respectively. The relative densities of Ni-Mo-Cr foams were measured at 4 ~ 5%. Room tempera-ture compressive curves of ESP Ni-Mo-Cr foams represented the typical compressive 3-stages (elastic, plateau, densification) of open-cell metallic foam. As a result of observation of deformed specimen, the fracture mode found to be changed from brittle to ductile as sintering temperature increased. Based on these findings, correlations between structural characteristics, microstructure, and compressive deformation behavior were also discussed.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 3; 1081-1086
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
D-gun Sprayed Fe-Al Single Particle Solidification
Krystalizacja pojedynczej cząstki Fe-Al naniesionej metodą detonacyjną
Autorzy:
Wołczyński, W.
Senderowski, C.
Morgiel, J.
Garzeł, G.
Powiązania:
https://bibliotekanauki.pl/articles/352240.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-Al coating
Ni-20Cr interlayer
rapid solidification
D-gun spraying
boron localization
competitive growth of phases
powłoki FeAl
międzywarstwy Ni-20Cr
szybkie krzepnięcie
metoda detonacyjna
lokalizacja boru
proces wzrostu faz
Opis:
Some Fe-Al particles less than 50 μm in diameter were deposited onto the steel substrate by means of the D-gun spraying. A solidification mechanism of an individual particle is described. The particle subjected to the description contained nominally 63 at.% Al. The description was preceded by the TEM / SAED analysis of both the Fe-Al coating and Ni-20Cr interlayer. The whole number of the analyzed particles was partially melted during the deposition. The solidification products like: amorphous phase sub-layer, oscillatory sub-layer which contains two types lamellae distributed alternately and typically non-equilibrium phase sub-layer were revealed. In the micro scale, solidification was considered as a process which occurred in two directions: towards the substrate and towards the non-melted particle part. Both solidification processes underwent the positive thermal gradients. The boron addition was localized within the eutectic precipitates pushed and then rejected by the solid/liquid interface of the solidifying non-equilibrium phase. The proposed model is a general one and therefore can be applied to other systems ;description.
Cząstki proszku Fe-Al niniejsze niż 50 μm w średnicy zostały osadzone detonacyjnie na podłożu stalowym. Opisuje się mechanizm krystalizacji pojedynczej cząstki. Cząstki poddane opisowi zawierały nominalnie 63 aL% Al. Opis poprzedzono badaniami struktury metodą TEM / SAED dotyczącymi zarówno powłoki Fe-Al jak i między warstwy Ni-20Cr. Wszystkie analizowane cząstki były częściowo nadtopione podczas osadzania. Zidentyfikowano produkty krystalizacji takie jak: podwarstwę amorficzną, podwarstwę oscylacyjną zawierającą periodycznie ułożone pły tki dwu faz oraz podwarstwę zawierającą fazę typowo nierównowagową. W mikroskali proces wzrostu faz jest analizowany jako zachodzący w dwu kierunkach: w stronę podłoża i w stronę niestopionej części cząstki. Obydwa procesy wzrostu zachodziły w obecności dodatniego gradientu temperatury. Bor dodany do powłoki został zlokalizowany w eutektyce odepchniętej przez front krystalizacji fazy typowo nierównowagowej. Proponowany model ma charakter ogólny i może być zastosowany do opisu innych systemów.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 1; 211-220
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Experimental and Thermodynamic Study of Selected in-Situ Composites from the Fe-Cr-Ni-Mo-C System
Autorzy:
Wieczerzak, K.
Bala, P.
Dziurka, R.
Stepien, M.
Tokarski, T.
Cios, G.
Gorecki, K.
Powiązania:
https://bibliotekanauki.pl/articles/352051.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-Cr-Ni-Mo-C
in-situ composites
intermetallic compounds
dilatometry
microstructure
Opis:
The aim of the study was to synthesize and characterize the selected in-situ composites from the Fe-Cr-Ni-Mo-C system, additionally strengthened by intermetallic compounds. The project of the alloys was supported by thermodynamic simulations using Calculation of Phase Diagram approach via Thermo-Calc. Selected alloys were synthesized in an arc furnace in a high purity argon atmosphere using a suction casting unit. The studies involved a range of experimental techniques to characterize the alloys in the as-cast state, including optical emission spectrometry, light microscopy, scanning electron microscopy, electron microprobe analysis, X-ray diffraction and microhardness tests. These experimental studies were compared with the Thermo-Calc data and high resolution dilatometry. The results of investigations presented in this paper showed that there is a possibility to introduce intermetallic compounds, such as χ and σ, through modification of the chemical composition of the alloy with respect to Nieq and Creq. It was found that the place of intermetallic compounds precipitation strongly depends on matrix nature. Results presented in this paper may be successfully used to build a systematic knowledge about the group of alloys with a high volume fraction of complex carbides, and high physicochemical properties, additionally strengthened by intermetallic compounds.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2B; 1241-1247
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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