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    Wyświetlanie 1-13 z 13
    Tytuł:
    Fabrication Of Porous Ti By Thermal Decomposition And Sintering Of PMMA/TiH2 Powder Compact
    Wytwarzanie porowatego tytanu przez rozkład termiczny i spiekanie wyprasek PMMA/TiH2
    Autorzy:
    Jeon, K. Ch.
    Kim, Y. D.
    Suk, M.-J.
    Oh, S.-T.
    Powiązania:
    https://bibliotekanauki.pl/articles/352341.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    porous Ti
    PMMA powders
    thermal decomposition of TiH2
    pore structure
    porowaty tytan
    PMMA
    rozkład termiczny
    struktura porów
    Opis:
    Porous Ti with controlled pore structure was fabricated by thermal decomposition and sintering process using TiH2 powders and Polymethylmethacrylates (PMMA) beads as pore forming agent. The beads sizes of 8 and 50 μm were used as a template for fabricating the porous Ti. The TiH2 powder compacts with 20 and 70 vol% PMMA were prepared by uniaxial pressing and sintered for 2 h at 1100°C. TGA analysis revealed that the PMMA and TiH2 were thermally decomposed at about 400°C forming pores and at about 600°C into metallic Ti phase. The porosity increased with increase in the amount of PMMA addition. Also, the microstructure observation showed that the pore size and shape were strongly dependent on the PMMA shapes.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1375-1377
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Double Step Sintering Behavior Of 316L Nanoparticle Dispersed Micro-Sphere Powder
    Dwuetapowe spiekanie mikrosferycznych nanocząstek proszku 316L
    Autorzy:
    Jeon, B.
    Sohn, S. H.
    Lee, W.
    Han, C.
    Kim, Y. D.
    Choi, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/355221.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    316L stainless steel
    nanoparticle dispersed micro-sphere
    pulse wire explosion
    sintering
    stal nierdzewna 316L
    spiekanie dwuetapowe
    mikrosferyczne nanocząstki
    Opis:
    316L stainless steel is a well-established engineering material and lots of components are fabricated by either ingot metallurgy or powder metallurgy. From the viewpoints of material properties and process versatility, powder metallurgy has been widely applied in industries. Generally, stainless steel powders are prepared by atomization processes and powder characteristics, compaction ability, and sinterability are quite different according to the powder preparation process. In the present study, a nanoparticle dispersed micro-sphere powder is synthesized by pulse wire explosion of 316L stainless steel wire in order to facilitate compaction ability and sintering ability. Nanoparticles which are deposited on the surface of micro-powder are advantageous for a rigid die compaction while spherical micro-powder is not to be compacted. Additionally, double step sintering behavior is observed for the powder in the dilatometry of cylindrical compact body. Earlier shrinkage peak comes from the sintering of nanoparticle and later one results from the micro-powder sintering. Microstructure as well as phase composition of the sintered body is investigated.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1155-1158
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Aluminum Nitride Formation From Aluminum Oxide/Phenol Resin Solid-Gel Mixture By Carbothermal Reduction Nitridation Method
    Wytwarzanie azotku aluminium z żelowej mieszaniny tlenku aluminium z żywicą fenolową metodą azotowania podczas carbotermicznej redukcji
    Autorzy:
    Mylinh, D. T.
    Yoon, D. H.
    Kim, C.-Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/356779.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    aluminum nitride
    powder
    carbothermal reduction
    nitridation
    solid-gel mixture
    azotek aluminium
    proszek
    redukcja karbotermiczna
    azotowanie
    żelowa mieszanina
    Opis:
    Hexagonal and cubic crystalline aluminum nitride (AlN) particles were successfully synthesized using phenol resin and alpha aluminum oxide (α-Al2O3) as precursors through new solid-gel mixture and carbothermal reduction nitridaton (CRN) process with molar ratio of C/Al2O3 = 3. The effect of reaction temperature on the decomposition of phenol resin and synthesis of hexagonal and cubic AlN were investigated and the reaction mechanism was also discussed. The results showed that α-Al2O3 powder in homogeneous solid-gel precursor was easily nitrided to yield AlN powder during the carbothermal reduction nitridation process. The reaction temperature needed for a complete conversion for the precursor was about 1700°C, which much lower than that when using α-Al2O3 and carbon black as starting materials. To our knowledge, phenol resin is the first time to be used for synthesizing AlN powder via carbothermal reduction and nitridation method, which would be an efficient, economical, cheap assistant reagent for large scale synthesis of AlN powder.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1551-1555
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects of Grain Boundary Morphologies on Stress Corrosion Cracking of Alloy 600
    Autorzy:
    Kim, H. P.
    Choi, M. J.
    Kim, S. W.
    Kim, D. J.
    Lim, Y. S.
    Hwang, S. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/352569.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    alloy 600
    NaOH
    stress corrosion cracking
    grain boundary morphologies
    Opis:
    Effects of grain boundary morphologies on stress corrosion cracking (SCC) of Alloy 600 have been studied in 40% NaOH at 315°C using C-ring specimens. The configuration of the grain boundary and the intergranular carbide density were controlled by heat treatment. SCC tests were performed at +150 mV above the corrosion potential. The specimen with a serrated grain boundary showed higher SCC resistance than that with a straight grain boundary. This appears to be caused by the fact that the specimen with the serrated grain boundary has longer SCC path. SCC resistance also increased with intergranular carbide density probably due to enhanced relaxation of stress at intergranular carbide.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1415-1419
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of Mo-Si-B Intermetallic Compound Powders Under Different Heat Treatment Conditions
    Autorzy:
    Park, J. H.
    Lee, S.
    Kim, D.
    Kim, Y.
    Yang, S. H.
    Lee, S. H.
    Powiązania:
    https://bibliotekanauki.pl/articles/353369.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Mo-Si-B alloys
    intermetallic compounds
    reitveld refinement
    T2 phase
    A15 phase
    Opis:
    In this research, we investigated the effects of reduction atmospheres on the creation of the Mo-Si-B intermetallic compounds (IMC) during the heat treatments. For outstanding anti-oxidation and elevated mechanical strength at the ultrahigh temperature, we fabricated the uniformly dispersed IMC powders such as Mo5SiB2 (T2) and Mo3Si (A15) phases using the two steps of chemical reactions. Especially, in the second procedure, we studied the influence of the atmospheres (e.g. vacuum, argon, and hydrogen) on the synthesis of IMCs during the reduction. Furthermore, the newly produced IMCs were observed by SEM, XRD, and EDS to identify the phase of the compounds. We also calculated an amount of IMCs in the reduced powders depending on the atmosphere using the Reitveld refinement method. Consequently, it is found that hydrogen atmosphere was suitable for fabrication of IMC without other IMC phases.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1509-1512
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Surface Treatment And Modification Of Graphene Using Organosilane And Its Thermal Stability
    Obróbka powierzchniowa i modyfikacja grafenu przy użyciu organosilanu i jego stabilność termiczna
    Autorzy:
    Kim, D.-S.
    Dhand, V.
    Rhee, K.-Y.
    Park, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/354056.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    graphite
    thermal properties
    Raman spectroscopy
    surface treatment
    3-APTES
    grafit
    właściwości termiczne
    spektroskopia Ramana
    obróbka powierzchniowa
    Opis:
    In this study, graphene was functionalized via acid oxidation in the presence of a mixture of concentrated sulfuric acid and nitric acid. The oxidized graphene was silanized using the coupling agent, 3-aminopropyltriethoxsilane, resulting in functionalized graphene. The oxidized graphene and functionalized graphene were characterized by X-Ray diffraction, Fourier transform infrared spectroscopy, High-resolution micro Raman spectroscopy, thermogravimetric analysis, and atomic force microscopy to confirm the presence of functional moieties on the graphene surface. Thermal studies also demonstrate that the functionalized material is thermally stable up to higher temperatures.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1387-1391
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects Of Environmental Factors On The Dispersion Behavior Of Iron Oxide In Aqueous Solutions With Poly Acrylic Acid
    Wpływ parametrów charakteryzujących wodne roztwory poli(kwasu akrylowego) na dyspersję tlenku żelaza
    Autorzy:
    Lee, E.-H.
    Kim, K.-M.
    Maeng, W.-Y.
    Hur, D.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/354513.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    polyacrylic acid
    dispersion stability
    magnetite
    nanoparticles
    suspension
    poli(kwas akrylowy)
    stabilność dyspersji
    magnetyt
    nanocząstki
    zawiesina
    Opis:
    After preparing aqueous suspensions from magnetite particles with a poly-acrylic acid, we investigated the effects of several experimental parameters. We characterized the stability of the suspensions using visual inspection, sedimentation, adsorption, and thermal stability of the dispersant. The dispersion stability is affected by the solution pH, the concentrations of magnetite particles, the molecular weight, the concentration of the dispersants, and the temperature. The stability of the suspensions increased as the concentration of the dispersant and the temperature increased. In terms of the molecular weights of the dispersant, the suspensions with dispersant of low-molecular weight (1800) were more stable than those of high-molecular weight (250000) at room temperature. However, at high temperature the suspensions with high-molecular weight showed stability. The adsorption efficiency of the dispersant was very low. The dispersant of high-molecular weight showed a higher thermal integrity than that of low-molecular weight. From this work, we obtained the optimum conditions for stable aqueous suspensions of magnetite particles.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1561-1564
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Manufacturing and Macroscopic Properties of Y2O3 Coating Layer on Ceramic (AlN) Substrate Fabricated by Aerosol Deposition
    Autorzy:
    Wi, D.-Y.
    Ham, G.-S.
    Kim, S.-H.
    Lee, K.-A.
    Powiązania:
    https://bibliotekanauki.pl/articles/353052.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    aerosol deposition
    Y2O3 coating layer
    AlN matrix
    nano indentation
    Opis:
    This study attempted to manufacture an Y2O3 ceramic coating layer on a ceramic (AlN) substrate using aerosol deposition (AD) and investigated its macroscopic properties. Pure Y2O3 powder with a polygonal shape and average size of 5.0 μm was used as initial feedstock. Using aerosol deposition with suitable process conditions, an Y2O3 coating layer was successfully fabricated on aluminum nitride (AIN). The thickness of the manufactured coating layer was approximately 10 mm. The coating layer consisted of Y2O3 phase identical to that in the initial powder, and no additional oxides were identified. In regard to the roughness of the Y2O3 coating layer, the average roughness (Ra) measured 1.32 μm, indicating that the surface roughness was relatively even compared to the initial powder size (5 μm). Mechanical properties of the Y2O3 coating layer were measured using nano indentation equipment, and the indentation modulus of the Y2O3 coating layer fabricated by aerosol deposition measured 136.5 GPa. The interface of the coating layer was observed using TEM, and the deposition mechanism of the Y2O3 coating layer manufactured by aerosol deposition was also discussed.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 3; 1463-1466
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Oxidation Behavior of Steel with Cr Content and Water Flow Rate
    Autorzy:
    Kim, D.-J.
    Kim, K. M.
    Shin, J. H.
    Cheong, Y. M.
    Lee, E. H.
    Lee, G. G.
    Kim, S. W.
    Kim, H. P.
    Choi, M. J.
    Lim, Y. S.
    Hwang, S. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/351548.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    steel
    flow accelerated corrosion
    Cr content
    flow rate
    surface oxides
    Opis:
    Fast water flow facilitates ferrous ion transport leading to flow accelerated corrosion (FAC) of carbon steel and the possibility of a large accident through a failure of a secondary pipe in a nuclear power plant. Ion transport is directly linked to oxide properties such as the thickness, chemical composition and porosity. This work deals with a precise observation of the cross section of the corroded specimen focusing on an oxide passivity and its thickness using SEM (scanning electron microscope) and TEM (transmission electron microscope) as well as an apparent weight loss and a surface observation for the specimens corroded using a rotating cylindrical electrode autoclave system in pure water of pH 7 at 150°C having dissolved oxygen below 1 ppb within a flow rate range of 0 to 10 m/s. The Cr content in steel was changed from 0.02 to 2.4 wt%. Increasing the Cr content in the alloy, the FAC rate and oxide thickness decreased. The oxide porosity tends to decrease with the Cr content and immersion time owing to the development of Cr containing oxide. The oxidation behavior is not changed with the immersion time.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1383-1387
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Recovery Of Electrodic Powder From Spent Nickel-Metal Hydride Batteries (NiMH)
    Odzyskiwanie proszku elektrodowego ze zużytych akumulatorów niklowo-wodorkowych (NiMH)
    Autorzy:
    Shin, S. M.
    Shin, D. J.
    Jung, G. J.
    Kim, Y. H.
    Wang, J. P.
    Powiązania:
    https://bibliotekanauki.pl/articles/356110.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    nickel-metal hybride (NiMH)
    electrodic powder
    nickel
    rare earth elements (REE)
    thermal treatment
    akumulator niklowo-wodorkowy
    proszek elektrodowy
    nikiel
    pierwiastki ziem rzadkich
    obróbka termiczna
    Opis:
    This study was focused on recycling process newly proposed to recover electrodic powder enriched in nickel (Ni) and rare earth elements (La and Ce) from spent nickel-metal hydride batteries (NiMH). In addition, this new process was designed to prevent explosion of batteries during thermal treatment under inert atmosphere. Spent nickel metal hydride batteries were heated over range of 300°C to 600°C for 2 hours and each component was completely separated inside reactor after experiment. Electrodic powder was successfully recovered from bulk components containing several pieces of metals through sieving operation. The electrodic powder obtained was examined by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDX) and image of the powder was taken by scanning electron microscopy (SEM). It was finally found that nickel and rare earth elements were mainly recovered to about 45 wt.% and 12 wt.% in electrodic powder, respectively.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1139-1143
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Allometric scaling of marbofloxacin pharmacokinetics: a retrospective analysis
    Autorzy:
    Yohannes, S.
    Hossain, M.A.
    Kim, J.Y.
    Lee, S.J.
    Kwak, D.M.
    Suh, J.W.
    Park, S.C.
    Powiązania:
    https://bibliotekanauki.pl/articles/31939.pdf
    Data publikacji:
    2014
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Opis:
    The association between physiologically dependent pharmacokinetic parameters (CLB, T1/2β, Vdss) of marbofloxacin and body weight was studied in eight animal species based on allometric equation Y = aWb, where ‘Y’ is the pharmacokinetic parameter, ‘W’ is body weight, ‘a’ is allometric coefficient (intercept) and ‘b’ is the exponent that describes relation between pharmacokinetic parameter and body weight. The body clearance of marbofloxacin has shown significant (P<0.0001) relation with size (Bwt) in various animal species. However, half-life and volume of distribution were not in association with body weight. Although half-life and volume of distribution were not in a good correlation with body weight, statistically significant association between the body clearance and body weight suggests validity of allometric scaling for predicting pharmacokinetic parameters of marbofloxacin in animal species that have not been studied yet. However further study considering large sample size and other parameters influencing pharmacokinetics of marbofloxacin is recommended.
    Źródło:
    Polish Journal of Veterinary Sciences; 2014, 17, 1
    1505-1773
    Pojawia się w:
    Polish Journal of Veterinary Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Carbon Co-Deposition During Gas Reduction of Water-Atomized Fe-Cr-Mo Powder
    Autorzy:
    Ali, B.
    Choi, S. H.
    Seo, S. J.
    Maeng, D. Y.
    Lee, C. G.
    Kim, T. S.
    Park, K. T.
    Powiązania:
    https://bibliotekanauki.pl/articles/352709.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    water atomization
    Fe-based powder
    oxide reduction
    powder metallurgy
    sinter-hardening alloys
    Opis:
    The water atomization of iron powder with a composition of Fe-3Cr-0.5Mo (wt.%) at 1600°C and 150 bar creates an oxide layer, which in this study was reduced using a mixture of methane (CH4) and argon (Ar) gas. The lowest oxygen content was achieved with a 100 cc/min flow rate of CH4, but this also resulted in a co-deposition of carbon due to the cracking of CH4. This carbon can be used directly to create high-quality, sinter hardenable steel, thereby eliminating the need for an additional mixing step prior to sintering. An exponential relationship was found to exist between the CH4 gas flow rate and carbon content of the powder, meaning that its composition can be easily controlled to suit a variety of different applications.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1119-1124
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Study On The Metal Carbide Composite Diffusion Bonding For Mechanical Seal
    Badanie łączenia dyfuzyjnego kompozytu metal węglik na mechaniczne uszczelnienie
    Autorzy:
    Kim, D.-K.
    Shon, I.-J.
    Song, J.
    Ryu, W.-J.
    Shin, H.-Ch.
    Kwon, E.-Y.
    Shin, H.
    Kang, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/356399.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    diffusion bonding
    nanostructures
    mechanical seal
    hard metal
    mechanical properties
    łączenie
    nanostruktura
    uszczelnienie mechaniczne
    twardy metal
    właściwości mechaniczne
    Opis:
    Mechanical Seal use highly efficient alternative water having a great quantity of an aqueous solution and has an advantage no corrosion brine. Metal Carbide composites have been investigated as potential materials for high temperature structural applications and for application in the processing industry. The existing Mechanical seal material is a highly expensive carbide alloy, and it is difficult to take a price advantage. Therefore the study of replacing body area with inexpensive steel material excluding O-ring and contact area which demands high characteristics is needed. The development of WC-Ni base carbide alloy optimal bonding composition technique was accomplished in this study. To check out the influence of bonding temperature and time, bonding characteristics of sintering temperature was experimented. The bonding statuses of this test specimen were excellent. The hardness of specimen and bonding rate were measured using ultrasound equipment. In this work, Powder of WC (involved VC, Cr), Co and Mo2C mixed by attrition milling for 24hours. Nanostructured WC-27.6wt.%Ni-1.5wt.%Si-0.11wt.%VC-1.1wt.%B4C composite were fabricated at 1190°C by high temperature vacuum furnace. To check out the influence of bonding temperature and time, bonding characteristics of sintering temperature was experimented. Its relative density was about 99.7%. The mechanical properties (hardness and fracture toughness) were 87.2 HRA and 4.2 M·Pam1/2, respectively. The bonding status of this test specimen was excellent and the thickness of bonding layer was 20 ~30§ at 1050 and 1060°C bonding temperature.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1479-1483
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-13 z 13

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