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    Wyświetlanie 1-13 z 13
    Tytuł:
    A Modified Penetration Model for Copper-Tungsten Shaped Charge Jets with Non-uniform Density Distribution
    Autorzy:
    Elshenawy, T.
    Elbeih, A.
    Li, Q. M.
    Powiązania:
    https://bibliotekanauki.pl/articles/358894.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    shaped charge
    jet penetration
    virtual origin
    non-uniform density distribution
    Opis:
    The penetration of a shaped charge jet with non-uniform density distribution was studied. The virtual origin model, which assumes a constant jet density, was modified to include the situation where the jet density deficit/reduction of an un-sintered copper-tungsten powder jet causes a non-uniform jet density distribution. A relation between the relative density ratio and the normalised jet velocity is proposed, based on which an analytical solution of the modified virtual origin model is obtained. The validity of the modified virtual origin model was demonstrated by its largely improved prediction in comparison with experimental and numerical results. It showed that the density reduction term reduces the penetration depth by 16.58% for an un-sintered copper-tungsten powder jet.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 927-943
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Coated Ammonium Dinitramide on the Properties of Nitrate-ester Plasticized Polyether Solid Rocket Propellants
    Autorzy:
    Pang, W. Q.
    Li, J. Q.
    DeLuca, L. T.
    Ke, W.
    Fu, X. L.
    Zhong, F. X.
    Li, H.
    Ji, Y. P.
    Powiązania:
    https://bibliotekanauki.pl/articles/358292.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    energetic materials
    NEPE composite solid propellants
    ADN
    hazardous properties
    combustion characteristics
    Opis:
    Several industrial and research types of nitrate-ester plasticized polyether (NEPE) solid propellants were experimentally analyzed. In general, their compositions differed in the mass fraction of ammonium dinitramide (ADN), which was used as a promising highly energetic filler, as an alternative to ammonium perchlorate (AP). ADN exhibits high performance, low signature and non-polluting characteristics. The propellant composition without ADN, but with AP, was used as the reference. The microstructure and granularity distribution of the uncoated and coated ADN particles were experimentally analyzed. It was found that uncoated ADN particles exhibited irregular shape, while the ADN particles after coating are spherical. Because of their irregular shape, uncoated ADN particles caused inferior processability of the propellant slurry when added to the propellant formulation. Consequently, the NEPE propellants with coated ADN were studied in further detail. The rheological properties, energetic properties, mechanical sensitivities and combustion properties (burning rate and pressure exponent) of the NEPE propellants with coated ADN were studied and compared with the reference NEPE propellant. The addition of ADN particles to the propellant formulations increased the standard theoretical specific impulse and heat of explosion of the propellants, while decreasing the density. The propellants containing ADN particles were much more sensitive to impact and friction compared to the reference sample. Moreover, increasing the ADN mass fraction in the propellant formulation can significantly affect the combustion behaviour and increase the burning rate and pressure exponent compared to of the reference formulation. However it appears that ADN is a very promising candidate as a new energetic material in compositions of NEPE propellants, although several important questions concerning ADN’s suitability, especially in the context of its sensitivity to friction and impact, remain to be answered.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 4; 590-609
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization and Application of Al/Ni Reactive Multilayers in Exploding Foils
    Autorzy:
    Wang, T.
    Zeng, Q.
    Li, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/358516.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    energetic material
    Al/Ni reactive multilayer foils
    bilayer thickness
    exploding foil initiator
    Opis:
    A self-propagating reaction achieved by initiating an Al/Ni reactive multilayer foil can generate significant heat. The interdiffusion rate of the reactants plays an important role in the foils properties and is mainly affected by premixing and the bilayer thickness. The present research aims to characterize Al/Ni multilayer foils and to investigate their influence on an exploding foil initiator. Samples with different bilayer thicknesses were fabricated by magnetron sputtering. The heat released and the flame velocity were characterized. Foils with a stored energy of about 1100 J/g were prepared and the heat released revealed the existence of a 4 nm premixing layer. The analytical model proposed by Mann was employed to match the measured flame velocities; the fitted model showed good agreement with the experimental results. To make a comparison, Cu and Al/Ni exploding foils with the same bridge size were fabricated and tested in the identical discharge circuit. The results showed that the energy deposition ratio of an Al/Ni foil was 67-69%, while the value for Cu was only 39-45%, which indicated that Al/Ni multilayers could effectively increase the energy utilization of an initiator. Larger average flyer velocities were also observed with the Al/Ni initiators.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 3; 547-558
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Compatibility Study of 2,6-Diamino-3,5-dinitropyridine-1-oxide with Some Energetic Materials
    Autorzy:
    Li, X.
    Wang, B.-L,
    Lin, Q.-H.
    Powiązania:
    https://bibliotekanauki.pl/articles/358871.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    compatibility
    energetic materials
    ANPyO
    Opis:
    For the application of 2,6-diamino-3,5-dinitropyridine-1-oxide (ANPyO) in composite explosives, the compatibility of ANPyO with some energetic materials was studied by the use of differential scanning calorimetry (DSC), where the energetic materials were cyclotrimethylenetrinitramine (RDX), cyclotetramethylenetetranitramine (HMX), 3,4-dinitrofurazanfuroxan (DNTF), hexanitrohexazaisowurtzitane (CL-20), 2,4,6-trinitrotoluene (TNT), 2,4,6-triamino-1,3,5-trinitrobenzene (TATB), 3-nitro-1,2,4-triazol-5-one (NTO), 2,6-diamino-3,5-dinitropyrazine-1-oxide (LLM-105), 5-amino-1H-tetrazole nitrate (5-ATEZN), ammonium perchlorate (AP), potassium perchlorate (KP), aluminum powder (Al), boron powder (B), magnesium hydride (MgH2) and magnesium borohydride (Mg(BH4)2). The results showed that the binary systems of ANPyO/CL-20, ANPyO/NTO, ANPyO/5-ATEZN, ANPyO/Al, ANPyO/B, ANPyO/MgH2 and ANPyO/Mg(BH4)2 are compatible, and that the systems of ANPyO with RDX, LLM-105, HMX, AP and KP are sensitive, and with DNTF, TNT and TATB are incompatible.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 978-988
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Measurement of the Heat of Reaction of Polytetrafluoroethylene/Aluminum Composites Based on Laser Initiation
    Autorzy:
    Li, S.
    Wu, Y.
    Lin, Q.
    Huang, C.
    Yang, S.
    Li, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358195.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    reactive materials
    PTFE/Al composites
    heat of reaction
    laser initiation
    Opis:
    Polytetrafluoroethylene/aluminum (PTFE/Al) composites are reactive materials which can release energy due to exothermic chemical reactions initiated under shock loading conditions. In order to accurately measure the potential maximum heat of reaction of PTFE/Al composites in an inert atmosphere, we propose in this paper a heat of reaction measurement system based on laser initiation. Our results show that the measurement system successfully initiates the chemical reaction between PTFE and Al in an argon atmosphere. The comparison between theoretical calculations and experimental data demonstrates that our measurement method is highly accurate and exhibits excellent consistency. Thus, the heat of reaction measurement system based on laser initiation is applicable for measuring the heat of reaction of PTFE/Al composites and also other complicated reactive materials.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 3; 534-546
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of Nano- and Micron- Sized Spheres of CL-20 by Electrospray
    Autorzy:
    Yan, S.
    Li, M.
    Sun, L.
    Jiao, Q.
    Huang, R.
    Powiązania:
    https://bibliotekanauki.pl/articles/358652.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    energetic materials
    explosives
    CL-20
    electrospray
    spherical particles
    Opis:
    The application of hexanitrohexaazaisowurtzitane (CL-20) in energetic materials will be expanded by its use as superfine particles. A method of fabricating nano- and micron-sized spheres of CL-20 by using electrospray is discussed. The effects of the precursor solution and the experimental conditions on the morphology and the crystal phase of the CL-20 particles are introduced. A variety of solvents was used to dissolve raw CL-20 for the preparation of the precursor solution with different CL-20 contents. The conductivity and viscosity of the precursor solutions were tested before the electrospray process. The electrostatic parameters were adjusted by changing the voltage and the distance between the nozzle and the plate. The morphology, crystal phase, mechanical sensitivity, density, and thermal stability of the raw CL-20 and the as-sprayed CL-20 samples were determined using scanning electron microscopy, X-ray diffraction, and differential scanning calorimetry (DSC). Furthermore, the density and the mechanical sensitivity were tested for the raw and the as-sprayed CL-20. DSC tests were conducted to compare the thermal stability and reactivity of the samples.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 4; 572-589
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Reinforcement of the TNT System by a Newly-designed GAP-based Polyurethane-Urea: a Molecular Simulation Investigation
    Autorzy:
    Qian, W.
    Shu, Y.
    Ma, Q.
    Li, H.
    Wang, S.
    Chen, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358512.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    TNT
    GAP
    polyurethane-urea
    inter-molecular interaction
    mechanical properties
    Opis:
    A glycidyl azide (GAP)-based polyurethane-urea (PUU) modifier used in the 1,3,5-trinitrotoluene (TNT)-based composite explosive was investigated by molecular simulation. Inter-molecular interactions were investigated using quantum chemistry calculation on the dimer of TNT and GAP-PUU, and attractive forces were found between the two molecules. The cohesive energy densities and the solubility parameters were obtained through molecular dynamics simulations combined with thermodynamic calculations on the TNT and GAP-PUU amorphous cell models, and the miscibility of the modifier in molten TNT was predicted to be good. The interaction energies and the mechanical properties were then obtained by molecular simulations and mechanical calculations on the solid-phase models of the GAP-PUU with TNT along three crystalline directions, and an improvement in the mechanical properties was predicted.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 2; 411-426
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A Facile Synthesis of 3,3'-Dinitro-5,5'-diamino-bi-1,2,4-triazole and a Study of Its Thermal Decomposition
    Autorzy:
    Ma, Q.
    Lu, H.
    Qu, Y.
    Liao, L.
    Li, J.
    Fan, G.
    Chen, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/358272.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    3,3’-dinitro-5,5’-diamino-bi-1,2,4-triazole
    facile synthesis
    DSC-TG
    RSFTIR
    TG-IR
    thermolysis
    Opis:
    3,3’-Dinitro-5,5’-diamino-bi-1,2,4-triazole (DABNT) was synthesized by a facile method and its crystalline density was determined as 1.839 g·cm−3 at 293(2) K by X-ray diffraction. Its thermal decomposition kinetics and mechanism were studied by means of differential scanning calorimetry-thermogravimetry (DCS-TG), in situ thermolysis by rapid-scan Fourier transform infrared spectroscopy (RSFTIR) and simultaneous TG-IR technology. The results showed that the apparent activation energies obtained by the Kissinger, Ozawa and Starink methods were 122.9 kJ·mol−1, 123.2 kJ·mol−1 and 123.5 kJ·mol−1, respectively. The thermodynamic parameters of ΔS≠, ΔH≠ and ΔG≠ were −37.5 J·K−1·mol−1, 118.4 kJ·mol−1 and 138.7 kJ·mol−1, respectively. The decomposition reaction process of DABNT starts with the transformation from a primary amine to a secondary amine and then the loss of one nitro-group from the DABNT structure. Gaseous products, such as N2O and H2O, were detected from decomposition in the range of 50-300 °C. Density functional theory (DFT) calculations were further employed to illustrate the decomposition mechanism. The above-mentioned information on the synthesis and thermal behaviour is quite useful for the scale-up and evaluation of the thermal safety of DABNT.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 2; 281-295
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Analysis of the Thermal Behaviour of CL-20, Potassium Perchlorate, Lithium Perchlorate and Their Admixtures by DSC and TG
    Autorzy:
    Zhang, J.-J.
    Guo, X.-J.
    Jiao, Q.-J.
    Zhang, H.-L.
    Li, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/358770.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    CL-20
    potassium perchlorate
    lithium perchlorate
    thermal stability
    phase transition
    Opis:
    The thermal decomposition characteristics of CL-20, potassium perchlorate (KP), lithium perchlorate (LP), a CL-20/KP mixture, and a CL-20/LP mixture were studied using thermogravimetry-differential scanning calorimetry (TG-DSC). The DSC curves for KP exhibited three endothermic peaks and one exothermic peak. The first two endothermic peaks correspond to the rhombic-cubic transition and the fusion of KP, respectively, the third indicates the fusion of KCl, while the exothermic peak is attributed to the decomposition of KP. The DSC curves obtained from LP showed four endothermic peaks and one exothermic peak. The first two endothermic peaks indicate the loss of adsorbed water and water of crystallization, while the third and fourth are associated with the fusion of LP and LiCl, respectively; the exothermic peak is due to the decomposition of LP. The presence of KP had little effect on the thermal decomposition of CL-20 while the addition of LP increased the temperature at which CL-20 exhibits an exothermic peak. In addition, the thermal decomposition of LP appeared to be catalyzed by the presence of CL-20.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 1; 115-130
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis, Structure and Energetic Properties of a Catenated N6, Polynitro Compound: 1,1’-Azobis(3,5-dinitropyrazole)
    Autorzy:
    Li, Y.-N.
    Shu, Y.-J.
    Wang, Y.-L.
    Wang, B.-Z.
    Zhang, S.-Y.
    Bi, F.-Q.
    Powiązania:
    https://bibliotekanauki.pl/articles/358573.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    energetic compound
    1,1’-azobis(3,5-dinitropyrazole)
    synthesis
    energetic properties
    Opis:
    A nitrogen-rich, polynitro energetic compound with an N,N-azo linkage, 1,1’-azobis(3,5-dinitropyrazole) (ABDNP), has been synthesized by an oxidative coupling reaction of 1-amino-3,5-dinitropyrazole with different oxidizing agents. The target compound was characterized by IR spectroscopy, 1H and 13C nuclear magnetic resonance spectroscopy, elemental analysis, mass spectra, X-ray diffraction and differential scanning calorimetry (DSC). The DSC results show that 1,1’-azobis(3,5-dinitropyrazole) decomposes at a relatively high onset temperature (202.9 °C), which indicates that 1,1’-azobis(3,5-dinitropyrazole) has acceptable thermal stability. The energetic properties were obtained, with a measured density and heat of formation matched by theoretically computed values based on the B3LYP method.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 2; 321-335
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Microstructural Evolution in HMX Based Plastic-bonded Explosive During Heating and Cooling Process: an in situ Small-angle Scattering Study
    Autorzy:
    Yan, G.
    Tian, Q.
    Liu, J.
    Fan, Z.
    Sun, G.
    Zhang, C.
    Wang, Y.
    Chen, B.
    Gong, J.
    Zhou, X.
    Yang, Z.
    Nie, F.
    Li, J.
    Li, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/358618.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    SANS
    SAXS
    HMX-PBX
    thermal damages
    phase transition
    Opis:
    The thermal damage in octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) based plastic-bonded explosive (PBX) was investigated using in situ small-angle neutron and X-ray scattering techniques. The microstructural evolution was quantitatively characterized by the model fitting parameters of total interfacial surface area (Sv) and void volume distribution. The Sv of HMX-PBX decreased markedly above 100 °C, indicating the movement of binder into the voids. After subsequent cooling to room temperature, the scattering intensity increased significantly with increasing storage time, and a new population of voids with average diameter of 20 nm was observed, accompanied by the gradual phase transition of HMX from δ- to β-phase. The experimental results implied that serious damage within the HMX-PBX was developed during storage after heating.
    Źródło:
    Central European Journal of Energetic Materials; 2016, 13, 4; 916-926
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermally induced damage in hexanitrohexaazaisowurtzitane
    Autorzy:
    Tian, Q.
    Yan, G.
    Sun, G.
    Huang, C.
    Xie, L.
    Chen, B.
    Huang, M.
    Li, H.
    Liu, X.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358735.pdf
    Data publikacji:
    2013
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    CL-20
    SAXS
    AFM
    thermal effects
    voids
    Opis:
    The evolution of the microstructure of hexanitrohexaazaisowurtzitane (CL-20) after a thermal stimulus plays a key role in the performance of CL-20. In the current work, microstructural variations of CL-20 caused by thermal treatment were investigated by X-ray diffraction, in situ variable-temperature optical microscopy, atom force microscopy, and small-angle X-ray scattering. A wave-like process, an abrupt volume expansion, movement, and fragmentation of CL-20 particles during phase transition were observed. After the phase transition (160 °C) the CL-20 sample acquired a very rough surface with numerous dimple depressions, and during the thermal decomposition stage (200 °C) a large number of voids were produced in both the bulk and the surface of the CL-20.
    Źródło:
    Central European Journal of Energetic Materials; 2013, 10, 3; 359-369
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effects of Polymeric Binders on the RDX-based Explosive Response Character under Slow Cook-off Conditions
    Autorzy:
    Yan, X.
    Li, X. D.
    Zhang, Y. R.
    Liu, L.
    Zhang, X. M.
    Tan, Y. X.
    Wang, H.
    Wang, X. Q.
    Powiązania:
    https://bibliotekanauki.pl/articles/358419.pdf
    Data publikacji:
    2018
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    RDX-based explosive
    slow cook-off experiment
    binder content
    binder type
    Opis:
    Due to safety requirements, insensitive behaviour under slow thermal heating (cook-off) conditions is a desirable behaviour for today’s munitions. In this paper a cook-off device is designed to test two groups of RDX-based PBX explosives. In the first group the binder type was varied and in the second group the binder content of the RDX-based explosive was changed. Eleven samples were examined in order to evaluate the influence of four different binders and seven different binder contents on the shell deformation and the degree of the involved reaction. The test results showed that the degree of the reaction can be improved by changing the binder content, but not by the binder type. This phenomenon was explained by the thermal-conduction theory.
    Źródło:
    Central European Journal of Energetic Materials; 2018, 15, 2; 339-350
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-13 z 13

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