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Wyświetlanie 1-15 z 54
Tytuł:
Effect of Annealing, Stoichiometry, and Surface on Magnetism of (Pr,Dy)FeCoB Microparticles Ensemble
Autorzy:
Kablov, E. N.
Ospennikova, O. G.
Kunitsyna, E. I.
Piskorskii, V. P.
Korolev, D. V.
Morgunov, R. B.
Powiązania:
https://bibliotekanauki.pl/articles/356579.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
rare earth metals
magnets
magnetisation
Mössbauer spectroscopy
X-ray spectroscopy
Opis:
Magnetic properties of powder (Pr,Dy)FeCoB ferrimagnetic alloys and effects of annealing, surface states were analyzed. X-ray photoelectron spectroscopy and Mössbauer spectra of powders indicate the effect of surface states on phase composition and magnetic properties of the studied powder, if particles average size is smaller than 10 μm. Effect of stoichiometry on magnetic anisotropy was found. Thermal stability of anisotropy field was proved by replacement of Fe atoms with Co atoms.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 3; 1923-1930
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Examination of the Properties of Samples from Glass-Epoxy Core Rods for Composite Insulators Subjected to DC High Voltage
Autorzy:
Wieczorek, K.
Jaroszewski, M.
Ranachowski, P.
Ranachowski, Z.
Powiązania:
https://bibliotekanauki.pl/articles/351254.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
DC high voltage
composite insulator
glass-epoxy core
dielectric spectroscopy
Raman spectroscopy
Opis:
This article presents the results of an examination performed on a set of samples of glass-epoxy core rods used in composite insulators with silicone rubber housings. The goal of the examination was to test the aging resistance of the core material when exposed to Direct Current (DC) high voltage. Long term exposure of a glass-epoxy core rod to DC high voltage may lead to the gradual degradation of its mechanical properties due to the ion migrations. Electrolysis of the core material (glass fiber) may cause electrical breakdown of the insulators and consequently lead to a major failure. After being aged for 6000 hours under DC high voltage, the samples were subjected to microscopic analysis. Their chemical composition was also examined using Raman spectroscopy and their dielectric losses and conductance in the broad range of frequencies were tested using dielectric spectroscopy.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1281-1286
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Loading Effect of Ag Nanoparticles on Photocatalytic Activity of TiO2 Nanorod Arrays Prepared by Hydrothermal Method
Autorzy:
Lee, Kwangmin
Yoo, Daeheung
Zakiyuddin, Ahmad
Powiązania:
https://bibliotekanauki.pl/articles/2049271.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
TiO2 nanorods
Ag nanoparticles
hydrothermal
Electrochemical impedance spectroscopy
UV-Vis spectroscopy
Opis:
Rutile-TiO2 nanorod thin films were formed on Ti disks via alkali treatment in NaOH solutions followed by heat treatment at 700°C. Ag nanoparticles were loaded on nanorods using a photo-reduction method to improve the photocatalytic properties of the prepared specimen. The surface characterization and the photo-electrochemical properties of the Ag-loaded TiO2 nanorods were investigated using a field-emission scanning electron microscope (FE-SEM), X-ray photoelectron spectroscopy (XPS), UV-Vis spectroscopy and electrochemical impedance spectroscopy (EIS). The TiO2 nanorods obtained after the heat treatment were 80 to 180 nm thick and 1 μm long. The thickness of the nanorods increased with the NaOH concentration. The UV-Vis spectra exhibit a shift in the absorption edge of the Ag-loaded TiO2 to the visible light range and further narrowing of the bandgap. The decrease in the size of the capacitive loops in the EIS spectra showed that the Ag loading effectively improved the photocatalytic activity of the TiO2 nanorods.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 3; 751-754
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis of the Phase Transitions in BNT-BT Lead-Free Ceramics Around Morphotropic Phase Boundary by Mechanical and Dielectric Spectroscopies
Autorzy:
Silva Jr, P. S.
Diaz, J. C. C. A.
Florêncio, O.
Venet, M.
M’Peko, J. C.
Powiązania:
https://bibliotekanauki.pl/articles/353072.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Lead-free piezoelectric ceramics
morphotropic phase boundary
phase transitions
mechanical spectroscopy
dielectric spectroscopy
Opis:
In this work, the syntheses and characterization by mechanical and dielectric spectroscopies of (1-x) Bi0.5Na0.5TiO3-xBaTiO3 (BNT-100xBT), with x = 0.05, 0.06 and 0.07, lead-free piezoelectric ceramics is reported. Ceramic samples of BNT-BT have been prepared by mixed-oxide method and then conventionally sintered. X-ray diffraction patterns of sintered samples, indicated for BNT-7BT the presence of tetragonal (P4mm) complex perovskite structure, whereas for BNT-5BT and BNT-6BT the samples exhibit a mixture of tetragonal (P4mm) and rhombohedral (R3c) crystalline phases, which reveal the presence of a morphotropic phase boundary (MPB) in the BNT-BT system. Measurements of internal friction, Q-1, and the storage modulus, E’, as a function of temperature at various frequencies were carried out in a Dynamic Mechanical Analyzer (DMA), in the temperature range from 0ºC to 600ºC. Dielectric profiles are recorded in the frequency range from 1kHz to 100kHz and the temperature range from room temperature to 475ºC. Mechanical loss spectra obtained for investigated compositions of BNT-BT samples showed different frequency-independent anomalies. Two main anomalies for BNT-5BT and BNT-6BT, observed around 100ºC and 430ºC were associated with the ferroelectric-antiferroelectric and antiferroelectricparaelectric phase transitions, respectively. The results obtained from mechanical loss measurements were supported by dielectric relaxation spectra. For BNT-7BT, outside the MPB, four different frequency-independent processes were observed.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 17-20
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Lanthanum Dopant on the Structure and Electric Properties of BaBi2Nb2O9 Ceramics
Autorzy:
Adamczyk-Habrajska, M.
Goryczka, T.
Szalbot, D.
Dzik, J.
Rerak, M.
Bochenek, D.
Powiązania:
https://bibliotekanauki.pl/articles/353535.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ferroelectric relaxor
ceramics
impedance spectroscopy
Opis:
The paper reports the consequences of lanthanum modifications of barium bismuth niobiate (BaBi2 Nb2 O9) ceramics. The discussed materials were prepared by solid state synthesis and a one-step sintering process. The investigations are focused on dielectric aspects of the modification. The presented results reveal that the trivalent lanthanum ions incorporate twovalent barium ions, which is connected with the creation of A-site cationic vacancies as well as oxygen vacancies. Such a scenario results in significant decreasing in grain boundaries resistivity. The activation energy of grain boundaries conductivity is significantly reduced in the case of lanthanum admixture.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 1; 207-214
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of CuO and V2O5 Effect on IR Spectra of Polycrystalline Bismuth Niobate
Autorzy:
Kuźniarska-Biernacka, I.
Lisińska-Czekaj, A.
Czekaj, D.
Powiązania:
https://bibliotekanauki.pl/articles/352587.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
BiNbO4
ceramics
SEM
FTIR spectroscopy
Opis:
Bismuth niobate (BiNbO4) ceramics were fabricated by mixed oxide method and sintered by presureless sintering method. BiNbO4 ceramics doped with V2 O5 additive in amount 0.125 wt%, 0.250 wt% and 1 wt% of was sintered at T = 910°C whereas BiNbO4 ceramics doped with 2 wt% of CuO additive was sintered at T = 890°C and T = 910°C. It was found that V2 O5 additive improved morphology of the ceramic samples. However, the chemical composition of BiNbO4 ceramics in relation to bismuth oxide and niobium oxide manifested a tendency of lack of Bi2 O3 component. Absorption bands for the BiNbO4 compound were identified. FTIR band positions associated with NbO6 octahedra suggested that the crystal structure changes after V2 O5 incorporation.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 817-821
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optical Properties of Intraocular Implants Coated with Silver Nanoparticles
Autorzy:
Jeż, Kinga
Gacek, Marcin
Nabiałek, Marcin
Tóth, László
Pike-Biegunski, M.
Powiązania:
https://bibliotekanauki.pl/articles/2049713.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
UV-Vis spectroscopy
intraocular lenses
silver nanoparticles
Opis:
Prolonged exposure to UV radiation, and ever-increasing life expectancy, mean that an increasing proportion of the population suffers from clouding of the intraocular lens. Nowadays, the performance of intraocular implantation procedures is commonplace. Unfortunately, with the increasing number of operations, the number of postoperative complications is also increasing. One way to avoid complications may be to use an intraocular implant that has been immersed in a solution containing silver nanoparticles. As part of the study, four selected intraocular implants – that are available on the ophthalmic market – were tested. In order to investigate the effect of silver particles on the optical properties of the implants, tests were carried out using a UV-VIS spectrophotometer. Two series of implants were tested: before and after immersion in a silver solution. The implants were immersed for a period of 7 days. It was found that the presence of silver particles does not have a negative impact on the translucency of the implants.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 2; 477-481
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Cold Rolling on Electrochemical Impedance Behavior of New β-Type Ti-6Mo-6V-5Cr-3Sn-2.5Zr Alloy
Autorzy:
Song, Hocheol
Zakiyuddin, Ahmad
Kim, Sinhye
Lee, Kwangmin
Powiązania:
https://bibliotekanauki.pl/articles/351262.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
beta-titanium alloy
electrochemical impedance spectroscopy
potentiodynamic polarization
Opis:
In this study, the corrosion properties of Ti-6Mo-6V-5Cr-3Sn-2.5Zr alloy were investigated as a function of the cold rolling ratio and annealing temperature. The annealing treatment was carried out at temperature of 680°C, 730°C, and 780°C. The highest corrosion potential observed in the specimen with a 10% rolling ratio was 179 mV, which was more positive than that of the nonrolled specimen (–0.214 VSSC). The lowest corrosion current density (1.30×10-8 A/cm2) was observed in the non-rolled specimen which suggested that the integrity of its passive oxide layer was superior to that of the cold-rolled specimens. Time-dependent EIS evaluation revealed that the consistency of the passive oxide layer was highly affected by the subjected rolling ratio over time.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 2; 487-490
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Professor Robert Schaller: Zener Medalist
Profesor Robert Schaller: Medalista Zenera
Autorzy:
Mari, D.
Powiązania:
https://bibliotekanauki.pl/articles/356080.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
internal friction
mechanical spectroscopy
tarcie wewnętrzne
spektroskopia mechaniczna
Opis:
The following is the text of an oral presentation delivered at the Zener Medal Award ceremony in Hefei on 23 September 2015.
Poniżej znajduje się tekst ustnej prezentacji wygłoszonej podczas ceremonii wręczenia medali Zenera w Hefei w dniu 23 września 2015 r.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 5-6
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Selective Corrosion of Al2Cu Intermetallic Phase in Orthophosphoric Acid Aqueous Solutions
Autorzy:
Kwolek, P.
Gradzik, A.
Szeliga, D.
Kościelniak, B.
Powiązania:
https://bibliotekanauki.pl/articles/351947.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
intermetallic phase
selective corrosion
orthophosphoric acid
electrochemical impedance spectroscopy
Opis:
Al2Cu phase has been obtained by melting pure metals in the electric arc furnace. It has been found that the intermetallic phase undergoes selective corrosion in the H3PO4 aqueous solutions. Aluminium is dissolved, the surface becomes porous and enriched with copper. The corrosion rate equals to 371 ±17 g∙m-2∙day-1 (aerated solution) and 284 ± 9 g∙m-2∙day-1 (deaerated solution). The surface of Al2Cu phase after selective corrosion was characterised by using electrochemical impedance spectroscopy. It was found that the surface area of the specimens increases with temperature due to higher corrosion rate and is between 2137 and 3896 cm2.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1223-1229
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Soft Magnetic Properties of Fe-Zr-(Pt)-Nb-Cu-B Amorphous Alloys
Autorzy:
Gondro, J.
Błoch, K.
Nabiałek, M.
Walters, S.
Powiązania:
https://bibliotekanauki.pl/articles/356965.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
amorphous alloys
Mössbauer spectroscopy
magnetic susceptibility
Curie temperature
magnetic properties
Opis:
This paper presents the results of investigations into the microstructure and magnetic properties of Fe86Zr7Nb1Cu1B5, Fe82Zr7Nb2Cu1B8 and Fe81Pt5Zr7Nb1Cu1B5 alloys. The alloys were investigated in their as-quenched state, in the form of thin ribbons with approximate dimensions as follows: width 3 mm and thickness 20 μm. The investigations were performed utilizing Mössbauer spectrometry and X-ray diffractometry. Also, an evaluation of the low-field magnetic susceptibility and measurements of the magnetization versus temperature and magnetizing field were performed.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2A; 707-710
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Corrosion Properties of Ca65-xMg17.5Zn17.5+x (x = 0, 2.5, 5) Alloys
Autorzy:
Babilas, R.
Wojciechowski, P.
Bajorek, A.
Sakiewicz, P.
Cesarz-Andraczke, K.
Powiązania:
https://bibliotekanauki.pl/articles/352466.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ca-based alloys
corrosion
hydrogen evolution
X-ray photoelectron spectroscopy
Opis:
The aim of the paper is to study the effect of zinc addition on the corrosion behavior of Ca65-xMg17.5Zn17.5+x(x = 0, 2.5, 5 at.%) alloys in simulated physiological fluids at 37°C. The electrochemical measurements allowed to determine a corrosion potential, which showed a positive shift from –1.60 V for Ca65Mg17.5Zn17.5 alloy to –1.58 V for Ca60Mg17.5Zn22.5 alloy, adequately. The more significant decrease of hydrogen evolution was noticed for Ca60Mg17.5Zn22.5 alloy (22.4 ml/cm2) than for Ca62.5Mg17.5Zn20 and Ca65Mg17.5Zn17.5 samples (29.9 ml/cm2 and 46.4 ml/cm2), consequently. The corrosion products after immersion tests in Ringer’s solution during 1 h were identified by X-ray diffraction and X-ray photoelectron spectroscopy as calcium, magnesium oxides, carbonates, hydroxides and calcium hydrate.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 1033-1040
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Raman Spectroscopy Studies of Carbon-Based Cathode Materials during Aluminum Electrolysis
Autorzy:
Wang, Wei
Chen, Weijie
Powiązania:
https://bibliotekanauki.pl/articles/352779.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminium electrolysis
carbon cathodes
Raman spectroscopy
creep deformation
sodium expansion
Opis:
The sodium expansion and creep strain of semi-graphitic cathodes are investigated using a modified Rapoport apparatus. To further understanding of the sodium and bath penetration damage processes, the impact of external stress fluence on the carbon cathode microstructure has been defined with XRD analysis, Raman spectroscopy and scanning electron microscope (SEM). Graphite atoms fracture into smaller fragments that are less directional than the pristine platelets, which allows for a possible filling of the cracks that thus develop by the sodium and bath during aluminum electrolysis. The average microcrystalline size (calculated by Raman spectroscopy) is reduced by the deformation. The decreased intensity and widened 'G' and 'D' peaks in the analysis indicate the poor order of the sheets along the stacking direction while the consistent layered graphite structure is sustained.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1257-1261
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Curie Temperature and Microstructural Changes Due to the Heating Treatment of Magnetic Amorphous Materials
Autorzy:
Gondro, J.
Błoch, K.
Brągiel, P.
Nabiałek, M.
Szota, M.
Powiązania:
https://bibliotekanauki.pl/articles/958228.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
amorphous alloys
magnetic properties
magnetic susceptibility
Mössbauer spectroscopy
Curie temperature
Opis:
Three distinct alloys: Fe86Zr7Nb1Cu1B5, Fe82Zr7Nb2Cu1B8, and Fe81Pt5Zr7Nb1Cu1B5 were characterized both magnetically and structurally. The samples, obtained with spinning roller method as a ribbons 3 mm in width and 20 μm thick, were investigated as-quenched and after each step of a multi steps heating treatment procedure. Each sample was annealed at four steps, fifteen minutes at every temperature, starting from 573K+600K up to +700K depending on type of alloy. Mössbauer spectroscopy data and transmission electron microscope (HRE M) pictures confirmed that the as-quenched samples are fully amorphous. This is not changed after the first stages of treatment heating leads to a reduction of free volumes. The heating treatment has a great influence on the magnetic susceptibilities. The treatment up to 600K improves soft magnetic properties: an χ increase was observed, from about 400 to almost 1000 for the samples of alloys without Pt, and from about 200 to 450 at maximum, for the Fe81Pt5Zr7Nb1Cu1B5. Further heating, at more elevated temperatures, leads to magnetic hardening of the samples. Curie temperatures, established from the location of Hopkinson’s maxima on the χ(T) curve are in very good agreement with those obtained from the data of specific magnetization, σ(T), measured in a field of 0.75T. As a critical parameter β was chosen to be equal 0.36 for these calculations, it confirmed that the alloys may be considered as ferromagnetic of Heisenberg type. Heating treatment resulted in decreasing of TC. These changes are within a range of several K.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 451-456
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 54

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