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    Wyświetlanie 1-6 z 6
    Tytuł:
    Synthesis of Silica Microspheres Containing Iron Oxide Nanoparticles for Removal of Organic Pollutant by Adsorption and Photocatalytic Decomposition
    Autorzy:
    Cho, Young-Sang
    Sung, Sohyeon
    Powiązania:
    https://bibliotekanauki.pl/articles/2049298.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    composite microsphere
    magnetic nanoparticle
    self-assembly
    adsorption
    Opis:
    Iron oxide nanoparticles were incorporated to form composite microspheres of SiO2 and Fe2O3 for magnetic separation of the particles after adsorption or photochemical decomposition. Economic material, sodium silicate, was purified by ion exchange to prepare aqueous silicic acid solution, followed by mixing with iron oxide nanoparticles. Resulting aqueous dispersion was emulsified, and composite microspheres of SiO2 and Fe2O3 was formed from the emulsion droplets as micro-reactors during heating. Removal of methylene blue using the composite microspheres was performed by batch adsorption process. Synthesis of composite microspheres of silica containing Fe2O3 and TiO2 nanoparticles was also possible, the particles could be separated using magnets efficiently after removal of organic dye.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 3; 771-776
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Rapid Synthesis of Gold Nano-Particles Using Pulse Waved Potential in a Non-Aqueous Electrolyte
    Autorzy:
    Jang, J. G.
    Lee, J.-O.
    Lee, C. K.
    Powiązania:
    https://bibliotekanauki.pl/articles/352529.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    gold
    nanoparticle
    nonaqueous electrolyte
    pulse wave
    catalyst
    Opis:
    Rapid synthesis of gold nanoparticles (AuNPs) by pulsed electrodeposition was investigated in the non-aqueous electrolyte, 1-ethyl-3-methyl-imidazoliumbis(trifluoro- methanesulfonyl)imide ([EMIM]TFSI) with gold trichloride (AuCl3). To aid the dissolution of AuCl3, 1-ethyl-3-methyl-imidazolium chloride ([EMIM]Cl) was used as a supporting electrolyte in [EMIM]TFSI. Cyclicvoltammetry experiments revealed a cathodic reaction corresponding to the reduction of gold at −0.4 V vs. Pt-QRE. To confirmthe electrodeposition process, potentiostatic electrodeposition of gold in the non-aqueous electrolyte was conducted at −0.4 V for 1 h at room temperature. To synthesize AuNPs, pulsed electrodeposition was conducted with controlled duty factor, pulse duration, and overpotential. The composition, particle-size distribution, and morphology of the AuNPs were confirmed by field-emission scanning electron microscopy (FE-SEM), energy-dispersive spectroscopy (EDS), and transmission electron microscopy (TEM). The electrodeposited AuNPs were uniformly distributed on the platinum electrode surface without any impurities arising from the non-aqueous electrolyte. The size distribution of AuNPs could be also controlled by the electrodeposition conditions.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1389-1392
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Magnetic Properties of (Nia-Znb)X Cu1-X Ferrite Nanoparticle Fabricated by Sol-Gel Process
    Autorzy:
    Yang, S.
    Kim, J.-G.
    Powiązania:
    https://bibliotekanauki.pl/articles/352091.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Ni-Zn-Cu ferrite
    nanoparticle
    soft magnetic property
    sol-gel
    Opis:
    In future, more mobile devices with different frequencies will be used at the same time. Therefore, it is expected that the trouble caused by wave interference between devices will be further intensified. In order to prevent this trouble, investigation of selective frequency transmission or absorption material is required. In this paper, magnetic properties of nickel-zinc-copper ferrite nano powder was researched as wave absorber. (Nia-Znb)xCu1-xFe2O4(NZCF) nanoparticles were fabricated by the sol-gel method. The influence of copper substitution on lattice parameter change was analyzed by X-ray diffraction (XRD), particle size was analyzed by scanning electron microscopy (SEM), and Magnetic properties analyzed by vibrating sample magnetometer (VSM). The NZCF and Nickel-zinc ferrite (NZF) lattice parameter difference was 0.028 Å and particle size was calculated as 30 nm with the XRD peak. The VSM results of (Ni0.3-Zn0.3)0.6Cu1-0.6Fe2O4 annealed sample at 700°C for 3hous were 58.5 emu/g (Ms), 22.8 Oe (Hc). It was the most suitable magnetic properties for wave absorber in this investigation.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1197-1200
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Phase Structure and Magnetic Properties of Intermetallic Cu-Ni Alloy Nanopowders Synthesized by the Electrical Explosion of Wire
    Autorzy:
    Nguyen, Minh-Thuyet
    Kim, Jin-Chun
    Powiązania:
    https://bibliotekanauki.pl/articles/352297.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Cu-Ni alloy
    nanoparticle
    phase structure
    magnetism
    explosion of wire
    Opis:
    Cu-Ni composite nanoparticles were successfully synthesized by electrical explosion of wire (EEW) method. Cu-Ni alloy and twisted wires with various Ni contents were used as the feeding material for a 3 kV charging voltage EEW machine in an ethanol ambient chamber. The phase structure and magnetic properties of the as-fabricated samples were studied. It was established that the prepared powders after drying have a spherical form with the particle size is under 100 nm. XRD analysis indicated that the nanopowders consisted of binary Cu-Ni phases. Only pure phases of the intermetallic compound Cu-Ni (Cu0.81Ni0.19 and Cu3.8Ni) were observed in the XRD patterns of the samples. The synthesized intermetallic Cu-Ni alloy nanopowders reveal magnetic behaviors, however, the lower Ni content samples exhibited paramagnetic behaviors, meanwhile, the higher Ni content samples exposed ferromagnetic properties.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 3; 893-898
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Formation And Stabilization Of Silver Nanoparticles In Ethanol By Phosphinic Acid
    Redukcja i stabilizacja nanocząstek srebra w etanolu przez kwas fosforowy
    Autorzy:
    Kim, J.-K.
    Shim, H.-M.
    Park, M. J.
    Koo, K.-K.
    Powiązania:
    https://bibliotekanauki.pl/articles/356073.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    silver
    nanoparticle
    kinetic analysis
    phosphinic acid
    reduction
    srebro
    nanocząstki
    analiza kinetyczna
    kwas fosforowy
    redukcja
    Opis:
    Although phosphinic acid (H3PO2) has a powerful reduction potential, the reduction of silver ions by phosphinic acid salt has not yet been reported. In this work, colloidal silver has successfully synthesized by reducing silver ions in ethanol with phosphinic acid as a reducing agent. The effects of [AgNO3]/[H3PO2] ratios and reaction temperature were considered. Spherical silver nanoparticles with cubic structure were successfully prepared and their diameters were measured to be 8.5±0.9 nm − 11.3±0.2 nm. Half-life analysis showed that the reduction of silver ions proceeded with the reaction order of 1.30 on concentration of phosphinic acid and activation energy of 120.7 kJ/mol.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1293-1296
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Double Step Sintering Behavior Of 316L Nanoparticle Dispersed Micro-Sphere Powder
    Dwuetapowe spiekanie mikrosferycznych nanocząstek proszku 316L
    Autorzy:
    Jeon, B.
    Sohn, S. H.
    Lee, W.
    Han, C.
    Kim, Y. D.
    Choi, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/355221.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    316L stainless steel
    nanoparticle dispersed micro-sphere
    pulse wire explosion
    sintering
    stal nierdzewna 316L
    spiekanie dwuetapowe
    mikrosferyczne nanocząstki
    Opis:
    316L stainless steel is a well-established engineering material and lots of components are fabricated by either ingot metallurgy or powder metallurgy. From the viewpoints of material properties and process versatility, powder metallurgy has been widely applied in industries. Generally, stainless steel powders are prepared by atomization processes and powder characteristics, compaction ability, and sinterability are quite different according to the powder preparation process. In the present study, a nanoparticle dispersed micro-sphere powder is synthesized by pulse wire explosion of 316L stainless steel wire in order to facilitate compaction ability and sintering ability. Nanoparticles which are deposited on the surface of micro-powder are advantageous for a rigid die compaction while spherical micro-powder is not to be compacted. Additionally, double step sintering behavior is observed for the powder in the dilatometry of cylindrical compact body. Earlier shrinkage peak comes from the sintering of nanoparticle and later one results from the micro-powder sintering. Microstructure as well as phase composition of the sintered body is investigated.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1155-1158
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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