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    Wyświetlanie 1-6 z 6
    Tytuł:
    High Concentration of Arsenic Removal from Acid Leaching Solution of Zinc Oxide Dust by Water-Quenched Slag
    Autorzy:
    Sun, H. Y.
    Sen, W.
    Kong, X.
    Liu, G. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/356676.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    arsenic removal
    water-quenched slag
    zinc oxide dust
    purification
    Opis:
    The present work provides a study on high concentration of arsenic removal from acid leaching solution of zinc oxide dust by water-quenched slag. The water-quenched slag is a waste slag produced from fuming furnace of lead pyrometallurgical process and used as a substitute of ferrous sulfate heptahydrate to precipitate arsenic at purification section. The effects of reaction temperature, reaction time, the addition of H2O2 and the addition of water-quenched slag on arsenic removal rate were systematically investigated. The reaction temperature of 70°C, reaction time of 1h, H2O2 addition of 10.8 mL/L and water-quenched slag addition of 17.8 g/L are identified as the best technical parameters. At the optimum conditions, the arsenic (III) with high concentration (As 4.13 g/L) is efficiently removed (arsenic removal rate > 99%). The filtrate (Fe 1.21 mg/L, As 1.53 mg/L) with low concentrations of arsenic and iron and the stable filter residue are also obtained successfully. The United States EPA Toxicity Characteristic Leaching Procedure (TCLP) test shows that the As leachability never exceeds the regulatory limit of 5 mg/L As. The results suggest that the water-quenched slag shows potential for removing high concentration of arsenic from acid leaching solution of zinc oxide dust.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 1; 425-430
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Strain Rate on the Microstructure of Warm-Deformed Ultrafined Medium-Carbon Steel
    Autorzy:
    Yuan, Q.
    Xu, G.
    Liu, S.
    Liu, M.
    Hu, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/355659.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    warm deformation
    medium-carbon steel
    ultrafine grain
    strain rate
    Fe3C
    Opis:
    In this study, medium-carbon steel was subjected to warm deformation experiments on a Gleeble 3500 thermosimulator machine at temperatures of 550°C and 650°C and strain rates of 0.001 s-1 to 1 s-1. The warm deformation behavior of martensite and the effects of strain rate on the microstructure of ultrafine grained medium-carbon steel were investigated. The precipitation behavior of Fe3C during deformation was analyzed and the results showed that recrystallization occurred at a low strain rate. The average ultrafine ferrite grains of 500 ± 58 nm were fabricated at 550°C and a strain rate of 0.001 s-1. In addition, the size of Fe3C particles in the ferrite grains did not show any apparent change, while that of the Fe3C particles at the grain boundaries was mainly affected by the deformation temperature. The size of Fe3C particles increased with the increasing deformation temperature, while the strain rate had no significant effect on Fe3C particles. Moreover, the grain size of recrystallized ferrite decreased with an increase in the strain rate. The effects of the strain rate on the grain size of recrystallized ferrite depended on the deformation temperature and the strain rate had a prominent effect on the grain size at 550°C deformation temperature. Finally, the deformation resistance apparently decreased at 550°C and strain rate of 1 s-1 due to the maximum adiabatic heating in the material.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 4; 1805-1813
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Tuning The Crystallographic Structure And Morphology Of Nanocrystalline CaB6 Films Deposited By DC Magnetron Sputtering
    Optymalizacja struktury krystalograficznej i morfologii nanokrystalicznych warstw CaB6 naniesionych metodą napylania magnetronowego
    Autorzy:
    Zhang, L.
    Zhao, G.
    Liu, H.
    Min, G.
    Yu, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/356295.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    CaB6 films
    crystallographic structure
    morphology
    argon pressure
    warstwy CaB6
    struktura krystalograficzna
    morfologia
    ciśnienie argonu
    Opis:
    Through changing the argon pressure, CaB6 films with different crystallographic orientation and morphology on glass substrates were prepared by direct current (DC) magnetron sputtering method. The film textures, crystallite sizes, composition and morphology were investigated by a spectrum of characterizing techniques in terms of X-ray diffraction (XRD), field emission scanning electron microscopy with energy dispersive spectrometer (FESEM-EDS), atomic force microscopy (AFM), Raman shift spectroscopy. The influence of argon pressure on microstructure was studied. The average grain size increased with the argon pressure increasing from 0.8 Pa to 1.5 Pa. Meanwhile, the dominant crystal face changed from (110) to (100). Then the grain size decreased when the argon pressure increased to 2.0 Pa. The surface morphology evolved from typical cauliflower-like nanocrystalline clusters to faceted rectangular pyramids. It was found that considerable amount of argon atoms were trapped in the films. The formation process of CaB6 films was also analyzed in this paper.
    Warstwy CaB6 naniesiono na podłoża szkliste metodą magnetronowego rozpylania stałoprądowego (DC). Poprzez kontrolę ciśnienia argonu otrzymano warstwy o różnej morfologii i orientacji krystalograficznej. Strukturę, wielkość krystalitów oraz skład chemiczny warstw badano przy zastosowaniu następujących technik: dyfrakcji rentgenowskiej (XRD), skaningowej mikroskopii elektronowej w połączeniu ze spektroskopią dyspersji energii promieniowania rentgenowskiego (SEM-EDS), mikroskopii sił atomowych (AFM) oraz spektroskopii Ramana. Badano wpływ ciśnienia argonu na mikrostrukturę warstwy. Wraz ze wzrostem ciśnienia argonu z 0,8 Pa do 1,5 Pa zwiększyła się średnia wielkość ziaren przy jednoczesnej zmianie głównych kierunków krystalograficznych – z (110) w (100). Natomiast w wyniku dalszego wzrostu ciśnienia do 2,0 Pa, wielkość ziaren zmniejszyła się. Zaobserwowano także zmiany w morfologii powierzchni. Stwierdzono, że znaczna ilość atomów argonu została uwięziona w warstwach. W niniejszej pracy poddano także analizie proces powstawania warstw CaB6.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2A; 897-901
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal Mechanical Stress Analysis of Ladle Lining with Integral Brick Joint
    Autorzy:
    Chang, W.
    Li, G.
    Kong, J.
    Sun, Y.
    Jiang, G.
    Liu, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/354915.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    ladle
    heat transfer model
    lining
    expansion joint
    thermal mechanical stress
    Opis:
    Based on the theory of heat transfer, the influence of expansion joints on the temperature and stress distribution of ladle lining is discussed. In view of the current expansion joint, the mathematical model of heat transfer and the three dimensional finite element model of ladle lining brick are established. By analyzing the temperature and stress distribution of ladle lining brick when the expansion joints are in different sizes, the thermal mechanical stress caused by the severe temperature difference can be reduced by the suitable expansion joint of the lining brick during the ladle baking and working process. The analysis results showed that the thermal mechanical stress which is caused by thermal expansion can be released through the 2 mm expansion joint, which is set in the building process. So we can effectively reduce the thermal mechanical stress of the ladle lining, and there is no risk of steel leakage, thus the service life of ladle can be effectively prolonged.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 2; 659-666
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of The Desorption-Recombination Temperature On The Microstructure And Magnetic Properties Of HDDR Processed Nd-Fe-B Powders
    Wpływ temperatury desorpcji-rekombinacji na mikrostrukturę i właściwości magnetyczne proszków Nd-Fe-B przetwarzanych metodą HDDR
    Autorzy:
    Lee, J.-G.
    Cha, H.-R.
    Liu, S.
    Yu, J.-H.
    Baek, Y.-K.
    Kwon, H.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/353723.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Nd-Fe-B
    HDDR
    permanent magnet
    grain boundary
    metoda HDDR
    magnes trwały
    granica ziarna
    Opis:
    The effect of the desorption-recombination temperature on the microstructure and magnetic properties of hydrogenation-disproportionation-desorption-recombination (HDDR) processed Nd-Fe-B powders was studied. The NdxB6.4Ga0.3Nb20.2Febal (x=12.5-13.5, at.%) casting alloys were pulverized after homogenizing annealing, and then subjected to HDDR treatment. During the HDDR process, desorption-recombination (DR) reaction was induced at two different temperature, 810°C and 820°C. The higher Nd content resulted in enhanced coercivity of the HDDR powder, and which was attributed to the thicker and more uniform Nd-rich phase along grain boundaries. But this uniform Nd-rich phase induced faster grain growth. The remanence of the powder DR-treated at 820°C is higher than that DR-treated at 810°C. In addition, it was also confirmed that higher DR temperature is much more effective to improve squareness.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1499-1501
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Bending, Impact Fracture Behavior and Characteristics of Stainless Steel Clad Plates with Different Rolling Temperature
    Autorzy:
    An, Q.
    Fan, K. Y.
    Ge, Y. F.
    Liu, B. X.
    He, J.
    Wang, S.
    Chen, C. X.
    Ji, P. G.
    Tolochko, O.
    Powiązania:
    https://bibliotekanauki.pl/articles/2049433.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    stainless steel clad plate
    interface characteristics
    bending behavior
    impact morphologies
    delamination crack
    Opis:
    The interface characteristics, bending and impact behavior, as well as fracture characteristics of stainless steel clad plates fabricated by vacuum hot rolling at different rolling temperatures of 1100°C, 1200°C and 1300°C are investigated in detail. The interface bonding strength is gradually increased with the increasing rolling temperature due to the sufficient diffusion behavior of alloy element. The bending toughness and impact toughness are gradually decreased, while the bending strength increase with the increase of the rolling temperature, which is attributed to mechanisms of matrix softening and interface strengthening at high rolling temperature. Due to the weak interface at 1100°C, the bending and impact crack propagation path was displaced by delamination cracks, which in turn lead to reduction in stress intensity of the main crack, playing an effective role in toughening the stainless steel clad plates. Moreover, the impact fracture morphologies of clad plates show a typical ductile-brittle transition phenomenon, which is attributed to the matrix softening behavior with the increasing rolling temperature.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 1; 229-239
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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