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Tytuł:
Atomistic Analysis Of Radiation-Induced Segregation In Ion-Irradiated Stainless Steel 316
Analiza w skali atomowej indukowanej promieniowaniem segregacji w stali nierdzewnej 316
Autorzy:
Lee, G.-G.
Jin, H.-H.
Chang, K.
Lee, B. H.
Kwon, J.
Powiązania:
https://bibliotekanauki.pl/articles/354713.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
atom probe tomography (APT)
radiation-induced segregation (RIS)
ion irradiation
irradiation defects
stainless steel
APT
RIS
stal nierdzewna
segregacja
Opis:
Stainless steel (SS) is a well-known material for the internal parts of nuclear power plants. It is known that these alloys exhibit radiation-induced segregation (RIS) at point defect sinks at moderate temperature, while in service. The RIS behavior of SS can be a potential problem by increasing the susceptibility to irradiation-assisted stress corrosion cracking. In this work, the RIS behavior of solute atoms at sinks in SS 316 irradiated with Fe4+ ions were characterized by atom probe tomography (APT). There were torus-shaped defects along with a depletion of Cr and enrichment of Ni and Si. These clusters are believed to be dislocation loops resulting from irradiation. The segregation of solutes was also observed for various defect shapes. These observations are consistent with other APT results from the literature. The composition of the clusters was analyzed quantitatively almost at the atomic scale. Despite the limitations of the experiments, the APT analysis was well suited for discovering the structure of irradiation defects and performing a quantitative analysis of RIS in irradiated specimens.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1179-1184
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of Compaction Pressure And Sintering Temperature On The Liquid Phase Sintering Behavior Of Al-Cu-Zn Alloy
Wpływ ciśnienia prasowania i temperatury spiekania na spiekanie stopu Al-Cu-Zn z udziałem fazy ciekłej
Autorzy:
Lee, S. H.
Ahn, B.
Powiązania:
https://bibliotekanauki.pl/articles/351836.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
powder metallurgy
liquid phase sintering
compaction pressure
Al-Cu-Zn alloy
metalurgia proszków
spiekanie w fazie ciekłej
ciśnienie prasowania
stop Al-Cu-Zn
Opis:
The liquid phase sintering characteristics of Al-Cu-Zn alloy were investigated with respect to various powder metallurgy processing conditions. Powders of each alloying elements were blended to form Al-6Cu-5Zn composition and compacted with pressures of 200, 400, and 600 MPa. The sintering process was performed at various temperatures of 410, 560, and 615°C in N2 gas atmosphere. Density and micro-Vickers hardness measurements were conducted at different processing stages, and transverse rupture strength of sintered materials was examined for each condition, respectively. The microstructure was characterized using optical microscope and scanning electron microscopy. The effect of Zn addition on the liquid phase sintering behavior during P/M process of the Al-Cu-Zn alloy was also discussed in detail.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1485-1489
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of Submicroscale Ag-Coated Cu Particles by Multi-Step Addition of Ag Plating Solution and Antioxidation Properties for Different Ag Shell Thicknesses
Autorzy:
Choi, E. B.
Lee, J.-H.
Powiązania:
https://bibliotekanauki.pl/articles/351202.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ag-coated Cu particle
submicrometer
Glycol-based Ag plating solution
mult-step addition
antioxidation
Opis:
For application as a low-cost conductive filler material, submicroscale Cu@Ag particles were fabricated at room temperature without any reductants by a multi-step addition method using an ethylene glycol-based Ag plating solution. Scanning electron microscopy images of the Ag-coated Cu particles demonstrated the formation of discrete Ag particles less than 100 nm in size as well as a thin Ag coating on Cu particles, during the early addition steps. However, as the thickness of the Ag coating increased, the small Ag particles agglomerated into Ag coatings with an increase in the number of Ag plating steps. Owing to the absence of additives such as surfactants, a comparison between the microstructural images and calculations indicated increased agglomeration between fabricated Ag-coated Cu particles with an increase in the number of Ag plating steps. However, thermogravimetric-differential scanning calorimetry of the agglomerated Ag-coated Cu particles after the fifth addition of the Ag plating solution demonstrated their antioxidation behavior even after 70 min in air at 150°C.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1137-1142
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characteristics Of The Porous Body Sintered By Nano-Sized Fe-Cr-Al Alloy Powder
Charakterystyka porowatego korpusu spiekanego z nanometrycznego proszku stopu Fe-Cr-Al
Autorzy:
Lee, S.-I.
Lee, S.-H.
Gu, B.-U.
Lee, D.-W.
Kim, B.-K.
Powiązania:
https://bibliotekanauki.pl/articles/356635.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-Cr-Al powder
metallic sponges
sintering temperature
oxidation resistance
proszek Fe-Cr-Al
proszek nanometryczny
temperatura spiekania
odporność na utlenianie
Opis:
Porous metal with uniform honeycomb structure was successfully produced by sintering using Fe-Cr-Al nano powder, which was prepared by the pulsed wire evaporation (PWE) in ethanol. Its process consisted of the several steps; 1) coating on the surface of polyurethane sponge with the liquid droplets generated from the ethanol-based slurry where the Fe-Cr-Al nano powders were uniformly dispersed, 2) heat treatment of debinding to remove the polyurethane sponge and 3) sintering of the porous green body formed by Fe-Cr-Al nano powders. The strut thickness of porous Fe-Cr-Al was increased by the increase of spraying times in ESP step. Also, The shrinkages and the oxidation resistance of the sintered porous body was increased with increase of sintering temperature. The optimal sintering temperature was shown to 1450°C in views to maximize the oxidation resistance and sinterability.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1275-1279
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Strut Thickness on Room and High Temperature Compressive Properties of Block-Type Ni-Cr-Al Powder Porous Metals
Autorzy:
Kang, B.-H.
Park, M.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/355591.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni-Cr-Al
powder porous metal
strut thickness
high temperature
compressive behavior
Opis:
This study investigated the effect of strut thickness on the room and high temperature compressive properties of block-type Ni-Cr-Al powder porous metals with ~3000 μm pore size manufactured using a new powder process. Two block-type Ni-Cr-Al porous metals with different strut thicknesses were manufactured. The strut thicknesses of two block foams were 340 μm (A) and 383 μm (B), respectively. Room temperature, 500°C, 650°C and 800°C compressive tests were performed. The compressive results identified typical elastic, plateau and densification regions of foam material in all temperature conditions. Regardless of the strut thickness, compressive strength (maximum peak stress) decreased as deformation temperature increased. In all deformation temperature ranges, the compressive strength measured higher in the porous metal with greater strut thickness (B). The high temperature deformation behavior of powder porous metal was confirmed to be affected by the structural factor and microstructural factor of the porous metal. With the findings described above, this study also discussed the high temperature deformation mechanism of the Ni-Cr-Al metal foam based on fracture surfaces after the high temperature compressions.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1329-1334
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Surfactant Addition on Bi2Te3 Nanostructures Synthesized by Hydrothermal Method
Autorzy:
Dharmaiah, P.
Lee, C. H.
Madavali, B.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/351609.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bismuth telluride
hydrothermal synthesis
spark plasma sintering
thermoelectric materials
X-ray diffraction
Opis:
In the present work, we have prepared Bi2Te3 nanostructures with different morphologies such as nano-spherical, nanoplates and nanoflakes obtained using various surfactant additions (EG, PVP, and EDTA) by a hydrothermal method. The shape of the nanoparticles can be controlled by addition of surfactants. The samples were characterized by x-ray diffraction (XRD) and scanning electron microscopy (SEM). It is found that the minority BiOCl phase disappears after maintained pH at 10 with EG as surfactant. SEM bulk microstructure reveals that the sample consists of fine and coarse grains. Temperature dependence of thermoelectric properties of the nanostructured bulk sample was investigated in the range of 300-450K. The presence of nanograins in the bulk sample exhibits a reduction of thermal conductivity and less effect on electrical conductivity. As a result, a figure of merit of the sintered bulk sample reached 0.2 at 400 K. A maximum micro Vickers hardness of 102 Hv was obtained for the nanostructured sample, which was higher than the other reported results.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1005-1010
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High Temperature Deformation Flow Of A ZK60A Magnesium Alloy After Extrusion
Płynięcie stopu magnezu ZK60A podczas wysokotemperaturowego odkształcenia w trakcie wytłaczania
Autorzy:
Kawasaki, M.
Lee, H. J.
Oh, M. C.
Ahn, B.
Powiązania:
https://bibliotekanauki.pl/articles/354374.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
activation energy
extrusion
flow mechanics
magnesium alloy
tensile property
energia aktywacji
wytłaczanie
mechanika przepływu
stop magnezu
rozciąganie
Opis:
Flow behavior of a ZK60A magnesium alloy after continuous casting and subsequent extrusion was examined in tension at a range of strain rates of 3.0×10-6 − 1.0×10-2 s-1 at temperatures of 473-623K. The results demonstrated that the alloy exhibited a maximum elongation of ~250% at 523K when tested at an initial strain rate of 1.0×10-5 s-1 and strain rate sensitivity, m, of ~0.3-0.4 and the activation energy of ~94 kJ/mol were calculated under the testing conditions. The detailed investigation suggested that the high temperature flow of the ZK60A alloy having submicrometer grains demonstrates quasi-superplastic flow behavior controlled by a dislocation viscous glide process.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1327-1330
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Characterization of CoCrFeNiMn High Entropy Alloy Powder Processed by Gas Atomization
Autorzy:
Park, T. G.
Lee, S. H.
Lee, B.
Cho, H. M.
Choi, W. J.
Kim, B. S.
Shin, K. S.
Kim, T.-S.
Powiązania:
https://bibliotekanauki.pl/articles/353649.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high entropy alloy
gas atomization
spark plasma sintering
CoCrFeNiMn
Opis:
In this study, precisely controlled large scale gas atomization process was applied to produce spherical and uniform shaped high entropy alloy powder. The gas atomization process was carried out to fabricate CoCrFeNiMn alloy, which was studied for high ductility and mechanical properties at low temperatures. It was confirmed that the mass scale, single phase, equiatomic, and high purity spherical high entropy alloy powder was produced by gas atomization process. The powder was sintered by spark plasma sintering process with various sintering conditions, and mechanical properties were characterized. Through this research, we have developed a mass production process of high quality and spherical high entropy alloy powder, and it is expected to expand applications of this high entropy alloy into fields such as powder injection molding and 3D printing for complex shaped components.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1055-1059
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Multistep Heat-Treatment Effects on Electrospun Nd-Fe-B-O Nanofibers
Autorzy:
Jeon, E. J.
Eom, N. S. A.
Lee, J.
Lee, B.
Cho, H. M.
On, J. S.
Choa, Y.-H
Kim, B. S.
Powiązania:
https://bibliotekanauki.pl/articles/354311.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nd-Fe-B
nanofibers
electrospinning
heat treatment
Opis:
Neodymium-Iron-Boron (Nd-Fe-B) magnets are considered to have the highest energy density, and their applications include electric motors, generators, hard disc drives, and MRI. It is well known that a fiber structure with a high aspect ratio and the large specific surface area has the potential to overcome the limitations, such as inhomogeneous structures and the difficulty in alignment of easy axis, associated with such magnets obtained by conventional methods. I n this work, a suitable heat-treatment procedure based on single-step and multistep treatments to synthesize sound electrospun Nd-Fe-B-O nanofibers of Φ572 nm was investigated. The single-step heat-treated (directly heat-treated at 800°C for 2 h in air) samples disintegrated along with the residual organic compounds, whereas the multistep heat-treated (sequential three-step heat-treated including three steps;: dehydration (250°C for 30 min in an inert atmosphere), debinding (650°C for 30 min in air), and calcination (800°C for 1 h in air)) fibers maintained sound fibrous morphology without any organic impurities. They could maintain such fibrous morphologies during the dehydration and debinding steps because of the relatively low internal pressures of water vapor and polymer, respectively. In addition, the NdFeO3 alloying phase was dominant in the multistep heat-treated fibers due to the removal of barriers to mass transfer in the interparticles.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1433-1437
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Double Step Sintering Behavior Of 316L Nanoparticle Dispersed Micro-Sphere Powder
Dwuetapowe spiekanie mikrosferycznych nanocząstek proszku 316L
Autorzy:
Jeon, B.
Sohn, S. H.
Lee, W.
Han, C.
Kim, Y. D.
Choi, H.
Powiązania:
https://bibliotekanauki.pl/articles/355221.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
316L stainless steel
nanoparticle dispersed micro-sphere
pulse wire explosion
sintering
stal nierdzewna 316L
spiekanie dwuetapowe
mikrosferyczne nanocząstki
Opis:
316L stainless steel is a well-established engineering material and lots of components are fabricated by either ingot metallurgy or powder metallurgy. From the viewpoints of material properties and process versatility, powder metallurgy has been widely applied in industries. Generally, stainless steel powders are prepared by atomization processes and powder characteristics, compaction ability, and sinterability are quite different according to the powder preparation process. In the present study, a nanoparticle dispersed micro-sphere powder is synthesized by pulse wire explosion of 316L stainless steel wire in order to facilitate compaction ability and sintering ability. Nanoparticles which are deposited on the surface of micro-powder are advantageous for a rigid die compaction while spherical micro-powder is not to be compacted. Additionally, double step sintering behavior is observed for the powder in the dilatometry of cylindrical compact body. Earlier shrinkage peak comes from the sintering of nanoparticle and later one results from the micro-powder sintering. Microstructure as well as phase composition of the sintered body is investigated.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1155-1158
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Quantitative Analysis of Cryomilled Nanocrystalline Ti-6Al-4V Alloy Powder by X-Ray Diffraction
Autorzy:
Oh, M.
Yu, H. K.
Lee, J.-H.
Oh, M. C.
Jung, S.-H.
Ahn, B.
Powiązania:
https://bibliotekanauki.pl/articles/356265.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nanocrystalline
cryomilling
Ti alloy
X-ray diffraction
size-strain plot method
Opis:
A nanocrystalline Ti alloy powder was fabricated using cryomilling. The grain size and lattice strain evolution during cryomilling were quantitatively analyzed using X-ray diffraction (XRD) based on the Scherrer equation, Williamson-Hall (W-H) plotting method, and size-strain (S-S) method assuming uniform deformation. Other physical parameters including stress and strain have been calculated. The average crystallite size and the lattice strain evaluated from XRD analysis are in good agreement with the result of transmission electron microscopy (TEM).
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1439-1442
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Compositional Dependence of Hardness of Ge-Sb-Se Glass for Molded Lens Applications
Zależność stężeniowa twardości szkła Ge-Sb-Se do zastosowań na formowane soczewki
Autorzy:
Park, J. K.
Lee, J. H.
Shin, S. Y.
Yi, J. H.
Lee, W. H.
Park, B. J.
Choi, J. H.
Kim, N. Y.
Choi, Y. G.
Powiązania:
https://bibliotekanauki.pl/articles/352228.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
chalcogenide glasses
Ge-Sb-Se glass
infrared lens
molded lens
infrared camera
szkło
Ge-Sb-Se
soczewki formowane
twardość szkła
kamera termowizyjna
Opis:
Chalcogenide glass in the ternary Ge-Sb-Se system is inherently moldable, thus being considered as a strong candidate material for use in infrared-transmitting lens applications from the viewpoint of thermal and mechanical stability. In an effort to experimentally determine compositional region suitable for the molded lens applications, we evaluate its compositional dependence of hardness. Among the constituent atoms, Ge content turns out to exert a most conspicuous correlation with hardness. This phenomenological behavior is then explained in connection with the structural evolution that Ge brings about.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1205-1208
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Evolution Of Precipitate Morphology During Extrusion In Mg ZK60A Alloy
Ewolucja morfologii wydzieleń podczas wytłaczania stopu Mg ZK60A
Autorzy:
Park, J.
Jung, K. H.
Lee, G. A.
Kawasaki, M.
Ahn, B.
Powiązania:
https://bibliotekanauki.pl/articles/356233.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnesium alloy
ZK60A
precipitation
extrusion
stopy magnezu
wydzielenia
wytłaczanie
Opis:
In this study, a continuously casted ZK60A magnesium alloy (Mg-Zn-Zr) was extruded in two different extrusion ratios, 6:1 and 10:1. The evolution of precipitates was investigated on the two extruded materials and compared with that of as-casted material. The microstructural analysis was performed by electron backscatter diffraction and transmission electron microscopy, and the compositional information was obtained using energy-dispersive X-ray spectroscopy. Several distinct morphologies of precipitates were observed, such as dot, rod, and disk shaped. The formation mechanisms of those precipitates were discussed with respect to the heat and strain during the extrusion process.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1423-1426
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
CO Oxidation Properties Of Selective Dissoluted Metallic Glass Composites
Utlenianie wybranych rozcieńczonych kompozytów szkieł metalicznych
Autorzy:
Kim, S. Y.
Lee, M. H.
Kim, T. S.
Kim, B. S.
Powiązania:
https://bibliotekanauki.pl/articles/355092.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
CO oxidation
metallic glasses
porous metal
catalyst materials
utlenianie
szkło metaliczne
metale porowate
materiał katalityczny
Opis:
Porous metallic materials have been widely used in many fields including aerospace, atomic energy, electro chemistry and environmental protection. Their unique structures make them very useful as lightweight structural materials, fluid filters, porous electrodes and catalyst supports. In this study, we fabricated Ni-based porous metallic glasses having uniformly dispersed micro meter pores by the sequential processes of ball-milling and chemical dissolution method. We investigated the application of our porous metal supported for Pt catalyst. The oxidation test was performed in an atmosphere of 1% CO and 3% O2. Microstructure observation was performed by using a scanning electron microscope. Oxidation properties and BET (Brunauer, Emmett, and Teller) were analyzed to understand porous structure developments. The results indicated that CO Oxidation reaction was dependent on the specific surface area.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1227-1229
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermal Conductivity and Microstructure of Copper Coated Graphite Composite by Spark Plasma Sintering Process
Autorzy:
Park, S. H.
Kim, D. B.
Lee, R. G.
Son, I. J.
Powiązania:
https://bibliotekanauki.pl/articles/355632.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metal matrix composites
thermal conductivity
thermal expansion
interfacial bonding
spark plasma sintering
Opis:
This study focuses on the fabrication of thermal management material for power electronics applications using graphite flake reinforced copper composites. The manufacturing route involved electroless plating of copper in the graphite flake and sintering process are optimized. The microstructures, interface, thermal properties, and relative density of graphite/Cu composites are investigated. The relative density of the composites shows 99.5% after sintering. Thermal conductivities and coefficients of thermal expansion of this composites were 400-480 Wm-1K-1 and 8 to 5 ppm k-1, respectively. Obtained graphite nanoplatelets-reinforced composites exhibit excellent thermo-physical properties to meet the heat dispersion and matching requirements of power electronic devices to the packaging materials.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1303-1306
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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