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Wyświetlanie 1-15 z 45
Tytuł:
Extraction Factor Of Pure Ammonium Paratungstate From Tungsten Scraps
Współczynnik ekstrakcji czystego parawolframianu amonu z odpadów wolframowych
Autorzy:
Pee, J-H.
Kim, G. H.
Lee, H. Y.
Kim, Y. J.
Powiązania:
https://bibliotekanauki.pl/articles/356567.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
raw material
recycling
ammonium paratungstate
tungsten scraps
extraction
surowce
recykling
parawolfrawian amonu
odpady wolframowe
ekstrakcja
Opis:
Typical oxidation process of tungsten scraps was modified by the rotary kiln with oxygen burner to increase the oxidation rate of tungsten scraps. Also to accelerate the solubility of solid oxidized products, the hydrothermal reflux method was adapted. By heating tungsten scraps in rotary kiln with oxygen burner at around 900° for 2hrs, the scraps was oxidized completely. Then oxidized products (WO3 and CoWO4) was fully dissolved in the solution of NaOH by hydrothermal reflux method at 150° for 2hrs. The dissolution rate of oxidized products was increased with increasing the reaction temperature and concentration of NaOH. And then CaWO4 and H2WO4 could be generated from the aqueous sodium tungstate solution. Ammonium paratungstate (APT) also could be produced from tungstic acid using by aqueous ammonium solution. The morphologies (cubic and plate types) of APT was controlled by the stirring process of purified solution of ammonium paratungstate.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1403-1405
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Extraction Factor Of Tungsten Sources From Tungsten Scraps By Zinc Decomposition Process
Współczynnik ekstrakcji związków wolframu z odpadów wolframowych w procesie rozkładu cynku
Autorzy:
Pee, J-H.
Kim, G. H.
Lee, H. Y.
Kim, Y. J.
Powiązania:
https://bibliotekanauki.pl/articles/354774.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
raw material
recycling
zinc decomposition process
tungsten carbide
tungstic acid
surowce
recykling
proces rozkładu cynku
węglik wolframu
kwas wolframowy
Opis:
Decomposition promoting factors and extraction process of tungsten carbide and tungstic acid powders in the zinc decomposition process of tungsten scraps which are composed mostly of tungsten carbide and cobalt were evaluated. Zinc volatility was suppressed by the enclosed graphite crucible and zinc volatilization pressure was produced in the reaction graphite crucible inside an electric furnace for ZDP (Zinc Decomposition Process). Decomposition reaction was done for 2hours at 650°, which 100% decomposed the tungsten scraps that were over 30 mm thick. Decomposed scraps were pulverized under 75μm and were composed of tungsten carbide and cobalt identified by the XRD (X-ray Diffraction). To produce the WC(Tungsten Carbide) powder directly from decomposed scraps, pulverized powders were reacted with hydrochloric acid to remove the cobalt binder. Also to produce the tungstic acid, pulverized powders were reacted with aqua regia to remove the cobalt binder and oxidize the tungsten carbide. Tungsten carbide and tungstic acid powders were identified by XRD and chemical composition analysis.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1311-1314
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of SiC Particles On Sinterability Of Al-Zn-Mg-Cu P/M Alloy
Wpływ cząstek SiC na spiekalność proszku stopowego Al-Zn-Mg-Cu
Autorzy:
Rudianto, H.
Jang, G. J.
Yang, S. S.
Kim, Y. J.
Dlouhy, I.
Powiązania:
https://bibliotekanauki.pl/articles/351304.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metal matrix composites
powder metallurgy
sintering
heat treatment
kompozyty metalowe
metalurgia proszków
spiekanie
obróbka cieplna
Opis:
Premix Al-5.5Zn-2.5Mg-0.5Cu alloy powder was analyzed as matrix in this research. Gas atomized powder Al-9Si with 20% volume fraction of SiC particles was used as reinforcement and added into the alloy with varied concentration. Mix powders were compacted by dual action press with compaction pressure of 700 MPa. High volume fraction of SiC particles gave lower green density due to resistance of SiC particles to plastic deformation during compaction process and resulted voids between particles and this might reduce sinterability of this mix powder. Sintering was carried out under ultra high purity nitrogen gas from 565°-580°C for 1 hour. High content of premix Al-5.5Zn-2.5Mg-0.5Cu alloy powder gave better sintering density and reached up to 98% relative. Void between particles, oxide layer on aluminum powder and lower wettability between matrix and reinforcement particles lead to uncompleted liquid phase sintering, and resulted on lower sintering density and mechanical properties on powder with high content of SiC particles. Mix powder with wt90% of Alumix 431D and wt10% of Al-9Si-vf20SiC powder gave higher tensile strength compare to another mix powder for 270 MPa. From chemical compositions, sintering precipitates might form after sintering such as MgZn2, CuAl2 and Mg2Si. X-ray diffraction, DSC-TGA, and SEM were used to characterize these materials.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1383-1385
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Analysis Of The Extrusion Process Of A Square Tube Multi-Channel Heat Pipe
Analiza procesu wytłaczania wielokanałowych ciepłowodów o kwadratowym przekroju
Autorzy:
Kim, K. S.
Kim, J. Y.
Powiązania:
https://bibliotekanauki.pl/articles/353935.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum hot extrusion
FE simulation
stress analysis
extrusion experiment
aluminium wytłaczane na gorąco
symulacja FE
analiza naprężeń
wytłaczanie
Opis:
Heat pipes have been recently in use for cooling purposes in various fields, including electronic circuit boards and vehicle parts that generate large amounts of heat. In order to minimize the loss of heat transferred, there is a need to maximize the contact area of the working fluid. This study produced a square tube multi-channel heat pipe to replace the existing circular pipe type to maximize the internal surface area thereof. This expands the surface, allowing the working fluid to come into contact with a wider area and enhancing thermal radiation performance. A mold for the production for such a product was designed, and finite element simulation was performed to determine whether production is possible.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1463-1466
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis And Characterization Of SiO2, SnO2 And TiO2 Metal Oxide Shells Covering Cu2O Particles
Synteza i charakterystyka powłok tlenkowych SiO2, SnO2 i TiO2 pokrywających cząstki Cu2O
Autorzy:
Yu, R.
Yun, J.
Kim, Y.
Powiązania:
https://bibliotekanauki.pl/articles/355566.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Cu2O
metal oxide coating
pH value
SiO2
TiO2
SnO2
powłoki tlenkowe
Opis:
In this work is described a means of improving the chemical stability of Cu2O@SiO2, Cu2O@SnO2 and Cu2O@TiO2 materials. The SiO2, SnO2 and TiO2 coated samples were stable from pH 3 to pH 10 for up to seven days. To determine the stability of the coated nanoparticles, and their colloidal solutions under acidic and basic conditions, colloidal nanoparticle solutions with various pH values were prepared and monitored over time. Details of the effect of variations in pH on the phase stability of core-shell type Cu2O were characterized using transmission electron microscopy and X-ray diffraction.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1159-1163
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Characterization of Black CoFe2O4 Pigments Using MOOH (M = Fe and Co) Nanorod
Autorzy:
Yu, R.
Yun, J.
Kim, Y.
Powiązania:
https://bibliotekanauki.pl/articles/355743.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
β-Co/FeOOH
CoFe2O4
black pigment
substitution
solid solution
Opis:
We studied the coloration and phase transformation of various iron based pigment with cobalt substitution method and heat treatment. First, we synthesized well defined one dimension β-Fe/CoOOH nanorods using the solid solution method. Yellowish β-Fe/CoOOH nanorods were transformed into reddish intermediate states and, finally, black CoFe2 O4 pigments was obtained. Divalent cobalt ions easily occupied tetrahedral sites. The prepared pigments were well characterized in terms of physical properties by using UV-vis, CIE Lab color parameter measurements, SEM (scanning electron microscopy) and XRD (powder X-ray diffraction). In addition, the magnetization property of the prepared CoFe2 O4 pigment was confirmed by VSM (vibrating sample magnetometer).
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1231-1234
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Experimental Study On Fracture Property Of Tapered Double Cantilever Beam Specimen With Aluminum Foam
Doświadczalne badanie pękania mimośrodowo rozciąganej zwężanej próbki z bocznym karbem wykonanej z piany aluminiowej
Autorzy:
Kim, Y. C.
Kim, S. S.
Cho, J. U.
Powiązania:
https://bibliotekanauki.pl/articles/352697.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum foam
tapered double cantilever beam (TDCB)
fracture behavior
adhesively bonded structures
adhesive fracture energy
piana aluminiowa
pękanie
stożkowa podwójna belka wspornikowa
struktura sklejona
Opis:
It is indispensable to evaluate fracture energy as the bonding strength of adhesive at composite material with aluminum foam. This specimen is designed with tapered double cantilever beam by British standards (BS 7991 and ISO 11343). 4 kinds of specimens due to m values of 2, 2.5, 3 and 3.5 are manufactured and compared each other with the experimental results. Adhesive fracture energy is calculated from the formulae of British standards. The value of m is the gradient which is denoted as the length and the height of specimen. As m becomes greater at static experimental result, the maximum load becomes higher and the displacement becomes lower. And the critical fracture energy becomes higher. As m becomes less at fatigue experimental result, the displacement becomes higher and the critical fracture energy becomes higher. Fracture behavior of adhesive can be analyzed by this study and these experimental results can be applied into real field effectively. The stability on TDCB structure bonded with aluminum foam composite can be predicted by use of this experimental result. Adhesive fracture energy is calculated from the formulae of British standards. Based on correlations obtained in this study, the fracture behavior of bonded material would possibly be analyzed and aluminum foam material bonded with adhesive would be applied to a composite structure in various fields, thereby analyzing the mechanical and fracture characteristic of the material.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1459-1462
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study on Effects of Mold Temperature on the Injection Molded Article
Autorzy:
Han, J.-H.
Kim, Y.-C.
Powiązania:
https://bibliotekanauki.pl/articles/351919.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
injection molding
mold temperature
cooling temperature
molded article
Opis:
This is a study of the effects of temperature of injection mold on the injection molded article. By supplying water of the proper temperature in the cooling line of mold in the cooling process, the mold was the appropriate temperature, and the deformation of the injection molded article was examined according to the mold temperature. In this study, we conducted simulation analysis and experiments, and the results were analyzed. The minimum deformation of the injection molded article model obtained by supplying 50°C water in the cooling line is 0.003 mm, and the maximum deformation was 0.813 mm. Injection molded article models obtained by supplying 20°C water were found to be a minimum of 0.002 mm, with deformation of up to 0.761 mm. When comparing both conditions, the error rate of injection molded article obtained by supplying 20°C water in the mold cooling line was lower by about 0.18%.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1271-1274
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spontaneous Formation of Titanium Nitride on the Surface of a Ti Rod Induced by Electro-Discharge-Heat-Treatment in an N2 Atmosphere
Autorzy:
Lee, W. H.
Yoon, Y. H.
Kim, Y. H.
Lee, Y. K.
Kim, J. Y.
Chang, S. Y.
Powiązania:
https://bibliotekanauki.pl/articles/352477.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
surface modification
diffusion
heat treatment
XPS
Opis:
A single pulse of 2.0 to 3.5 kJ of input energy from a 450 mF capacitor was applied to a commercially pure Ti rod in a N2 atmosphere. The surface of the Ti rod transformed from TiO2 into titanium nitride in times as short as 159 msec, providing a bimodal morphology of the cross-section. A much higher value of hardness that was observed at the edge of the cross-section was attributed to nitrogen-induced solid-solution hardening that occurred during the electrical discharge process. The activation energy (Ea) for the diffusion process was estimated to be approximately 86.9 kJ/mol. Results show that the electrical discharge process is a possible potential method for the nitriding of Ti; advantages include a short processing time and control of the nitrided layer without dimensional changes.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1281-1285
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Modification of Self-Consolidated Microporous Ti Implant Compacts Fabricated by Electro-Discharge-Sintering in Air
Autorzy:
Jo, Y. J.
Yoon, Y. H.
Kim, Y. H.
Chang, S. Y.
Kim, J. Y.
Lee, Y. K.
Van Tyne, C. J.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/356790.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
implant
porous
sintering
X-ray photoelectron spectroscopy (XPS)
Opis:
A single pulse of 0.75-2.0 kJ/0.7g of atomized spherical Ti powders from 300 mF capacitor was applied to produce a microporous Ti implant compact by electro-discharge-sintering (EDS). A solid core in the middle of the compact surrounded by a microporous layer was found. X-ray photoelectron spectroscopy was employed to study the surface characteristics of the EDS Ti compact and it revealed that Ti, C and O were the main constituents on the surface with a smaller amount of N. The surface was lightly oxidized and was primarily in the form of TiO2 resulting from the air oxidation during EDS processing. The lightly oxidized surface of the EDS compact also exhibited Ti nitrides such as TiN and TiON, which revealed that the reaction between air constituents and the Ti powders even in times as short as 128 msec.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1287-1291
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Heat Treatment on the Microstructure and Tensile Deformation Behavior of Oxide Dispersion Strengthened Alloys Manufactured by Complex Milling Process
Autorzy:
Kim, Y.-K.
Kim, J.-H.
Gwon, J.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352535.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ball milling
oxide dispersion strengthening
microstructure
tensile deformation behavior
Opis:
This study attempted to manufacture an ODS alloy by combining multiple milling processes in mechanical alloying stage to achieve high strength and fracture elongation. The complex milling process of this study conducted planetary ball milling, cryogenic ball milling and drum ball milling in sequential order, and then the microstructure and tensile deformation behavior were investigated after additional heat treatment. The oxide particles distributed within the microstructure were fine oxide particles of 5~20 nm and coarse oxide particles of 100~200 nm, and the oxide particles were confirmed to be composed of Cr, Ti, Y and O. Results of tensile tests at room temperature measured yield strength, tensile strength and elongation as 1320 MPa, 2245 MPa and 4.2%, respectively, before heat treatment, and 1161 MPa, 2020 MPa and 5.5% after heat treatment. This results indicate that the ODS alloy of this study gained very high strengths compared to other known ODS alloys, allowing greater plastic zones.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1335-1340
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Self-Consolidation Mechanism of Ti5Si3 Compact Obtained by Electro-Discharge-Sintering Directly from Physically Blended Ti-37.5 At.% Si Powder Mixture
Autorzy:
Chang, S. Y.
Cheon, Y. W.
Yoon, Y. H.
Kim, Y. H.
Kim, J. Y.
Lee, Y. K.
Lee, W. H.
Powiązania:
https://bibliotekanauki.pl/articles/353022.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
sintering
mechanical alloying
powder consolidation
intermetallic compounds
titanium silicide
Opis:
Characteristics of electro-discharge-sintering of the Ti-37.5at.% Si powder mixture was investigated as a function of the input energy, capacitance, and discharge time without applying any external pressure. A solid bulk of Ti5Si3 was obtained only after in less than 129 μsec by the EDS process. During a discharge, the heat is generated to liquefy and alloy the particles, and which enhances the pinch pressure can condensate them without allowing a formation of pores. Three step processes for the self-consolidation mechanism during EDS are proposed; (a) a physical breakdown of oxide film on elemental as-received powder particles, (b) alloying and densifying the consolidation of powder particles by the pinch pressure, and (c) diffusion of impurities into the consolidated surface.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1299-1302
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of AZ31/CNT Surface Nano-composite by Double-pass Friction Stir Processing
Autorzy:
Kim, J. Y.
Hwang, J.-W.
Kim, H. Y.
Lee, S. M.
Jung, W.-S.
Byeon, J.-W.
Powiązania:
https://bibliotekanauki.pl/articles/355624.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
surface modification
Double-pass Friction Stir Processing
AZ31
composite
CNT
Opis:
Double-pass Friction Stir Processing (FSP) was applied to fabricate an AZ31/CNT nano-composite for surface hardening of lightweight structural components. The effects of double-pass FSP as well as groove depth (i.e., volume fraction of CNT) on the CNT distribution, dynamically recrystallized grain size, and resulting microhardness were studied. Double-pass FSP was performed for the CNT-filled plate-type specimen with different groove depths of 2, 3, and 4 mm. By applying double-pass FSP, the average size of CNT clusters decreased, implying a more homogeneous distribution. Compared with the FSPed specimen without CNT, grain size was refined from 19 μm to 3 μm and microhardness increased from 52 Hv to 83 Hv (i.e., 71% increase).
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1039-1042
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Design Of A Bi-Functional α-Fe2O3/Zn2SiO4:Mn2+ By Layer-By-Layer Assembly Method
Projektowanie dwufunkcyjnych proszków α-Fe2O3/Zn2SiO4:Mn2+ metodą warstwa po warstwie
Autorzy:
Yu, R.
Yun, J.
Pee, J-H.
Kim, Y.
Powiązania:
https://bibliotekanauki.pl/articles/352623.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
red pigment
α-Fe2O3
Zn2SiO4:Mn2+ layer
phosphor
bi-functional
czerwony pigment
Zn2SiO4: Mn2+
fosfor
proszki dwufunkcyjne
Opis:
This work describes the design of bi-functional α-Fe2O3/Zn2SiO4:Mn2+ using a two-step coating process. We propose a combination of pigments (α-Fe2O3) and phosphor (Zn2SiO4:Mn2+ ) glaze which is assembled using a layer-by-layer method. A silica-coated α-Fe2O3 pigment was obtained by a sol-gel method and a Zn2+ precursor was then added to the silica-coated α-Fe2O3 to create a ZnO layer. Finally, the Zn2SiO4:Mn2+ layer was prepared with the addition of Mn2+ ions to serve as a phosphor precursor in the multi-coated α-Fe2O3, followed by annealing at a temperature above 1000°C. Details of the phase structure, color and optical properties of the multi-functional α-Fe2O3/Zn2SiO4:Mn2+ were characterized by transmission electron microscopy and X-ray diffraction analyses.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1165-1167
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Hafnium and Zirconium to Glass Forming Ability, Thermal Stability, Plasticity Deformation and Crystallization of Ni-Free Pentabasic Ti-Based Bulk Metallic Glasses
Autorzy:
Oak, J.-J.
Kim, Y. H.
Bae, K.-C.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/352087.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti-based alloy
metallic glass
Ti fiber
glass formability
plastic deformation
Opis:
The newly designed Ti-based bulk metallic glass (BMG) in which case of fracture behavior was observed 1990MPa to compressive strength with a wide plastic deformation around 7% after process of elastic deformation. This phenomenon can be compared with those of Ti-based alloys and other Ti-based BMGs and indicates high potential to be applied in use. It was evaluated the Ti-based BMG for thermal stability that the reduced glass parameters, ΔTx, Trg and γ, are 79K, 0.50 and 0.38, respectively. In addition, it reveals high activation energies for crystallization in which are estimated to Ex1 = 291.77 ±9.71 kJ/mol, Ex2 = 588.77 ±28.88 kJ/mol and Ex3 = 330.26 ±3.61 kJ/mol on kissinger plotting in this study.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1081-1087
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 45

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