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Wyświetlanie 1-15 z 35
Tytuł:
Evaluation of Carbides in Turbine Blade Made of IN713C Superalloy After Hot Isostatic Pressing
Autorzy:
Kościelniak, B.
Roskosz, S.
Cwajna, J.
Powiązania:
https://bibliotekanauki.pl/articles/351248.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
IN713C superalloy
hot isostatic pressing
turbine blades
qualitative and quantitative analysis of carbides
Opis:
The IN713C is nickel-based superalloy, used to produce low pressure turbine blades in a process of investment casting. However, porosity which is formed during the casting, decreases mechanical properties of IN713C. Therefore, to eliminate porosity, a process of hot isostatic pressing was applied. Nonetheless, HIP also least to some changes in the microstructure of tested material. The main aim of this paper is to characterize the morphology of carbides before and after hot isostatic pressing. Microstructural characterization was carried out with the use of a scanning electron microscope equipped with an energy dispersive X-ray spectrometer and an electron backscatter diffraction detector. The size and shape of carbides were evaluated by quantitative metallography methods methods. The results show that the amount, size and heterogeneity of arrangement of the carbides increased after application of HIP treatment.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 247-252
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Impact Characteristic According to the Structure of Crash Box at the Vehicle
Autorzy:
Min, B. S.
Cho, J. U.
Powiązania:
https://bibliotekanauki.pl/articles/355072.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminum foam
crash box
impact characteristic
deformation
stress
internal energy
durability
Opis:
The crash box between a bumper and a car body in automobiles can reduce impacts for car bodies with a bumper at a low-speed collision by preventing the shocks. Also, this crash box is the part playing a very important role for the safety of vehicle and the reduction of repair cost, and many studies have been investigated for the performance. In this study, aluminum foam was inserted in an aluminum crash box to analyze the relationships of deformation, stress and internal energy. The compression characteristics are compared with six cases. In addition, the load due to displacement at experiment for a case is verified by modeling with finite elements and performing the structural analysis. As these study results for investigating characteristics of the crash box, it is thought that the effective designs of crash box to enhance the durability for collision are made possible.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1047-1050
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Milling Time Parameter on the Microstructure and the Thermoelectric Properties of n-Type Bi2Te2.7Se0.3 Alloys
Autorzy:
Sharief, P.
Madavali, B.
Koo, J. M.
Kim, H. J.
Hong, S.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/354418.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ball milling
milling time
microstructure
thermoelectric properties
ZT
Opis:
Nanostructured thermoelectric materials receiving great attention for its high thermoelectric performance. In this research, nanostructured n-type Bi2 Te2.7 Se0.3 alloys have prepared using high energy ball milling and followed by spark plasma sintering. Also, we have varied ball milling time to investigate milling time parameter on the thermoelectric properties of n-type Bi2 Te2.7 Se0.3 powder. The powders were discrete at 10 min milling and later particles tend to agglomerate at higher milling time due to cold welding. The bulk fracture surface display multi-scale grains where small grains intersperse in between large grains. The maximum Seebeck coefficient value was obtained at 20-min milling time due to their lower carrier density. The κ values were decreased with increasing milling time due to the decreasing trend observed in their κL values. The highest ZT of 0.7 at 350 K was observed for 30-min milling time which was ascribed to its lower thermal conductivity. The Vickers hardness values also greatly improved due to their fine microstructure.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 2; 585-590
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Multistep Heat-Treatment Effects on Electrospun Nd-Fe-B-O Nanofibers
Autorzy:
Jeon, E. J.
Eom, N. S. A.
Lee, J.
Lee, B.
Cho, H. M.
On, J. S.
Choa, Y.-H
Kim, B. S.
Powiązania:
https://bibliotekanauki.pl/articles/354311.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nd-Fe-B
nanofibers
electrospinning
heat treatment
Opis:
Neodymium-Iron-Boron (Nd-Fe-B) magnets are considered to have the highest energy density, and their applications include electric motors, generators, hard disc drives, and MRI. It is well known that a fiber structure with a high aspect ratio and the large specific surface area has the potential to overcome the limitations, such as inhomogeneous structures and the difficulty in alignment of easy axis, associated with such magnets obtained by conventional methods. I n this work, a suitable heat-treatment procedure based on single-step and multistep treatments to synthesize sound electrospun Nd-Fe-B-O nanofibers of Φ572 nm was investigated. The single-step heat-treated (directly heat-treated at 800°C for 2 h in air) samples disintegrated along with the residual organic compounds, whereas the multistep heat-treated (sequential three-step heat-treated including three steps;: dehydration (250°C for 30 min in an inert atmosphere), debinding (650°C for 30 min in air), and calcination (800°C for 1 h in air)) fibers maintained sound fibrous morphology without any organic impurities. They could maintain such fibrous morphologies during the dehydration and debinding steps because of the relatively low internal pressures of water vapor and polymer, respectively. In addition, the NdFeO3 alloying phase was dominant in the multistep heat-treated fibers due to the removal of barriers to mass transfer in the interparticles.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1433-1437
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of the Microstructure and Thermoelectric Properties of P-Type BiSbTe Alloys by Usage of Different Revolutions Per Minute (RPM) During Mechanical Milling
Autorzy:
Yoon, S.-M.
Madavali, B.
Yoon, Y.-N.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/354749.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Bi0.5Sb1.5Te3 alloys
mechanical alloying
spark plasma sintering
thermoelectric properties
Opis:
In this work, p-type Bi0.5Sb1.5Te3 alloys were fabricated by high-energy ball milling (MA) and spark plasma sintering. Different revolutions per minute (RPM)s were used in the MA process, and their effect on microstructure, and thermoelectric properties of p-type Bi0.5Sb1.5Te3 were systematically investigated. The crystal structure of milled powders and sintered samples were characterized using X-ray diffraction. All the powders exhibited the same morphology albeit with slight differences find at 1100 RPM conditions. A slight grain size refinement was observed on the fracture surfaces from 500 to 1100 RPM specimens. The temperature dependence of Seebeck coefficient, electrical conductivity, and power factors were measured as a function of temperature with different RPM conditions. The power factor shows almost same (~3.5 W/mK2 at RT) for all samples due to unchanged Seebeck and electrical conductivity values. The peak ZT of 1.07 at 375K is obtained for 1100 RPM specimen due to low thermal conductivity.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1167-1171
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Ga2O3 Nanoparticles Dispersion on Microstructure and Thermoelectric Properties of p-Type BiSbTe Based Alloys
Autorzy:
Kim, E.-B.
Koo, J.-M.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/351366.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
thermoelectric properties
Bi0.5Sb1.5Te3 alloys
Seebeck coefficient
mechanical alloying
spark plasma sintering
Opis:
In this study, p-type Bi0.5Sb1.5Te3 based nanocomposites with addition of different weight percentages of Ga2O3 nanoparticles are fabricated by mechanical milling and spark plasma sintering. The fracture surfaces of all Bi0.5Sb1.5Te3 nanocomposites exhibited similar grain distribution on the entire fracture surface. The Vickers hardness is improved for the Bi0.5Sb1.5Te3 nanocomposites with 6 wt% added Ga2O3 due to exhibiting fine microstructure, and dispersion strengthening mechanism. The Seebeck coefficient of Bi0.5Sb1.5Te3 nanocomposites are significantly improved owing to the decrease in carrier concentration. The electrical conductivity is decreased rapidly upon the addition of Ga2O3 nanoparticle due to increasing carrier scattering at newly formed interfaces. The peak power factor of 3.24 W/mK2 is achieved for the base Bi0.5Sb1.5Te3 sintered bulk. TheBi0.5Sb1.5Te3 nanocomposites show low power factor than base sample due to low electrical conductivity.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 993-997
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Secondary steel refining for continuous sequence bloom casting for high oxide cleanness final products
Rafinacja pozapiecowa ciekłej stali do ciągłego sekwencyjnego odlewania z przeznaczeniem na wyroby o dużej czystości tlenkowej
Autorzy:
Zdonek, B.
Szypuła, I.
Kozłowski, J.
Szczęch, S.
Powiązania:
https://bibliotekanauki.pl/articles/354603.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
rafinacja
czystość tlenkowa
odlewanie sekwencyjne
secondary refining
oxide cleanness
sequence continuous casting
Opis:
Steelmaking and secondary refining process technology of resulphurized liquid steel with low content of total oxygen, assigned for continuous casting of strands for rolled and forged products for automotive industry was developed. The influence of secondary steel refining parameters on total oxygen content as well as amount and morphology of non-metallic inclusions was examined. It was found, that content of total oxygen and amount of non-metallic inclusions in steel decrease as steel refining time in the ladle becomes longer, and the chemical composition of non-metallic inclusions in steel changes from modified calcium aluminates to spinel inclusion of CaOźAl2O3źMgO type. The total oxygen content in steel from continuous casting in four cast sequence ranged from 6 to 25 ppm, with percentage share of non-metallic inclusions from 0.09 to 0.30 per cent and equivalent diameter 0.78 to 1.59 µm.
Opracowano technologię wytapiania i rafinacji pozapiecowej ciekłej stali z regulowaną zawartością siarki, z niską zawartością tlenu całkowitego, przeznaczoną do odlewania w sekwencji wlewków ciągłych na wyroby walcowane i kute dla przemysłu motoryzacyjnego. Zbadano wpływ parametrów technologicznych rafinacji pozapiecowej stali na zawartość tlenu całkowitego oraz na ilość i morfologię wtrąceń niemetalicznych. Stwierdzono, że zawartość tlenu całkowitego w stali oraz liczność wtrąceń niemetalicznych zmniejszają się w miarę wydłużania czasu rafinacji stali w kadzi, a skład chemiczny wtrąceń niemetalicznych zmienia się ze zmodyfikowanych glinianów wapnia we wtrącenia spinelowe typu CaOźAl2O3ź MgO. Zawartości tlenu całkowitego w stali odlewanej w cztero wytopowej sekwencji wynosiły od 6 do 25 ppm, przy procentowym udziale wtrąceń niemetalicznych - od 0,09 do 0,30 % i średnicy równoważnej od 0,78 do 1,59 µm.
Źródło:
Archives of Metallurgy and Materials; 2012, 57, 1; 347-353
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication and Characterization of CoCrFeNiMn High Entropy Alloy Powder Processed by Gas Atomization
Autorzy:
Park, T. G.
Lee, S. H.
Lee, B.
Cho, H. M.
Choi, W. J.
Kim, B. S.
Shin, K. S.
Kim, T.-S.
Powiązania:
https://bibliotekanauki.pl/articles/353649.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
high entropy alloy
gas atomization
spark plasma sintering
CoCrFeNiMn
Opis:
In this study, precisely controlled large scale gas atomization process was applied to produce spherical and uniform shaped high entropy alloy powder. The gas atomization process was carried out to fabricate CoCrFeNiMn alloy, which was studied for high ductility and mechanical properties at low temperatures. It was confirmed that the mass scale, single phase, equiatomic, and high purity spherical high entropy alloy powder was produced by gas atomization process. The powder was sintered by spark plasma sintering process with various sintering conditions, and mechanical properties were characterized. Through this research, we have developed a mass production process of high quality and spherical high entropy alloy powder, and it is expected to expand applications of this high entropy alloy into fields such as powder injection molding and 3D printing for complex shaped components.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1055-1059
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of Non-Metallic Inclusions Formed as a Result of Deoxidation on the Fatigue Strength of 15CrNi6 and 16MnCr5 Steel
Autorzy:
Lipa, S.
Sawicki, J.
Dybowski, K.
Pietrasik, R.
Januszewicz, B.
Powiązania:
https://bibliotekanauki.pl/articles/353324.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
fatigue strength
non-metallic inclusions
thermo-chemical treatment
Opis:
This paper presents the findings of fatigue strength tests of 15CrNi6 steel following low-pressure carburizing and oil quenching, subjected to cycles of one-sided three-point bending. The fatigue fractures were compared with the results of fatigue strength studies of 16MnCr5 steel following low-pressure carburizing and nitrogen quenching. The fatigue tests for 16MnCr5 steel were conducted as part of a high-cycle resonance test, with a pendular bending load. The study also involved an analysis of the effects on non-metallic inclusions in the structure on the mechanism of fatigue destruction. The inclusions were found to initiate fatigue cracks. In both cases, a similar method of a fatigue fissure initiation was observed, independent of the study method or specimen material.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1345-1350
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of a Spherical Titanium Powder by Combined Combustion Synthesis and DC Plasma Treatment
Autorzy:
Choi, S. H.
Ali, B.
Hyun, S. K.
Sim, J. J.
Choi, W. J.
Joo, W.
Lim, J. H.
Lee, Y. J.
Kim, T. S.
Park, K. T.
Powiązania:
https://bibliotekanauki.pl/articles/356067.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
combustion synthesis
DC plasma treatment
titanium powder
3D printing process
combustion parameters
Opis:
Combustion synthesis is capable of producing many types of refractory and ceramic materials, as well as metals, with a relatively lower cost and shorter time frame than other solid state synthetic techniques. TiO2 with Mg as reductant were dry mixed and hand compacted into a 60 mm diameter mold and then combusted under an Ar atmosphere. Depending on the reaction parameters (Mg concentration 2 ≤ α ≤ 4), the thermocouples registered temperatures between 1160°C and 1710°C . 3 mol of Mg gave the optimum results with combustion temperature (Tc) and combustion velocity (Uc) values of 1372°C and 0.26 cm/s respectively. Furthermore, this ratio also had the lowest oxygen concentration in this study (0.8 wt%). After combustion, DC plasma treatment was carried out to spheroidize the Ti powder for use in 3D printing. The characterization of the final product was performed using X-ray diffraction, scanning electron microscopy, energy dispersive spectroscopy, and N/O analysis.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1057-1062
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect Of Different Mechanical Milling Processes On Morphology And Microstructural Changes Of Nano And Micron Al-Powders
Wpływ różnych procesów mielenia na morfologię i mikrostrukturę nanometrycznych i mikronowych proszków Al
Autorzy:
Kim, H.-S.
Madavali, B.
Eom, T.-J.
Kim, C.- M.
Koo, J.-M.
Lee, T. H.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/355715.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al alloys
high-energy ball milling
low energy ball milling
plastic deformation
stopy Al
wysokoenergetyczne mielenie kulkowe
mielenie energooszczędne
odkształcenia plastyczne
Opis:
In this research, effect of the various mechanical milling process on morphology and microstructural changes of nano and micron Al-powders was studied. The milling of Al-powders was performed by both high energy and low energy ball milling process. The influence of milling (pulverizing) energy on the structural changes of Al-powders was studied. Al-nanoparticles were agglomerated during the MA and its size was increased with increasing milling while micron Al-powder gets flattened shape during high energy ball milling due to severe plastic deformation. Meanwhile, structural evolution during high energy ball milling of the nano powder occurred faster than that of the micron powder. A slight shift in the position of X-ray diffraction peaks was observed in nano Al-powders but it was un-altered in macro Al-powders. The variation in lattice parameters was observed only for nano Al powders during the high energy ball milling due to lattice distortion.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1235-1239
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Fabrication of Fe-TiB2 Nanocomposites by Spark-Plasma Sintering of a (FeB, TiH2) Powder Mixture
Autorzy:
Huynh, X.-K.
Kim, B.-W.
Kim, J.-S.
Powiązania:
https://bibliotekanauki.pl/articles/351368.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-TiB2 nanocomposite
mechanical activation
spark plasma sintering
self-propagating high-temperature synthesis reaction
Opis:
Fe-40wt% TiB2 nanocomposites were fabricated by mechanical activation and spark-plasma sintering of a powder mixture of iron boride (FeB) and titanium hydride (TiH2). The powder mixture of (FeB, TiH2) was prepared by high-energy ball milling in a planetary ball mill at 700 rpm for 3 h followed by spark-plasma sintering (SPS) at various conditions. Analysis of the change in relative sintered density and densification rate during sintering showed that a self-propagating high-temperature synthesis reaction occurs to form TiB2 from FeB and Ti. A sintered body with relative density higher than 98% was obtained after sintering at 1150°C for 5 and 15 min. The microstructural observation of sintered compacts with the use of FE-SEM and TEM revealed that ultrafine particulates with approximately 5 nm were evenly distributed in an Fe-matrix. A hardness value of 83 HRC was obtained, which is equivalent to that of conventional WC-20 Co systems.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1043-1047
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Mechanical Activation on the in situ Formation of TiB2 Particulates in the Powder Mixture of TiH2 and FeB
Autorzy:
Huynh, X.-K.
Kim, B.-W.
Kim, J. S.
Powiązania:
https://bibliotekanauki.pl/articles/355844.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
mechanical activation
in situ formation
TiB2 particulate
Fe-matrix
specific ball-milling energy
Opis:
The in situ formation of TiB2 particulates via an interface reaction between Ti and FeB powders was studied. The effects of mechanical activation by high-energy milling on the decomposition of TiH2 and the interface reactions between Ti and FeB powders to form TiB2 were investigated. Powder mixtures were fabricated using planetary ball-milling under various milling conditions. The specific ball-milling energy was calculated from the measured electrical power consumption during milling process. High specific milling energy (152.6 kJ/g) resulted in a size reduction and homogeneous dispersion of constituent powders. This resulted in a decrease in the decomposition temperature of TiH2 and an increase in the formation reaction of TiB2 particulates in the Fe matrix, resulting in a homogeneous microstructure of nanoscale TiB2 evenly distributed within the Fe matrix. In contrast, the powder mixture milled with low specific milling energy (36.5 kJ/g) showed an inhomogeneous microstructure composed of relatively large Fe-Fe2 B particles surrounded by a thin layer of Fe-TiB2 within a finely dispersed Fe-TiB2 matrix region.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1393-1398
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Reduction of Thermal Conductivity Through Complex Microstructure by Dispersion of Carbon Nanofiber in p-Type Bi0.5Sb1.5Te3 Alloys
Autorzy:
Sharief, P.
Madavali, B.
Sohn, Y.
Han, J. H.
Song, G.
Hong, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/2049341.pdf
Data publikacji:
2021
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bismuth telluride
carbon nano fiber
grain size
Thermal conductivity
ZT
Opis:
The influence of nano dispersion on the thermoelectric properties of Bi2Te3 was actively investigating to wide-spread thermoelectric applications. Herein this report, we have systematically controlled the microstructure of Bi0.5Sb1.5Te3 (BST) alloys through the incorporation of carbon nanofiber (CNF), and studied their effect on thermoelectric properties, and mechanical properties. The BST/x-CNF (x-0, 0.05, 0.1, 0.2 wt.%) composites powder was fabricated using high energy ball milling, and subsequently consolidated the powder using spark plasma sintering. The identification of CNF in bulk composites was analyzed in Raman spectroscopy and corresponding CNF peaks were recognized. The BST matrix grain size was greatly reduced with CNF dispersion and consistently decreased along CNF percentage. The electrical conductivity was reduced and Seebeck coefficient varied in small-scale by embedding CNF. The thermal conductivity was progressively diminished, obtained lattice thermal conductivity was lowest compared to bare sample due to induced phonon scattering at interfaces of secondary phases as well as highly dense fine grain boundaries. The peak ZT of 0.95 achieved for 0.1 wt.% dispersed BST/CNF composites. The Vickers hardness value of 101.8 Hv was obtained for the BST/CNF composites.
Źródło:
Archives of Metallurgy and Materials; 2021, 66, 3; 803-808
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Surfactant Addition on Bi2Te3 Nanostructures Synthesized by Hydrothermal Method
Autorzy:
Dharmaiah, P.
Lee, C. H.
Madavali, B.
Hong, S.-J.
Powiązania:
https://bibliotekanauki.pl/articles/351609.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bismuth telluride
hydrothermal synthesis
spark plasma sintering
thermoelectric materials
X-ray diffraction
Opis:
In the present work, we have prepared Bi2Te3 nanostructures with different morphologies such as nano-spherical, nanoplates and nanoflakes obtained using various surfactant additions (EG, PVP, and EDTA) by a hydrothermal method. The shape of the nanoparticles can be controlled by addition of surfactants. The samples were characterized by x-ray diffraction (XRD) and scanning electron microscopy (SEM). It is found that the minority BiOCl phase disappears after maintained pH at 10 with EG as surfactant. SEM bulk microstructure reveals that the sample consists of fine and coarse grains. Temperature dependence of thermoelectric properties of the nanostructured bulk sample was investigated in the range of 300-450K. The presence of nanograins in the bulk sample exhibits a reduction of thermal conductivity and less effect on electrical conductivity. As a result, a figure of merit of the sintered bulk sample reached 0.2 at 400 K. A maximum micro Vickers hardness of 102 Hv was obtained for the nanostructured sample, which was higher than the other reported results.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1005-1010
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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