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    Wyświetlanie 1-9 z 9
    Tytuł:
    Thermal Analysis On The Kinetics Of Magnesium-Aluminum Layered Double Hydroxides In Different Heating Rates
    Analiza termiczna kinetyki rozkładu warstwowego podwójnego wodorotlenku magnezu aluminium przy różnych szybkościach grzania
    Autorzy:
    Hongbo, Y.
    Meiling, C.
    Xu, W.
    Hong, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/351862.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    layered double hydroxides
    thermal analysis
    kinetics
    warstwowy podwójny wodorotlenek
    analiza termiczna
    kinetyka
    Opis:
    The thermal decomposition of magnesium-aluminum layered double hydroxides (LDHs) was investigated by thermogravimetry analysis and differential scanning calorimetry (DSC) methods in argon environment. The influence of heating rates (including 2.5, 5, 10, 15 and 20K/min) on the thermal behavior of LDHs was revealed. By the methods of Kissinger and Flynn-Wall-Ozawa, the thermal kinetic parameters of activation energy and pre-exponential factor for the exothermic processes under non-isothermal conditions were calculated using the analysis of corresponding DSC curves.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1357-1359
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Synthesis Of Magnesium-Aluminum Layered Double Hydroxides By Mechanochemical Method And Its Solid State Reaction Kinetics
    Mechaniczno-chemiczna synteza warstwowego podwójnego wodorotlenku magnezu aluminium i kinetyka reakcji w stanie stałym
    Autorzy:
    Hongbo, Y.
    Meiling, C.
    Xiuhui, W.
    Hong, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/351963.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    layered double hydroxides
    mechanochemical method
    kinetic
    warstwowy podwójny wodorotlenek
    metoda mechaniczno-chemiczna
    kinetyka
    Opis:
    A mechanochemical method is developed in preparing magnesium-aluminum-layered double hydroxides (MgAl-LDHs). This approach includes activation process and diffusion process. In order to verify the LDHs structure and study the reaction kinetics, X-ray diffraction (XRD) patterns, inductively coupled plasma(ICP) and physical adsorption instrument were characterized. The results show that activation time can change the surface of particles and affect the reaction grade. During the diffusion process, reaction time is the most important factor. The reaction energy (ΔQ) was calculated that is 6kJ/mol.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1455-1457
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of Heat-Treatment On Microstructure And Magnetic Properties Of Nanocrystallized Mn-Zn Ferrite Powders
    Wpływ obróbki cieplnej na mikrostrukturę i właściwości magnetyczne nanokrystalicznych proszków ferrytu Mn-Zn
    Autorzy:
    Lee, W. H.
    Hong, C. S.
    Chang, S. Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/351552.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    high energy ball milling
    nanosized particles
    crystallite size
    magnetic properties
    frezowanie kulowe
    nanocząstki
    wielkości krystalitów
    właściwości magnetyczne
    Opis:
    The initial ferrite powders were subjected to high energy ball milling at 300rpm for 3h, and subsequently heat-treated at 573-1273K for 1h. Based on the observation of microstructure and measurement of magnetic properties, the heat-treatment effect was investigated. The size of initial powders was approximately 70μm. After milling, the powders with approximately 230nm in size were obtained, which were composed of the nano-sized particles of approximately 15nm in size. The milled powders became larger to approximately 550nm after heat-treatment at 973K. In addition, the size of particles increased to approximately 120nm with increasing temperature up to 973K. The coercivity of initial powders was almost unchanged after milling, whereas the saturation magnetization increased. As the heat-treatment temperature increased, the saturation magnetization gradually increased and the maximum coercivity was obtained at 773K.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1347-1350
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Trace Elements (Co, Cr) on the Microstructure and Physical Properties of Al-Si-Cu-Mg-Fe Extruded Alloy
    Autorzy:
    Ahn, S. S.
    Sharief, P.
    Lee, C. H.
    Son, H. T.
    Kim, Y. H.
    Kim, Y. C.
    Hong, S.
    Hong, S. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/352787.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Si alloy
    microstructure
    extrusion
    coefficient of thermal expansion
    trace elements
    Opis:
    Trace elements Co, Cr were added to investigate their influence on the microstructure and physical properties of Al-Si extruded alloy. The Co, Cr elements were randomly distributed in the matrix, forms intermetallic phase and their existence wereconfirmed by XRD, EDS and SEM analysis. With addition of trace elements, the microstructure was modified, Si particle size was reduced and the growth rate of β-(Al5 FeSi) phase limited. Compared to parent alloy, hardness and tensile strength were enhanced while the linear coefficient of thermal expansion (CTE) was significantly reduced by 42.4% and 16.05% with Co and Cr addition respectively. It is considered that the low CTE occurs with addition of Co was due to the formation of intermetallic compound having low coefficient of thermal expansion. The results suggested that Co acts as an effective element in improving the mechanical properties of Al-Si alloy.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 3; 857-862
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Investigation of the Microstructure and Thermoelectric Properties of P-Type BiSbTe Alloys by Usage of Different Revolutions Per Minute (RPM) During Mechanical Milling
    Autorzy:
    Yoon, S.-M.
    Madavali, B.
    Yoon, Y.-N.
    Hong, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/354749.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Bi0.5Sb1.5Te3 alloys
    mechanical alloying
    spark plasma sintering
    thermoelectric properties
    Opis:
    In this work, p-type Bi0.5Sb1.5Te3 alloys were fabricated by high-energy ball milling (MA) and spark plasma sintering. Different revolutions per minute (RPM)s were used in the MA process, and their effect on microstructure, and thermoelectric properties of p-type Bi0.5Sb1.5Te3 were systematically investigated. The crystal structure of milled powders and sintered samples were characterized using X-ray diffraction. All the powders exhibited the same morphology albeit with slight differences find at 1100 RPM conditions. A slight grain size refinement was observed on the fracture surfaces from 500 to 1100 RPM specimens. The temperature dependence of Seebeck coefficient, electrical conductivity, and power factors were measured as a function of temperature with different RPM conditions. The power factor shows almost same (~3.5 W/mK2 at RT) for all samples due to unchanged Seebeck and electrical conductivity values. The peak ZT of 1.07 at 375K is obtained for 1100 RPM specimen due to low thermal conductivity.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1167-1171
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Reduction of Thermal Conductivity Through Complex Microstructure by Dispersion of Carbon Nanofiber in p-Type Bi0.5Sb1.5Te3 Alloys
    Autorzy:
    Sharief, P.
    Madavali, B.
    Sohn, Y.
    Han, J. H.
    Song, G.
    Hong, S. J.
    Powiązania:
    https://bibliotekanauki.pl/articles/2049341.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    bismuth telluride
    carbon nano fiber
    grain size
    Thermal conductivity
    ZT
    Opis:
    The influence of nano dispersion on the thermoelectric properties of Bi2Te3 was actively investigating to wide-spread thermoelectric applications. Herein this report, we have systematically controlled the microstructure of Bi0.5Sb1.5Te3 (BST) alloys through the incorporation of carbon nanofiber (CNF), and studied their effect on thermoelectric properties, and mechanical properties. The BST/x-CNF (x-0, 0.05, 0.1, 0.2 wt.%) composites powder was fabricated using high energy ball milling, and subsequently consolidated the powder using spark plasma sintering. The identification of CNF in bulk composites was analyzed in Raman spectroscopy and corresponding CNF peaks were recognized. The BST matrix grain size was greatly reduced with CNF dispersion and consistently decreased along CNF percentage. The electrical conductivity was reduced and Seebeck coefficient varied in small-scale by embedding CNF. The thermal conductivity was progressively diminished, obtained lattice thermal conductivity was lowest compared to bare sample due to induced phonon scattering at interfaces of secondary phases as well as highly dense fine grain boundaries. The peak ZT of 0.95 achieved for 0.1 wt.% dispersed BST/CNF composites. The Vickers hardness value of 101.8 Hv was obtained for the BST/CNF composites.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 3; 803-808
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Surface Characterization of Metallic Fuel Slugs Prepared by Modified Injection Casting
    Autorzy:
    Mun, S.-U.
    Kim, K.-H.
    Oh, S.-J.
    Park, J.-Y.
    Hong, S.-I.
    Powiązania:
    https://bibliotekanauki.pl/articles/351428.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    sodium-cooled fast reactor
    metallic fuel slug
    U-Zr alloy
    surface characterization
    injection casting
    Opis:
    Metallic fuel slugs containing rare-earth (RE) elements have high reactivity with quartz (SiO2) molds, and a reaction layer with a considerable thickness is formed at the surface of metallic fuel slugs. The surface characterization of metallic fuel slugs is essential for safety while operating a fast reactor at elevated temperature. Hence, it is necessary to evaluate the surface characteristics of the fuel slugs so that chemical interaction between fuel slug and cladding can be minimized in the reactor. When the Si element causes a eutectic reaction with the cladding, it deteriorates the metallic fuel slugs. Thus, it is necessary to examine the characteristics of the surface reaction layer to prevent the reaction of the metallic fuel slugs. In this study, we investigated the metallurgical characteristics of the surface reaction layer of fabricated U-10wt.%Zr-Xwt.%RE (X = 0, 5, 10) fuel slugs using injection casting. The results showed that the thickness of the surface reaction layer increased as the RE content of the metallic fuel slugs increased. The surface reaction layer of the metallic fuel slug was mainly formed by RE, Zr and the Si, which diffused in the quartz mold.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 2; 1049-1053
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect Of Ti Powder Addition On The Fabrication Of TiO2 Nanopowders
    Wpływ dodatku nanoproszku Ti na zagęszczanie i spiekanie nanoproszków TiO2
    Autorzy:
    Raihanuzzaman, R. M.
    Park, H. Y.
    Ghomashchi, R.
    Kwon, T. H.
    Son, H.-T.
    Hong, S.-J.
    Powiązania:
    https://bibliotekanauki.pl/articles/353186.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    TiO2 nanopowder
    magnetic pulsed compaction
    densification
    sintering
    nanoproszek Ti
    magnetyczne zagęszczanie impulsowe
    zagęszczanie
    spiekanie
    Opis:
    Sintered samples of Ti added TiO2 nanopowders were fabricated by combined application of magnetic pulsed compaction (MPC) and sintering. The effect of Ti nano powder on density, shrinkage and hardness of the samples were investigated as part of the study. The optimum processing conditions were found to be around 0.5 GPa MPC pressure and 1450°C sintering temperature, illustrating maximum density, hardness and minimum shrinkage. High pressure compaction using MPC was found to enhance density with increasing MPC pressure up to 0.9 GPa, and significantly reduce the total shrinkage (about 16% in this case) in the sintered bulks compared to other general processes (about 18%). While sintered samples blended with micro Ti showed presence of microstructural cracks, the samples with 1-2% nano Ti had less or no cracks on them. Overall, the inclusion of nano Ti indicated improvement in mechanical properties of TiO2 nanopowders sintered preforms as opposed to micro Ti-added TiO2.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1473-1477
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Improved Mechanical Properties of Al-Si Alloys by Adding an Extrusion Process to Conventional Processing Method
    Autorzy:
    Han, J. Y.
    Femi, O. E.
    Kilicaslan, F.
    Jeong, C. U.
    Baeg, C. H.
    Hong, S. J.
    Koo, J. M.
    Powiązania:
    https://bibliotekanauki.pl/articles/355114.pdf
    Data publikacji:
    2017
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Al-Si alloys
    extrusion
    mechanical properties
    Opis:
    In this study, the mechanical properties of Al-Si alloys was improved by selecting higher Si content and avoiding distortion in Al-Si matrix by adding an extrusion process such that the fabrication processes casting and extrusion were in sequence. Cast billets were extruded at ratios 4:1 and 10:1 to obtained two extruded bars with different processing parameters. The as-extruded samples were characterized and investigated for microstructure and mechanical properties. Optical Microscope was used to examined phase morphologies and microstructures of the extruded Al-Si bars. Mechanical properties were conducted on each sample to study the effectiveness of the additional extrusion process in high Si content Al-Si alloys. The result shows that by increasing the extrusion ratio, the size of the primary Si particle reduces leading to a higher density, better tensile and yield strength compared to the cast billet.
    Źródło:
    Archives of Metallurgy and Materials; 2017, 62, 2B; 1179-1183
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-9 z 9

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