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Tytuł:
Preparation of Nickel Powders by Reduction of Nickel Hydroxide Using the Taylor Fluid Flow
Autorzy:
Park, I.-J.
Kim, D.-W.
Kim, G.-H.
Chae, H.-J.
Jung, H.-C.
Powiązania:
https://bibliotekanauki.pl/articles/355021.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ni(OH)2
nickel
Taylor fluid flow
fine powder
Opis:
In this study, Ni(OH)2 was synthesized by the continuous reaction by the Taylor fluid flow and compared with those prepared from the conventional batch type reaction. The nickel powders were synthesized by reduction of Ni(OH)2 in an aqueous solution with hydrazine hydrate acting as the reductant. And then the characteristics of the nickel powder according to the synthesis method were compared. The average particle size of the synthesized Ni(OH)2 using Taylor reactor was generally decreased about 1.5~2.5 times more than the batch reaction. The nickel powders prepared by the batch reaction highly agglomerated with non-uniform particles. In the Taylor reaction, the agglomeration of particles was broken and uniform nickel powder was produced.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1443-1447
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Impact Toughness of Offshore Steel
Autorzy:
Cheng, T.-C.
Yu, C.
Yang, T.-C.
Huang, C.-Y.
Lin, H.-C.
Shiue, R.-K.
Powiązania:
https://bibliotekanauki.pl/articles/351264.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
low-temperature impact toughness
prior austenite grain size
hardenability
bainite
Opis:
This study focused on the effects of microstructures on the low-temperature impact toughness of directly water-quenched offshore steel. Martensite dominated the microstructure directly below the quenched surface. In contrast, mainly lower bainite, martensite, and low amount of ferrite were observed in the central region of the quenched specimen. The ductile to brittle transition temperature of tempered martensite was significantly lower than that of a bainite-dominated microstructure. It is found that low-angle boundaries within the bainite packets greatly impair the low-temperature impact toughness of the steel. The absence of high-angle boundaries in the lower bainite packets significantly deteriorates the low-temperature impact energy of offshore steel.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 1; 167-172
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Kinetics of Grain Growth in 718 Ni-Base Superalloy
Kinetyka wzrostu ziaren w nadstopie niklu 718
Autorzy:
Huda, Z.
Zaharinie, T.
Metselaar, H. S. C.
Ibrahim, S.
Min, Goh J.
Powiązania:
https://bibliotekanauki.pl/articles/352555.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
nickel-base superalloy
microstructures
grain growth
kinetics
activation energy
nadstop niklu
mikrostruktura
wzrost ziaren
kinetyka
energia aktywacji
Opis:
The Haynes® 718 Ni-base superalloy has been investigated by use of modern material characterization, metallographic and heat treatment equipment. Grain growth annealing experiments at temperatures in the range of 1050 – 1200 oC (1323–1473K) for time durations in the range of 20 min-22h have been conducted. The kinetic equations and an Arrhenius-type equation have been applied to compute the grain-growth exponent n and the activation energy for grain growth, Qg, for the investigated alloy. The grain growth exponent, n, was computed to be in the range of 0.066-0.206; and the n values have been critically discussed in relation to the literature. The activation energy for grain growth, Qg, for the investigated alloy has been computed to be around 440 kJ/mol; and the Qg, data for the investigated alloy has been compared with other metals and alloys and ceramics; and critically analyzed in relation to our results.
Nadstop na bazie niklu Haynes ® 718 badano przy użyciu nowoczesnych urządzeń do charakterystyki materiałów, metalografii i obróbki cieplnej. Przeprowadzono badania wzrostu ziarna podczas wyżarzania w zakresie temperatur 1050 - 1200 ° C (1323-1473K) w czasie trwania od 20 minut do 22 godzin. Równania kinetyczne i równanie typu Arrheniusa zostały zastosowane do obliczania wykładnika wzrostu ziarna n oraz energii aktywacji wzrostu ziarna, Qg, dla badanego stopu. Obliczona wartość wykładnika wzrostu ziarna, n, mieści się w zakresie od 0.066 do 0.206 i została krytycznie przedyskutowana w odniesieniu do literatury. Obliczona energia aktywacji wzrostu ziaren, Qg, wynosi dla badanego stopu na około 440 kJ / mol. Dane Qg dla badanego stopu porównywano z danymi dla innych metali, stopów i ceramiki oraz krytycznie analizowano w odniesieniu do naszych wyników.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 3; 847-852
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High Purity Tungsten Spherical Particle Preparation From WC-Co Spent Hard Scrap
Wytwarzanie wysokiej czystości sferycznych cząstek wolframu z twardego złomu WC-Co
Autorzy:
Han, C.
Na, H.
Choi, H.
Kim, Y.
Powiązania:
https://bibliotekanauki.pl/articles/351951.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
WC-Co
spent hard scrap
hydrometallurgy
RF thermal plasma
twardy złom
hydrometalurgia
plazma termiczna
Opis:
Tungsten carbide-cobalt hard metal scrap was recycled to obtain high purity spherical tungsten powder by a combined hydrometallurgy and physical metallurgy pathway. Selective leaching of tungsten element from hard metal scrap occurs at solid / liquid interface and therefore enlargement of effective surface area is advantageous. Linear oxidation behavior of Tungsten carbide-cobalt and the oxidized scrap is friable to be pulverized by milling process. In this regard, isothermally oxidized Tungsten carbide-cobalt hard metal scrap was mechanically broken into particles and then tungsten trioxide particle was recovered by hydrometallurgical method. Recovered tungsten trioxide was reduced to tungsten particle in a hydrogen environment. After that, tungsten particle was melted and solidified to make a spherical one by RF (Ratio Frequency) thermal plasma process. Well spherical tungsten micro-particle was successfully obtained from spent scrap. In addition to the morphological change, thermal plasma process showed an advantage for the purification of feedstock particle.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1507-1509
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
An Analysis Of Stress Intensity Factor Due To Normal Stress For A Cracked Plate Reinforced With A Sheet By Seam Welding
Analiza współczynnika intensywności naprężeń wynikających z prostopadłego naprężenia dla pękniętej płyty wzmocnionej płytą przyspawaną szwem
Autorzy:
Kim, O.-H.
Kim, Y. C.
Powiązania:
https://bibliotekanauki.pl/articles/352434.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stress intensity factor
seam welding
singular integral equation
reinforcement effect
współczynnik intensywności naprężeń
spawanie
efekt wzmacniający
Opis:
It is essential in damage tolerance design to determine the stress intensity factor theoretically. The stress intensity factor for a cracked plate that is reinforced with a sheet by seam welding is determined theoretically and plotted as function of the seam welding location and stiffness ratio. The singular integral equation is derived based on the compatibility condition between the cracked plate and the reinforcement plate, and it is solved by means of Erdogan and Gupta‘s method. The theory is verified by comparing the results of the present analysis with those of a numerical analysis. The results from the present analysis show that the reinforcement effect improves as the welding line is situated closer to the crack and as the stiffness ratio of the cracked plate and the reinforcement plate increases.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1441-1444
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterization Of The Graded Microstructure In Powder Sintered Porous Titanium
Charakterystyka gradientowej mikrostruktury porowatego tytanu spiekanego z proszku
Autorzy:
Oak, J.-J.
Bang, J. I.
Bae, K.-C.
Kim, Y. H.
Lee, Y. C.
Chun, H. H.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/356239.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
titanium
powder metallurgy
porous structure
sintering
biomaterial
tytan
metalurgia proszków
struktura porowata
spiekanie
biomateriał
Opis:
The proposed sintering process produce porosity and functional graded microstructure in the sinterd titanium powders. Titanium powders with different micro sizes were sintered at the proposed temperature region at 1200 and 1300°C for 2h. The apatite-forming on the graded microstructure is observed by immersion test in Hanks balanced salt soluion at 37°C. Sintering condition of titanium powders is estimated by thermogravitmetry-differential thermal analysis (TG-DTA). The synthersied surface structures and apatite-forming ability were characterized by a field emission scanning electron microscopy (FE-SEM) observation and energy dispersive X-ray spectroscopy (EDS) analysis. As results, these graded microstructure of sintered porous titanium powders reveals apatite-forming ability as osseointegration by calcification in Hanks balanced salt soluion(HBSS) at 37°C.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1265-1269
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
De-Lubrication Behavior Of Novel EBS Based Admixed Lubricant In Aluminum P/M Alloy
Zachowanie nowego lubrykantu na bazie EBS w trakcie spiekania proszku stopu aluminium
Autorzy:
Oh, M. C.
Seok, H.
Kim, H. J.
Ahn, B.
Powiązania:
https://bibliotekanauki.pl/articles/354258.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
admixed lubricant
compaction pressure
powder metallurgy
sintering
Al-Cu-Mg alloy
lubrykant
zagęszczanie
metalurgia proszków
spiekanie
stop Al-Cu-Mg
Opis:
The objective of the present research is to develop a novel lubricant for Al-Cu-Mg P/M alloy and to address the effects of the lubricant and compaction pressure on sintered properties. A lubricant mixture consisting of Ethylene Bis Stearamide, Zn-Stearate, and fatty acid was newly developed in this study, and the de-lubrication behavior was compared with that of other commercial lubricants, such as Ethylene Bis Stearamide, Zn-Stearate, and Al-Stearate. Density and transverse rupture strength of sintered materials with each lubricant were examined, respectively. The microstructural analysis was conducted using optical microscope.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1427-1431
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Strain Measurements in Free Tube Hydroforming Process
Autorzy:
Sadłowska, H.
Morawiński, Ł.
Jasiński, C.
Powiązania:
https://bibliotekanauki.pl/articles/351278.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
strain measurement
hydroforming
stereovision
Opis:
The paper presents a method of measuring deformations of cylindrical samples on the testing machine for free tube hydroforming experiments. During experiments a sample made of a thin-walled metal tube is expanded by the internal pressure of the working liquid and additionally subjected to axial compression. This results in a considerable circumferential deformation of the tube and its shortening. Analysis of the load cases and their impact on the deformations can be helpful in determining e.g. tube material properties or general limiting conditions in the tube hydroforming process. In connection with the above, the value of deformations and knowledge of their course during experiment has become one of the most important problems related to the issue described above.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 1; 257-263
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study on Effects of Mold Temperature on the Injection Molded Article
Autorzy:
Han, J.-H.
Kim, Y.-C.
Powiązania:
https://bibliotekanauki.pl/articles/351919.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
injection molding
mold temperature
cooling temperature
molded article
Opis:
This is a study of the effects of temperature of injection mold on the injection molded article. By supplying water of the proper temperature in the cooling line of mold in the cooling process, the mold was the appropriate temperature, and the deformation of the injection molded article was examined according to the mold temperature. In this study, we conducted simulation analysis and experiments, and the results were analyzed. The minimum deformation of the injection molded article model obtained by supplying 50°C water in the cooling line is 0.003 mm, and the maximum deformation was 0.813 mm. Injection molded article models obtained by supplying 20°C water were found to be a minimum of 0.002 mm, with deformation of up to 0.761 mm. When comparing both conditions, the error rate of injection molded article obtained by supplying 20°C water in the mold cooling line was lower by about 0.18%.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1271-1274
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Experimental Investigation Of Segregation Of Carbon Atoms Due To Sub-Zero Cryogenic Treatment In Cold Work Tool Steel By Mechanical Spectroscopy And Atom Probe Tomography
Doświadczalne badania segregacji atomów węgla w stali narzędziowej do pracy na zimno po obróbce kriogenicznej metodą spektroskopii mechanicznej i tomografii atomowej
Autorzy:
Min, N.
Li, H. M.
Xie, C.
Wu, X. C.
Powiązania:
https://bibliotekanauki.pl/articles/351716.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
cryogenic treatment
isothermal martensite
atom probe tomography
mechanical spectroscopy
Cottrell atmosphere
obróbka kriogeniczna
izotermiczny martenzyt
tomografia atomowa
spektroskopia mechaniczna
atmosfera Cottrella
Opis:
In this work, we present mechanical spectroscopy of cold work tool steel subjected to sub-zero cryogenic soaking treatment to reveal the carbon segregation and the subsequent carbides refinement. The maximum of Snoek-Köster (SK) peak height was obtained in the sample subjected to soaking 1h at −130°C cryogenic treatment. The SK peak height is reduced with prolonging the soaking time. The results indicate that an increase in the height of SK peak is connected with an increase in dislocation density and the number of segregated carbon atoms in the vicinity of dislocations or twin planes after martensite transformation at −130°C which is confirmed by corresponding TEM and atom probe tomography measurement. Hence, it is suggested that the isothermal martensite, formed during the cryogenic soaking treatment decreases (APT) the height of SK peak.
W pracy przedstawiono wyniki spektroskopii mechanicznej stali narzędziowej do pracy na zimno poddanej obróbce kriogenicznej w celu odsłonięcia segregacji węgla i późniejszego tworzenia węglików. Dzięki połączeniu transmisyjnej mikroskopii elektronowej (TEM) i tomografii atomowej (APT) uzyskano maksymalny pik Snoek-Köstera (SK) w próbce poddanej obróbce kriogenicznej przez 1 godzinę w −130°C. Wysokość piku SK obniża się wraz z wydłużeniem czasu obróbki. Wyniki wskazują, że zwiększenie wysokości piku SK jest połączone ze wzrostem gęstości dyslokacji i liczby segregowanych atomów węgla w sąsiedztwie dyslokacji lub płaszczyzn bliźniaczych po przemianie martenzytycznej w -130°C, co potwierdzone jest odpowiednimi pomiarami TEM oraz APT. W związku z tym proponuje się, że izotermiczny martenzyt powstały podczas obróbki kriogenicznej zmniejsza wysokość piku SK.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2A; 1109-1113
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Hafnium and Zirconium to Glass Forming Ability, Thermal Stability, Plasticity Deformation and Crystallization of Ni-Free Pentabasic Ti-Based Bulk Metallic Glasses
Autorzy:
Oak, J.-J.
Kim, Y. H.
Bae, K.-C.
Park, Y. H.
Powiązania:
https://bibliotekanauki.pl/articles/352087.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti-based alloy
metallic glass
Ti fiber
glass formability
plastic deformation
Opis:
The newly designed Ti-based bulk metallic glass (BMG) in which case of fracture behavior was observed 1990MPa to compressive strength with a wide plastic deformation around 7% after process of elastic deformation. This phenomenon can be compared with those of Ti-based alloys and other Ti-based BMGs and indicates high potential to be applied in use. It was evaluated the Ti-based BMG for thermal stability that the reduced glass parameters, ΔTx, Trg and γ, are 79K, 0.50 and 0.38, respectively. In addition, it reveals high activation energies for crystallization in which are estimated to Ex1 = 291.77 ±9.71 kJ/mol, Ex2 = 588.77 ±28.88 kJ/mol and Ex3 = 330.26 ±3.61 kJ/mol on kissinger plotting in this study.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1081-1087
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Vacuum Hot-Press Process on The Sintered Characteristics and Mechanical Properties of A High-Density Cr-31.2 Mass% Ti Alloy
Autorzy:
Chang, S.-H.
Li, C.-L.
Huang, K.-T.
Yang, T.-H.
Powiązania:
https://bibliotekanauki.pl/articles/356911.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Cr-31.2 mass% Ti alloy
vacuum hot-press sintering
relative density
TRS
electrical conductivity
Opis:
In this study, two different compositions of submicron-structured titanium (760 nm) and micron-structured chromium (4.66 μm) powders were mixed to fabricate Cr-31.2 mass% Ti alloys by vacuum hot-press sintering. The research imposed various hot-press sintering pressures (20, 35 and 50 MPa), while the sintering temperature maintained at 1250°C for 1h. The experimental results showed that the optimum parameters of the hot-press sintered Cr-31.2 mass% Ti alloys were 1250°C at 50 MPa for 1h. Also, the relative density reached 99.94%, the closed porosity decreased to 0.04% and the hardness and transverse rupture strength (TRS) values increased to 81.90 HRA and 448.53 MPa, respectively. Moreover, the electrical conductivity is enhanced to 1.58 × 104 S·cm-1 However, the grain growth generated during the high-temperature and high-pressure of the hot-press sintering process resulted in the grain coarsening phenomenon of the Cr-31.2 mass% Ti alloys after 1250°C hot-press sintering at 50 MPa for 1h. In addition, the Cr-31.2 mass% Ti alloys were fabricated with the submicron-structured titanium (760 nm) and chromium (588 nm) powders showed more effective compaction than the micron-structured titanium (760 nm) and chromium (4.66 μm) powders did. The closed porosity decreases to 0.02% and the hardness values increase to 83.23 HRA. However, the agglomeration phenomenon of the Cr phase and brittleness of the TiCr2 Laves phases easily led to a slight decrease in TRS (400.54 MPa).
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 4; 1715-1723
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Trace Elements (Co, Cr) on the Microstructure and Physical Properties of Al-Si-Cu-Mg-Fe Extruded Alloy
Autorzy:
Ahn, S. S.
Sharief, P.
Lee, C. H.
Son, H. T.
Kim, Y. H.
Kim, Y. C.
Hong, S.
Hong, S. J.
Powiązania:
https://bibliotekanauki.pl/articles/352787.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Al-Si alloy
microstructure
extrusion
coefficient of thermal expansion
trace elements
Opis:
Trace elements Co, Cr were added to investigate their influence on the microstructure and physical properties of Al-Si extruded alloy. The Co, Cr elements were randomly distributed in the matrix, forms intermetallic phase and their existence wereconfirmed by XRD, EDS and SEM analysis. With addition of trace elements, the microstructure was modified, Si particle size was reduced and the growth rate of β-(Al5 FeSi) phase limited. Compared to parent alloy, hardness and tensile strength were enhanced while the linear coefficient of thermal expansion (CTE) was significantly reduced by 42.4% and 16.05% with Co and Cr addition respectively. It is considered that the low CTE occurs with addition of Co was due to the formation of intermetallic compound having low coefficient of thermal expansion. The results suggested that Co acts as an effective element in improving the mechanical properties of Al-Si alloy.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 857-862
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Sintering and Microstructures of SUS 316L Powder Produced by 3D Printing Process
Autorzy:
Kim, W. J.
Nguyen, H.-H.
Kim, H. Y.
Nguyen, M.-T.
Park, H. S.
Kim, J.-C.
Powiązania:
https://bibliotekanauki.pl/articles/356018.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stainless steel
3D printing
selective laser sintering
SUS 316L
flake powder
Opis:
Selective laser sintering (SLS) is a type of laminating sintering technique, using CO2 laser with (metal, polymer, and ceramic) powders. In this result, the flake SUS 316L was used to achieve a high porous product, and compare to spherical type. After SLS, the porosity of flake-type sample with 34% was quite higher than that of the spherical-type one that had only 11%. The surface roughness of the flake SLS sample were also investigated in both inner and surface parts. The results show that the deviation of the roughness of the surface part is about 64.40μm, while that of the internal one was about 117.65μm, which presents the containing of high porosity in the uneven surfaces. With the process using spherical powder, the sample was quite dense, however, some initial particles still remained as a result of less energy received at the beneath of the processing layer.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2B; 1215-1218
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxide Formation In Metal Injection Molding Of 316L Stainless Steel
Tworzenie tlenków podczas wtryskiwania proszku stali nierdzewnej 316L
Autorzy:
Jang, J. M.
Lee, W.
Ko, S.-H.
Han, C.
Choi, H.
Powiązania:
https://bibliotekanauki.pl/articles/351352.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
powder injection molding
sintering
316L stainless steel
sintering atmosphere
micro parts
wtryskiwanie proszku
spiekanie
stal nierdzewna 316L
mikro-część
Opis:
The effects of sintering condition and powder size on the microstructure of MIMed parts were investigated using water-atomized 316L stainless steel powder. The 316L stainless steel feedstock was injected into micro mold with micro features of various shapes and dimensions. The green parts were debound and pre-sintered at 800°C in hydrogen atmosphere and then sintered at 1300°C and 1350°C in argon atmosphere of 5torr and 760torr, respectively. The oxide particles were formed and distributed homogeneously inside the sample except for the outermost region regardless of sintering condition and powder size. The width of layer without oxide particles are increased with decrease of sintering atmosphere pressure and powder size. The fine oxides act as the obstacle on grain growth and the high sintering temperature causes severe grain growth in micro features due to larger amount of heat gain than that in macro ones.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1281-1285
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł

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