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Tytuł:
Manufacturing And High Temperature Oxidation Properties Of Electro-Sprayed Fe-24.5% Cr-5%Al Powder Porous Metal
Wytwarzanie i wysokotemperaturowe utlenianie elektro-rozpylanego porowatego proszku Fe-24.5% Cr-5%Al
Autorzy:
Lee, K-A.
Oh, J-S.
Kong, Y-M.
Kim, B-K.
Powiązania:
https://bibliotekanauki.pl/articles/350912.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
powder porous metal
electro-spray process
electric wire explosion
Fe-24Cr-5Al
high temperature oxidation
porowaty proszek metalu
elektrorozpylanie
utlenianie wysokotemperaturowe
Opis:
Fe-Cr-Al based Powder porous metals were manufactured using a new electro-spray process, and the microstructures and high-temperature oxidation properties were examined. The porous materials were obtained at different sintering temperatures (1350°C, 1400°C, 1450°C, and 1500°C and with different pore sizes (500 μm, 450 μm, and 200 μm). High-temperature oxidation experiments (TGA, Thermal Gravimetry Analysis) were conducted for 24 hours at 1000°C in a 79% N2+ 21% O2, 100 mL/min. atmosphere. The Fe-Cr-Al powder porous metals manufactured through the electro-spray process showed more-excellent oxidation resistance as sintering temperature and pore size increased. In addition, the fact that the densities and surface areas of the abovementioned powder porous metals had the largest effects on the metal’s oxidation properties could be identified.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1169-1173
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characteristics Of The Porous Body Sintered By Nano-Sized Fe-Cr-Al Alloy Powder
Charakterystyka porowatego korpusu spiekanego z nanometrycznego proszku stopu Fe-Cr-Al
Autorzy:
Lee, S.-I.
Lee, S.-H.
Gu, B.-U.
Lee, D.-W.
Kim, B.-K.
Powiązania:
https://bibliotekanauki.pl/articles/356635.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-Cr-Al powder
metallic sponges
sintering temperature
oxidation resistance
proszek Fe-Cr-Al
proszek nanometryczny
temperatura spiekania
odporność na utlenianie
Opis:
Porous metal with uniform honeycomb structure was successfully produced by sintering using Fe-Cr-Al nano powder, which was prepared by the pulsed wire evaporation (PWE) in ethanol. Its process consisted of the several steps; 1) coating on the surface of polyurethane sponge with the liquid droplets generated from the ethanol-based slurry where the Fe-Cr-Al nano powders were uniformly dispersed, 2) heat treatment of debinding to remove the polyurethane sponge and 3) sintering of the porous green body formed by Fe-Cr-Al nano powders. The strut thickness of porous Fe-Cr-Al was increased by the increase of spraying times in ESP step. Also, The shrinkages and the oxidation resistance of the sintered porous body was increased with increase of sintering temperature. The optimal sintering temperature was shown to 1450°C in views to maximize the oxidation resistance and sinterability.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1275-1279
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermodynamic Description of Ternary Fe-B-X Systems. Part 3: Fe-B-Mn
Opis termodynamiczny trójskładnikowych układów Fe-B-X. Część 3: Fe-B-Mn
Autorzy:
Miettinen, J.
Lilova, K.
Vassilev, G.
Powiązania:
https://bibliotekanauki.pl/articles/353752.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
phase diagrams
thermodynamic modelling
Fe-based systems
Fe-B-X systems thermodynamic database
Fe-B-Mn system
diagramy fazowe
modelowanie termodynamiczne
systemy na bazie Fe
termodynamiczny system Fe-B-X
system Fe-B-Mn
Opis:
A thermodynamic optimization of the ternary Fe-B-Mn system is presented. The thermodynamic parameters of the binary sub-systems, Fe-Mn, Fe-B and B-Mn, are taken from earlier assessments slightly modifying the B-Mn system description. The thermodynamic parameters of the Fe-B-Mn system are optimized in this study using literature experimental thermodynamic and phase equilibrium data. The solution phases of the system are described using the substitutional solution model and the borides are treated as stoichiometric or semi-stoichiometric phases of the (A,B)pCq type described with the two-sublattice models.
Przedstawiono termodynamiczny opis trójskładnikowego układu Fe-B-Mn. Parametry termodynamiczne dwuskładnikowych stopów Fe-Mn, Fe-B i B-Mn zostały zaczerpnięte z wcześniejszych opracowań, przy tym opis układu B-Mn został nieznacznie zmodyfikowany. Parametry termodynamiczne dla układu Fe-B-Mn zostały zoptymalizowane w tej pracy w oparciu o eksperymentalne równowagi fazowe i dane termodynamiczne zaczerpnięte z literatury. Roztwory stałe w układzie Fe-B-Mn opisano przy użyciu modelu roztworu substytucyjnego, a borki traktowane sa jako fazy stechiometryczne lub półstechiometryczne typu (A,B)pCq opisane przy użyciu modelu dwu podsieci.
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 4; 1481-1485
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation of a Ceramic Proppants for Hydraulic Fracturing Using F - Type Fly Ash
Autorzy:
Kasprzyk, K.
Kogut, K.
Zboromirska-Wnukiewicz, B.
Dyjakon, A.
Powiązania:
https://bibliotekanauki.pl/articles/355374.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
proppants
ceramic materials
shale gas
hydraulic fracturing
fly ash
Opis:
In the paper, the technology of the production of the modified ceramic proppants used in the shale gas extracting process is described. The natural available materials and uncomplicated process to new ceramic proppants preparation were applied. The modification of the ceramic proppants based on the addition of the waste material as fly ash. The produced ceramic material in the form of granules characterized by high mechanical properties and low production costs. Moreover, the obtained good values of compressive strength and gas permeability for investigated proppants confirmed that this material has appropriate properties to be used in the hydraulic fracturing.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 2; 1065-1070
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Combined Effect of Zr and Si on Isothermal Oxidation of Ti
Autorzy:
Ha, S.-H.
Kim, B.-H.
Yoon, Y.-O.
Lim, H.-K.
Kim, S. K.
Powiązania:
https://bibliotekanauki.pl/articles/353260.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Ti
Zr
Si
silicide
oxidation
Opis:
In this study, the combined effect of Zr and Si on isothermal oxidation of Ti for 25 and 50h at 820°C, which is the temperature related to exhaust valves operation, was investigated. Si addition into Ti-5mass%Zr alloy led to a distribution of silicide Ti5Si3 phase formed by a eutectic reaction. The Ti sample containing only Zr showed more retarded oxidation rate than Ti-6Al-4V, the most prevalent Ti alloy, at the same condition. However, while a simultaneous addition of Zr and Si resulted in greater increase of oxidation resistance. The oxide layer formed after the addition of Zr and Si comprised TiO2, ZrO2, and SiO2.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1493-1495
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure and Electrical Resistivity Dependence of Molybdenum Thin Films Deposited by DC Modulated Pulsed Magnetron Sputtering
Autorzy:
Wicher, B.
Chodun, R.
Nowakowska-Langier, K.
Okrasa, S.
Król, K.
Minikayev, R.
Strzelecki, G.
Zdunek, K.
Powiązania:
https://bibliotekanauki.pl/articles/350987.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
magnetron sputtering
modulated pulse magnetron sputtering
plasma&films characterization
Opis:
This work reports the results of a study of Mo thin films synthesis by DC Pulsed Magnetron Sputtering method (PMS), operating at pulse main frequency of 100 kHz and modulated by the additional modulation frequency, driving in the range of 5-1000 Hz (modulated Pulse Magnetron Sputtering – mPMS). We have studied the influence of mPMS on plasma chemical reactions and mechanisms of layer growth using optical emission spectroscopy technique. Our experiment showed strong influence of mPMS method, on the morphology (scanning electron microscopy), phase composition (X-ray diffractometry) and electric properties (4-point probes method) of nanocrystalline and amorphous Mo films. From the utilitarian point of view, low value of resistivity – 43,2 μΩcm of synthesized Mo films predestines them as back contacts for thin solar cells CIGS. Our results revealed that additional modulation frequency should be considered as an important factor for optimization of films synthesis by means of PMS-based methods.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1339-1344
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Selected Aspects of Manufacturing of Aluminium Sponge
Autorzy:
Stręk, A. M.
Lipowska, B.
Wańczyk, K.
Powiązania:
https://bibliotekanauki.pl/articles/355824.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metal sponge
aluminium sponge
investment casting
precursor thickening
Opis:
The present article describes selected aspects of investment casting technology for manufacturing of open-cell aluminium. The main focus is, among others, on the precursor thickening. Two groups of total 30 samples were produced, basing on open-cell polyurethane foam used as the precursor. Each of the two sample groups was thickened with a different type of suspension consisting of carbonaceous substances and organic binders. The influence of the coating mixture type was compared, leading to conclusions regarding the desired composition and fluidity of the suspensions. Both sample groups of the obtained open-cell aluminium had stochastic cell distributions, the average pore diameter was 5.2 mm and the PPI index was 8. The apparent densities were respectively: 0.485 g/cm3 and 0.312 g/cm3 , which reflected the impact of the precursor coating. Additionally, samples from both groups differed in quality.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 1145-1150
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Radiographic quality assessment of welded joints in building structures produced according to requirements of standard EN-1090-2, quality level "B +"
Radiograficzna ocena jakości złączy spawanych w konstrukcjach budowlanych wykonywanych według wymagań normy EN-1090-2, na poziomie jakości "B+"
Autorzy:
Staniszewski, K.
Sikora, S.
Czuchryj, J.
Powiązania:
https://bibliotekanauki.pl/articles/350886.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
złącza spawane
jakość B
welded joints
quality B
Opis:
While assessing the quality of welded joints it may become necessary to establish various quality levels in the same joint or implement specific requirements for an already adopted quality level. The latter case can be observed in standard EN 1090-2, in which additional requirements were adopted for quality level B and thus a new quality level designated as B+ was created. Most of the additional requirements are concerned with imperfections detected by means of radiography. For this reason it was necessary to compare the principles governing the assessment of the quality of welded joints from radiographic examination point of view, according to the requirements of standard EN ISO 5817 and those of EN 1090-2. A conducted comparative analysis aims at optimising the aforesaid principles in relation to the requirements presented therein.
Podczas określania jakości złączy spawanych może być konieczne ustalenie różnych poziomów jakości w tym samym złączu lub wprowadzenie szczególnych wymagań dla przyjętego poziomu jakości. Ostatni przypadek zaobserwowano w nowej normie EN 1090-2, w której dla poziomu jakości B ustalono wymagania dodatkowe. Nowy poziom jakości oznaczono symbolem B+. Większość dodatkowych wymagań dotyczy niezgodności wykrywanych metodą radiograficzną. Z tego powodu porównano zasady oceny jakości złączy spawanych z punktu widzenia kontroli radiograficznej według wymagan norm EN ISO 5817 i EN 1090-2. Przeprowadzona analiza porównawcza powinna przyczynić się do zoptymalizowania tych zasad ze względu na przedstawione w normach wymagania.
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 1; 99-104
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hot Pressed K0.5Na0.5NbO3 Material for Piezoelectric Transformer for Energy Harvesting
Autorzy:
Kozielski, L.
Feliksik, K.
Wodecka-Duś, B.
Szalbot, D.
Tutu, S.
Powiązania:
https://bibliotekanauki.pl/articles/353060.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
energy harvesting
piezoelectric effect
piezoelectric transformer
piezoelectric properties
Opis:
An optimized method of vibration Energy Harvesting is based on a step-down transformer that regulates the power flow from the piezoelectric element to the desired electronic load. Taking into account parameters of the whole system, the “optimal” voltage gain the piezoelectric transformer can be determined where the harvested power is maximized for the actual level of mechanical excitation. Consequently the piezoelectric transformers can be used to boost up the conversion of mechanical strain into electrical power with considerable potential in Energy Harvesting applications. Nowadays however, the most important factor is usage of lead free material for its construction. Additional desired parameters of such ceramics include high value of piezoelectric coefficients, low dielectric losses and reasonable power density. This work for first time proposes a lead free K0.5Na0.5NbO3 (KNN) material implementation for stack type of piezoelectric transformer that is designed for load efficiency optimization of vibration energy harvester.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1275-1280
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Grain Boundary Wetting and Material Performance in an Industrial EZ33A Mg Cast Alloy
Autorzy:
Straumal, A. B.
Tsoy, K. V.
Mazilkin, I. A..
Nekrasov, A. N.
Bryła, K.
Powiązania:
https://bibliotekanauki.pl/articles/352347.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
grain boundary
wetting
cast alloy
Mg
mechanical properties
Opis:
The grain boundary wetting phase transition in an industrial EZ33A cast alloy is studied. 12% of the grain boundaries are completely wetted at the temperature slightly higher than the eutectic transformation temperature (530°C). The fraction of wetted grain boundaries increases with temperature, reaches a maximum of 85% at 570°C, and does not change further until the alloy melts. In the as-cast state, the alloy has low ductile properties at the ambient temperature. The microstructure in the as-cast state corresponds to the wetting state at about 560°C, which indicates that the cooling rate in casting is almost equal to that in quenching. The volume and the surface fraction of the second phase and the hardness measured at the least wetted state of samples point toits good machinability. The wetting data are used to suggest a sequence of heat treatment and machining for processing EZ33A alloy parts.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 3; 869-873
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Deposition of Gold Nanoparticles Onto Activated Carbon
Osadzanie nanocząstek złota na węglu aktywnym
Autorzy:
Jaworski, W.
Streszewski, B.
Szaciłowski, K.
Pacławski, K.
Powiązania:
https://bibliotekanauki.pl/articles/351364.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
gold nanoparticles
activated carbon
functionalization
amines
nanocząstki złota
węgiel aktywny
funkcjonalizacja
aminy
Opis:
This work reports the results of spectrophotometric, dynamic light scattering (DLS) and microscopic (SEM) studies of the gold nanoparticles (AuNPs) deposition on activated carbon (AC) surface modified with primary (ethanolamine) and secondary (diethylenetriamine and triethylenetetramine) amines. It was found that this method is efficient for deposition of AuNPs from aqueous solution. However, nanoparticles change their morphology depending on the kind of amine used in experiments. On the AC surface modified with ethanolamine, the uniform spherical AuNPs were formed. In case of diethylenetriamine and triethylenetetramine application, the agglomerates of AuNPs are present. The diameter of individual AuNPs did not exceed 15 nm and was bigger as compared with the diameter of particles present in precursor solution (ca. 10 nm).
W pracy przedstawiono wyniki badań spektrofotometrycznych, metodą dynamicznego rozpraszania światła (DLS) oraz mikroskopowe (SEM) dotyczące osadzania nanocząstek złota na węglu aktywnym, modyfikowanym aminami: pierwszorzędową (etanoloamina) i drugorzędowymi (dietylenotriamina i trietylenotetraamina). Wykazano, że ten sposób modyfikacji umożliwia osadzanie nanocząstek złota z roztworu wodnego na powierzchni węgla. W zależności od rodzaju używanej aminy ulega jednak zmianie morfologia osadów nanocząstek. Na powierzchni węgla aktywnego, modyfikowanego etanoloaminą, tworzą się jednorodne cząstki złota o kształcie sferycznym. W przypadku zastosowania dietylenotriaminy oraz trietylenotetraaminy obserwowano powstawanie agregatów nanocząstek. Średnica pojedynczych nanocząstek nie przekraczała 15 nm i była większa od średnicy nanocząstek obecnych w roztworze prekursora (ok. 10 nm).
Źródło:
Archives of Metallurgy and Materials; 2014, 59, 3; 899-903
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Influence of Heat Treatment on the Magnetization Process (within Strong Magnetic Fields) for the Alloy: Fe61Co10Y8Cu1B20
Autorzy:
Gruszka, K.
Nabiałek, M.
Błoch, K.
Powiązania:
https://bibliotekanauki.pl/articles/353778.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
bulk amorphous
Kronmüller method
XRD
structural defects
Opis:
Samples of Fe61Co10Y8Cu1B20 alloy were investigated in the ‘approach to ferromagnetic saturation’ region by using the Kronmüller method. The amorphous material was obtained by radially cooling the molten alloy under a protective atmosphere of inert gas. Following this manufacturing process, static magnetic hysteresis loops were measured for samples, before and after a controlled isothermal annealing process, using a LakeShore vibrating magnetometer (VSM). From analysis of the primary magnetization curves, the distribution of structural defects and the average exchange distance for these defects were determined.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 2A; 499-502
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrochemical Method of Copper Powder Synthesis on Rotating Electrode in the Presence of Surfactants
Autorzy:
Wojtaszek, K.
Cebula, F.
Partyka, B.
Deszcz, P.
Włoch, G.
Socha, R. P.
Woźny, K.
Żabiński, Piotr
Wojnicki, Marek
Powiązania:
https://bibliotekanauki.pl/articles/2203711.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
copper powder
electrochemical synthesis
rotating electrode
ethylene glycol
Opis:
This paper presents a method of synthesizing copper powders by electrochemical method with the use of a rotating working electrode. The influence of the rotation speed of the working electrode, the current density, the concentration of copper ions, and the addition of ethylene glycol on the shape, size, and size distribution of the obtained powders were investigated. Properties of the synthesized powders were characterized by scanning electron microscopy (SEM) and X-ray powder diffractometry (XRD). It has been shown that it is possible to obtain copper powders with a size of 1 µm by an electrochemical method using the rotary cathode, in sulphate bath with addition of ethylene glycol as a surfactant. Increasing current density causes a decrease in the average size of the obtained powder particles. The addition of 2.5% of ethylene glycol prevents the formation of dendritic powders. The change in the concentration of copper ions in the range from 0.01 to 0.15 mol/dm3 in the electrolyte did not show any significant effect on the size of obtained particles. However, higher concentrations of copper limiting the presence of dendritic-shape particles. Changing the speed of rotation of the electrode affects both the size and the shape of synthesized copper powder. For the rotational speed of the electrode of 115 rpm, the obtained powders have a size distribution in the range of 0-3 µm and an average particle size of 1 µm. The particles had a polygonal shape with an agglomeration tendency.
Źródło:
Archives of Metallurgy and Materials; 2023, 68, 1; 375--386
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical properties of Ni-Fe-Cu-P-B alloy produced by two component melt spinning (TCMS)
Autorzy:
Wojciechowska, M.
Ziewiec, K.
Kąc, S.
Prusik, K.
Powiązania:
https://bibliotekanauki.pl/articles/351728.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metallic glasses
scanning electron microscopy (SEM)
nanoindentation
transmission electron microscopy TEM
mechanical properties
Opis:
The aim of this work was to investigate the microstructure and mechanical properties of the two-component melt-spun (TCMS) alloy produced from Ni40Fe40B20 and Ni70Cu10P20 melts. The Ni40Fe40B20, Ni70Cu10P20, Ni55 Fe20 Cu5 P10 B10 alloys were arc-melted. Then the alloys were melt-spun in the two different ways i.e.: by casting from a single-chamber crucible and from the two-chamber crucible. All of the above mentioned alloys were processed in the first way and the Ni40Fe40B20 and Ni70Cu10P20 were simultaneously cast on the copper roller from the two-chamber crucible. The microstructure of the alloy was studied using transmission electron microscopy (TEM), scanning electron microscopy (SEM) with energy dispersive spectrometry (EDS) and light microscopy. The mechanical properties were investigated using tensile testing and nanoindentation. The two-component melt-spun (TCMS) amorphous Ni55 Fe20 Cu5 P10 B10 alloy present hardness, tensile strength and Young modulus on the significantly higher level than for a single phase amorphous Ni55 Fe20 Cu5 P10 B10 alloy and slightly below the corresponding values for the Ni40Fe40B20.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 1; 137-140
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure and Compression Properties of Fe-Cr-B Alloy Manufactured using Laser Metal Deposition
Autorzy:
Joo, Y.-A.
Yoon, T.-S.
Park, S.-H.
Lee, K.-A.
Powiązania:
https://bibliotekanauki.pl/articles/352075.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Fe-Cr-B composite
laser Metal Deposition
bulk type
microstructure
compressive properties
Opis:
Fe-Cr-B alloy is a material with precipitation of boride inside Fe matrix, and it features outstanding hardness and wear resistance properties. However, Fe-Cr-B alloy is a difficult material to process, making it difficult to use as a bulk type structure material which requires delicate shapes. This study attempted to manufacture Fe-Cr-B alloy using a 3D printing process, laser metal deposition. This study also investigated the microstructure, hardness and compression properties of the manufactured alloy. Phase analysis results is confirmed that α-Fe phase as matrix and (Cr, Fe)2B phase as reinforcement phase. In the case of (Cr, Fe)2B phase, differences were observed according to the sample location. While long, coarse, unidirectional needle-type boride phases (~11 μm thickness) were observed in the center area of the sample, relatively finer boride phases (~6 μm thickness) in random directions were observed in other areas. At room temperature compression test results confirmed that the sample had a compression strength is approximately 2.1 GPa, proving that the sample is a material with extremely high strength. Observation of the compression fracture surface identified intergranular fractures in areas with needle-type boride, and transgranular fractures in areas with random borides. Based on this results, this study also reviewed the deformation behavior of LMD Fe-Cr-B alloy in relation to its microstructures.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1459-1462
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł

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