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    Wyświetlanie 1-5 z 5
    Tytuł:
    Comparative analysis of experimental and theoretical zero-field splitting and Zeeman electronic parameters for Fe²⁺ ions in FeX₂·4H₂O (X = F, Cl, Br, I) and [Fe(H₂O)₆](NH₄)₂(SO₄)₂
    Autorzy:
    Zając, M.
    Rudowicz, C.
    Powiązania:
    https://bibliotekanauki.pl/articles/1055040.pdf
    Data publikacji:
    2017-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    33.35.+r
    71.70.Ch
    71.70.Ej
    76.20.+q
    76.30.-v
    76.30.Fc
    87.80.Lg
    Opis:
    Spectroscopic and magnetic properties of Fe²⁺ (3d⁶; S=2) ions at orthorhombic sites in FeX₂·4H₂O (X = F, Cl, Br, I) crystals are compared with those in [Fe(H₂O)₆](NH₄)₂(SO₄)₂ (FASH). The microscopic spin Hamiltonian modeling utilizing the package MSH/VBA enables prediction of the zero-field splitting parameters and the Zeeman electronic ones. Wide ranges of values of the microscopic parameters, i.e. the spin-orbit (λ), spin-spin (ρ) coupling constants, and the crystal-field (ligand-field) energy levels (Δp_{i}) within the ⁵D multiplet are considered to establish the dependence of the zero-field splitting parameters b_{k}^{q} (in the Stevens notation) and the Zeeman factors g_{i} on λ, ρ, and Δp_{i}. By matching the theoretical spin Hamiltonian parameters and the experimental ones measured by EMR, the suitable values of λ, ρ, and Δp_{i} are determined. The novel aspect is prediction of the fourth-rank zero-field splitting parameters and the ρ (spin-spin)-related contributions, not considered in previous studies. The MSH predictions provide guidance for high-magnetic field and high-frequency EMR measurements.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 1; 19-23
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    An NMR study of Pr$\text{}_{0.5}$Ca$\text{}_{0.5}$Mn$\text{}_{1-x}$Ga$\text{}_{x}$O$\text{}_{3}$ (x=0 and 0.03)
    Autorzy:
    Oates, C. J.
    Kapusta, Cz.
    Riedi, P. C.
    Sikora, M.
    Zając, D.
    Rybicki, D.
    Martin, C.
    Yaicle, C.
    Maignan, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/2037129.pdf
    Data publikacji:
    2004
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    76.60.-k
    75.47.Gk
    Opis:
    An NMR study of polycrystalline Pr$\text{}_{0.5}$Ca$\text{}_{0.5}$Mn$\text{}_{1-x}$Ga$\text{}_{x}$O$\text{}_{3}$ (x=0 and 0.03) at 3 K is presented. Zero field spin-echo spectra of the Ga doped compound consist of an overlapping $\text{}^{69,71}$Ga signal at 74~MHz (hyperfine field of 5.3 T), a $\text{}^{55}$Mn double exchange line at 375 MHz (35.5 T) and a weak Mn$\text{}^{3+}$ signal between 400 and 550 MHz. Measurements in an applied field show a step-like increase in the double exchange line intensity, which corresponds to an increase in the amount of the ferromagnetic metallic phase. This coincides with a step-like feature in the bulk magnetization measurements. The effect is similar to that in the previous field dependent $\text{}^{55}$Mn NMR measurements of Pr$\text{}_{0.67}$Ca $\text{}_{0.33}$MnO$\text{}_{3}$. At the demagnetized and remanent state, a variation of spin- spin relaxation time, T$\text{}_{2}$, across the $\text{}^{55}$Mn line, due to the Suhl-Nakamura interaction is observed, which suggests that the ferromagnetic metallic double exchange regions, at liquid helium temperatures, are at least 4 nm in size.
    Źródło:
    Acta Physica Polonica A; 2004, 105, 1-2; 189-195
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A $\text{}^{55}$Mn NMR Study of La$\text{}_{0.33}$Nd$\text{}_{0.33}$Ca$\text{}_{0.34}$Mn O$\text{}_{3}$ with $\text{}^{16}$O and $\text{}^{18}$O
    Autorzy:
    Rybicki, D.
    Kapusta, Cz.
    Riedi, P. C.
    Oates, C. J.
    Sikora, M.
    Zając, D.
    De Teresa, J. M.
    Marquina, C.
    Ibarra, M. R.
    Powiązania:
    https://bibliotekanauki.pl/articles/2037128.pdf
    Data publikacji:
    2004
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    76.60.-k
    75.47.Gk
    Opis:
    A $\text{}^{55}$Mn NMR study of $\text{}^{16}$O and $\text{}^{18}$O containing La$\text{}_{0.33}$Nd$\text{}_{0.33}$Ca$\text{}_{0.34}$Mn O$\text{}_{3}$ is reported. The spin-echo spectra measured at 4.2 K and zero field consist of a double exchange line corresponding to the ferromagnetic metallic regions. The line intensity is more than an order of magnitude lower for the $\text{}^{18}$O compound, which indicates an order of magnitude lower content of the ferromagnetic metallic phase in this compound. The frequency dependence of the spin-spin relaxation time T$\text{}_{2}$ shows a pronounced minimum at the center of the double exchange line of both compounds due to the Suhl-Nakamura interaction, which indicates that the ferromagnetic metallic regions are at least 10~nm in size. The results are discussed in terms of the influence of oxygen isotopic substitution on phase segregation.
    Źródło:
    Acta Physica Polonica A; 2004, 105, 1-2; 183-188
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    NMR Study of (Sr,Ba,La)$\text{}_{2}$Fe$\text{}_{1+y}$Mo$\text{}_{1-y}$O$\text{}_{6}$ Double Perovskites
    Autorzy:
    Zając, D.
    Kapusta, Cz.
    Riedi, P. C.
    Sikora, M.
    Oates, C. J.
    Rybicki, D.
    De Teresa, J. M.
    Serrate, D.
    Marquina, C.
    Ibarra, M. R.
    Powiązania:
    https://bibliotekanauki.pl/articles/2041522.pdf
    Data publikacji:
    2004-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.25.+z
    76.60.-k
    78.70.Gq
    75.47.Gk
    Opis:
    The $\text{}^{95}$Mo and $\text{}^{97}$Mo NMR spin-echo study of (Sr,Ba,La)$\text{}_{2}$Fe$\text{}_{1 +y}$Mo$\text{}_{1-y}$O$\text{}_{6}$ double perovskites is reported. Powder samples of Ba$\text{}_{1.44}$Sr$\text{}_{0.36}$La$\text{}_{0.2}$FeMoO$\text{}_{6}$ and (Ba$\text{}_{0.8}$Sr$\text{}_{0.2}$)$\text{}_{2-2x}$La$\text{}_{x}$#$\text{}_{x}$ Fe$\text{}_{1+y}$Mo$\text{}_{1-y}$O$\text{}_{6}$, where# denotes vacancies, for: x=0, y=0; x=0.1, x=0.2 and x=0.3, y=0 and y=0.2 were measured at 4.2 K and no applied magnetic field. NMR signals are observed at 55-100 MHz for the main line and 30-55 MHz for low-frequency satellite. The main line and the satellite are attributed to the ideal and defect positions of Mo atoms. La and vacancy doping introduce more defects, however, increasing the Fe/Mo ratio decreases the amount of defect Mo sites. La doping causes a satellite pattern at the high frequency side of the spectrum, which is related to different numbers of the La next neighbours. The effect is attributed to an increase in the electron density and the corresponding magnetic moment at the adjacent Mo sites and reveals a local character of the electron doping.
    Źródło:
    Acta Physica Polonica A; 2004, 106, 5; 759-765
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Local Magnetic and Electronic Properties of the A$\text{}_{2}$FeM'O$\text{}_{6}$ (A = Ba, Sr, Ca, M' = Mo, Re) Double Perovskites
    Autorzy:
    Zając, D.
    Sikora, M.
    Prochazka, V.
    Borowiec, M.
    Stępień, J.
    Kapusta, Cz.
    Riedi, P. C.
    Marquina, C.
    De Teresa, J. M.
    Ibarra, M. R.
    Powiązania:
    https://bibliotekanauki.pl/articles/2047344.pdf
    Data publikacji:
    2007-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.30.-m
    76.60.-k
    76.60.Jx
    78.80.En
    Opis:
    The results of a combined NMR, X-ray absorption spectroscopy and X-ray magnetic cirrcular dichroism study of the AA'FeMoO$\text{}_{6}$ and AA'FeReO$\text{}_{6}$ double perovskites are presented. They revealed a dependence of electronic and magnetic properties, including a d-electron transfer between Fe and Mo sites, on the structural tolerance factor. The maximum value of the 4d Mo electron occupation and the corresponding Mo moment is obtained for the tolerance factor of unity. This corresponds to the maximum strength of the magnetic interaction and, respectively, to the Curie temperature. The dominant T$\text{}^{5}\text{}^{/}\text{}^{2}$ type temperature dependence of the Mo hyperfine field reveals the half-metallicity of the AA'FeMoO$\text{}_{6}$ compounds. Antisite defects and antiphase boundaries have been identified in NMR measurements and the strength of their magnetic coupling have been determined. A considerable orbital contribution to the Re and Fe magnetic moments were found in the NMR and X-MCD measurements on the AA'FeReO$\text{}_{6}$ compounds. Its magnitude decreases with increasing structural tolerance factor and is correlated with their magnetic anisotropy.
    Źródło:
    Acta Physica Polonica A; 2007, 111, 6; 797-820
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-5 z 5

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