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Wyświetlanie 1-15 z 15
Tytuł:
A sixth-order finite volume method for the 1D biharmonic operator: Application to intramedullary nail simulation
Autorzy:
Costa, R.
Machado, G. J.
Clain, S.
Powiązania:
https://bibliotekanauki.pl/articles/330268.pdf
Data publikacji:
2015
Wydawca:
Uniwersytet Zielonogórski. Oficyna Wydawnicza
Tematy:
finite volume method
polynomial reconstruction operator
harmonic operator
biharmonic operator
high order method
Opis:
A new very high-order finite volume method to solve problems with harmonic and biharmonic operators for one-dimensional geometries is proposed. The main ingredient is polynomial reconstruction based on local interpolations of mean values providing accurate approximations of the solution up to the sixth-order accuracy. First developed with the harmonic operator, an extension for the biharmonic operator is obtained, which allows designing a very high-order finite volume scheme where the solution is obtained by solving a matrix-free problem. An application in elasticity coupling the two operators is presented. We consider a beam subject to a combination of tensile and bending loads, where the main goal is the stress critical point determination for an intramedullary nail.
Źródło:
International Journal of Applied Mathematics and Computer Science; 2015, 25, 3; 529-537
1641-876X
2083-8492
Pojawia się w:
International Journal of Applied Mathematics and Computer Science
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Extraction of Ziziphus lotus fruit syrups: effect of enzymatic extraction and temperature on their rheological and chemical properties
Autorzy:
Letaief, T.
Mejri, J.
Ressureicao, S.
Abderrabba, M.
Costa, R.
Powiązania:
https://bibliotekanauki.pl/articles/2083051.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Instytut Agrofizyki PAN
Tematy:
Ziziphus lotus L.
syrup
shear-thinning
rheology
enzymatic extraction
Opis:
Fruit syrups are attracting increasing interest in the food industry. Ziziphus lotus fruit syrups were elaborated through the traditional and enzymatic methods with 30, 50 and 70° Brix. A chemical analysis revealed that Ziziphus lotus fruit powder and syrups present a potential source of energy through their relatively higher content of carbohydrates. Rheological oscillatory tests showed that syrups of 30°Brix demonstrate a viscous type of behaviour, the 70°Brix syrups possess an elastic behaviour, while the 50°Brix syrups present a mixed behaviour over the temperature range of 20 to 80°C. These syrups did not demonstrate any thixotropy or time dependence of viscosity. The complex viscosity was described successfully with a mathematical model that incorporates both independent variables, with an Arrhenius-type dependence on temperature, with an activation energy of 21.94 kJ mol-1 for the whole Brix range. The flow behaviour evaluation of the 30 and 50°Brix showed that these are shear-thinning fluids, tending to Newtonian fluids at higher temperatures. The dynamic viscosity was well described by the power law and the dependence of its parameters on temperature was adequately described by a Turian approach. The syrups of Ziziphus lotus fruit demonstrated a potential for further beneficial research with a view to obtaining a commercial food product.
Źródło:
International Agrophysics; 2021, 35, 1; 31-40
0236-8722
Pojawia się w:
International Agrophysics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Measurement Precision Under Repeatability Conditions of a Batch of Sound Power Assessment for Blenders in Reverberation Room
Autorzy:
Costa-Felix, R. P. B.
Powiązania:
https://bibliotekanauki.pl/articles/177133.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
metrology
measurement precision
sound power assessment
reverberation room
Opis:
A set of sound power assessments was performed to determine measurement precision in specified conditions by the comparison method in a reverberation room with a fixed position array of six microphones. Six blenders (or mixers) and, complementary, a reference sound source were the noise sources. Five or six sound power calculations were undertaken on each noise source, and the standard deviation (sr) was computed as “measurement precision under repeatability conditions” for each octave band from 125 Hz to 8 kHz, and in dB(A). With the results obtained, values of sr equal 1.0 dB for 125 Hz and 250 Hz, 0.8 dB for 500 Hz to 2 kHz, and 0.5 dB for 4 kHz and 8 kHz. Those can be considered representative as sound power precision for blenders according to the measurement method used. The standard deviation of repeatability for the A-weighted sound power level equals 0.6 dB. This paper could be used for house or laboratory tests to check where their uncertainty assessment for sound power determination is similar or not to those generated at the National Metrology Institute.
Źródło:
Archives of Acoustics; 2016, 41, 3; 591-597
0137-5075
Pojawia się w:
Archives of Acoustics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Water-based poly(urethane-urea) dispersions —meeting the European Union legislation
Dyspersje wodne poli(uretanowo-mocznikowe) w świetle wymagań prawodawstwa Unii Europejskiej
Autorzy:
Fernandes, I. P.
Costa, M. R.
Ferreira, M. J.
Barreiro, M. F.
Powiązania:
https://bibliotekanauki.pl/articles/947121.pdf
Data publikacji:
2015
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
poly(urethane-urea)
water-based dispersion
European Union legislation
N-methyl-pyrrolidone free products
poli(uretano-mocznik)
dyspersja wodna
prawodawstwo Unii Europejskiej
produkty wolne od N-metylo-pirolidonu
Opis:
This article discusses the synthesis methods of water-based poly(urethane-urea) dispersions (PUD), which over the past few decades have developed a solid reputation for high performance applications, particularly in the field of adhesives and coatings. PUDs are mostly environmentally compatible products since they do not contain or contain only low amounts of volatile organic compounds (VOC). This is an important feature in view of the present environmental policies, where governments and internal agencies are placing emphasis on developing sustainable processes, improving work conditions and reducing emissions of toxic and polluting substances into the atmosphere. In this context, this paper will discuss the main approaches applied to PUD synthesis in order to meet severe environmental restrictions resulting from the EU legislation.
Omówiono metody syntezy dyspersji wodnych poli(uretanowo-mocznikowych) (PUD), które znajdują coraz szersze zastosowanie, szczególnie w produkcji klejów i powłok. PUD są na ogół produktami bezpiecznymi dla środowiska, ze względu na brak lub małą zawartość lotnych związków organicznych (VOC), co jest ważne w świetle obecnej polityki ochrony środowiska. Przedstawione w pracy metody syntezy PUD uwzględniają wymagania wynikające z prawodawstwa Unii Europejskiej w zakresie spełniania surowych ograniczeń środowiskowych.
Źródło:
Polimery; 2015, 60, 9; 536-540
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Level-Based Approach to Prioritize Telecommunications R&D
Autorzy:
Fialho, J.
Godinho, P.
Costa, J. P.
Afonso, R.
Regalado, J. G.
Powiązania:
https://bibliotekanauki.pl/articles/307952.pdf
Data publikacji:
2008
Wydawca:
Instytut Łączności - Państwowy Instytut Badawczy
Tematy:
multicriteria decision support
R&D project evaluation
Opis:
In this paper, an approach to evaluate R&D projects in telecommunications is presented. These Project have particular features that cannot be properly incorporated by classical evaluation methods. This approach incorporates different criteria, both quantitative and qualitative, and also management flexibility and uncertainty. Thus, it is an approach that can be applied to real data of R&D projects in a telecommunications company.
Źródło:
Journal of Telecommunications and Information Technology; 2008, 4; 40-43
1509-4553
1899-8852
Pojawia się w:
Journal of Telecommunications and Information Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Correlation between clinical efficacy on pruritus and serum interleukin-31 levels in dogs with atopic dermatitis treated with lokivetmab
Autorzy:
Calesso, J.R.
Marques, V.S.
de Carvalho, O.V.
Costa-Val, A.P.
Powiązania:
https://bibliotekanauki.pl/articles/16647579.pdf
Data publikacji:
2023
Wydawca:
Polska Akademia Nauk. Czasopisma i Monografie PAN
Tematy:
atopic dermatitis
interleukin-31
lokivetmab
monoclonal antibody
pruritus
Opis:
Studies on serum interleukin (IL)-31 levels in dogs with atopic dermatitis (AD) and their correlation with disease severity are limited. To the author’s knowledge, there are no studies that measured serum IL-31 in dogs treated with lokivetmab injections, a selective inhibitor of this key cytokine in pruritus. The aim of the study was to evaluate serum IL-31 levels in dogs treated with lokivetmab and correlate it with the severity of canine atopic dermatitis using the pruritus visual analog scale (pVAS) and canine atopic dermatitis extent and severity index (CADESI-04). Ten client-owned dogs diagnosed with AD received two injections of lokivetmab four weeks apart. Disease severity was assessed using the pVAS and CADESI-04 scores before and after both injections. In addition, canine serum IL-31 levels were measured at the same moments. Serum IL-31 was detected in all dogs in the study. There was a significant reduction in pVAS scores and serum IL-31 after administrations. However, there was no difference in CADESI-04 scores, and there was no significant correlation between CADESI-04 scores and serum IL-31 in dogs diagnosed with AD. Nonetheless, a significant positive correlation was observed between the pVAS scores and serum IL-31 levels with lokivetmab therapy, which reinforces the role of IL-31 in the pathogenesis of pruritus in dogs with AD. The data presented here provide further evidence that IL-31 is directly involved in pruritus pathogenesis in dogs with AD. In addition, blocking IL-31 has a significant antipruritic effect, but has no influence on skin lesion severity and extension.
Źródło:
Polish Journal of Veterinary Sciences; 2023, 26, 2; 231-238
1505-1773
Pojawia się w:
Polish Journal of Veterinary Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Comparative simulation study of production scheduling in the hybrid and the parallel flow
Autorzy:
Varela, M. L. R.
Trojanowska, J.
Carmo-Silva, S.
Costa, N. M. L.
Machado, J.
Powiązania:
https://bibliotekanauki.pl/articles/407017.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
approach for supporting manufacturing scheduling decision making
heuristics
hybrid flow shop
parallel flow shops
makespan
Opis:
Scheduling is one of the most important decisions in production control. An approach is proposed for supporting users to solve scheduling problems, by choosing the combination of physical manufacturing system configuration and the material handling system settings. The approach considers two alternative manufacturing scheduling configurations in a two stage product oriented manufacturing system, exploring the hybrid flow shop (HFS) and the parallel flow shop (PFS) environments. For illustrating the application of the proposed approach an industrial case from the automotive components industry is studied. The main aim of this research to compare results of study of production scheduling in the hybrid and the parallel flow, taking into account the makespan minimization criterion. Thus the HFS and the PFS performance is compared and analyzed, mainly in terms of the makespan, as the transportation times vary. The study shows that the performance HFS is clearly better when the work stations’ processing times are unbalanced, either in nature or as a consequence of the addition of transport times just to one of the work station processing time but loses advantage, becoming worse than the performance of the PFS configuration when the work stations’ processing times are balanced, either in nature or as a consequence of the addition of transport times added on the work stations’ processing times. This means that physical layout configurations along with the way transport time are including the work stations’ processing times should be carefully taken into consideration due to its influence on the performance reached by both HFS and PFS configurations.
Źródło:
Management and Production Engineering Review; 2017, 8, 2; 69-80
2080-8208
2082-1344
Pojawia się w:
Management and Production Engineering Review
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A 3D trabecular bone homogenization technique
Autorzy:
Marques, Marco Costa
Belinha, J.
Oliveira, A. F.
Manzanares Cespedes, M.C.
Natal Jorge, R.M.
Powiązania:
https://bibliotekanauki.pl/articles/27324130.pdf
Data publikacji:
2020
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
fabric tensor
homogenization technique
multiscale
bone
tensor tkaniny
technika homogenizacji
wieloskalowe
kość
Opis:
Purpose: Bone is a hierarchical material that can be characterized from the microscale to macroscale. Multiscale models make it possible to study bone remodeling, inducing bone adaptation by using information of bone multiple scales. This work proposes a computationally efficient homogenization methodology useful for multiscale analysis. This technique is capable to define the homogenized microscale mechanical properties of the trabecular bone highly heterogeneous medium. Methods: In this work, a morphology-based fabric tensor and a set of anisotropic phenomenological laws for bone tissue was used, in order to define the bone micro-scale mechanical properties. To validate the developed methodology, several examples were performed in order to analyze its numerical behavior. Thus, trabecular bone and fabricated benchmarks patches (representing special cases of trabecular bone morphologies) were analyzed under compression. Results: The results show that the developed technique is robust and capable to provide a consistent material homogenization, indicating that the homogeneous models were capable to accurately reproduce the micro-scale patch mechanical behavior. Conclusions: The developed method has shown to be robust, computationally less demanding and enabling the authors to obtain close results when comparing the heterogeneous models with equivalent homogenized models. Therefore, it is capable to accurately predict the micro-scale patch mechanical behavior in a fraction of the time required by classic homogenization techniques.
Źródło:
Acta of Bioengineering and Biomechanics; 2020, 22, 3; 139--152
1509-409X
2450-6303
Pojawia się w:
Acta of Bioengineering and Biomechanics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A comparative study on the performance of radiation detectors from the HgI2 crystals grown by different techniques
Autorzy:
Martins, J. F. T.
Costa, F. E.
dos Santos, R. A.
de Mesquita, C. H.
Hamada, M. M.
Powiązania:
https://bibliotekanauki.pl/articles/146916.pdf
Data publikacji:
2012
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
crystal growth
iodide mercury crystal
physical vapor transport (PVT)
radiation detector
semiconductor crystal
Opis:
In this work, the establishment of a technology for HgI2 purification and crystal growth is described, aiming at a future application of this crystal as a room temperature radiation semiconductor detector. Two methods of crystal growth were studied in the development of this work: (1) physical vapor transport (PVT) and (2) saturated solution from dimethylsulphoxide (DMSO) complexes. In order to evaluate the crystals obtained using each of these methods, systematic measurements were carried out for determining the stoichiometry, structure, orientation, surface morphology and impurity of the crystal. The influence of these physicochemical properties of the crystals developed was evaluated in terms of their performance as a radiation detector. The best response to radiation was found for the crystals grown by the PVT technique. Significant improvement in the performance of HgI2 radiation detector was found, purifying the crystal by means of two successive growths by the PVT technique.
Źródło:
Nukleonika; 2012, 57, 4; 555-562
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Cost-effective approach to lung cancer risk for a radiological dispersal device (RDD) scenario
Autorzy:
Costa, Karolina P. S.
Lima, Sergio X.
Brum, Tercio
Lima, Zelmo R.
Amorim, Jose C. C.
Healy, Matthew J. F.
Vital, Helio C.
Prah, Matjaž
Andrade, Edson R.
Powiązania:
https://bibliotekanauki.pl/articles/146560.pdf
Data publikacji:
2019
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
environment
contamination
radiation
cost-effectiveness
risk
Opis:
A release of radioactive material into the environment can lead to hazardous exposure of the population and serious future concerns about health issues such as an increased incidence of cancer. In this context, a practical methodology capable of providing useful basic information from the scenario can be valuable for immediate decisions and future risk assessment. For this work, the simulation of a radiological dispersal device (RDD) filled with americium-241 was considered. The radiation dose simulated by the HotSpot code was used as an input to the epidemiological equations from BEIR V producing the data used to assess the risk of lung cancer development. The methodology could be useful in providing training for responders aimed to the initial support addressed to decision-making for emergency response at the early phase of an RDD scenario. The results from the simulation allow estimating (a) the size of the potentially affected population, (b) the type of protection action considering gender and location of the individuals, (c) the absorbed doses, (d) the matrix of lung cancer incidence predictions over a period of 5 years, and (e) the cost-effectiveness in the initial decision environment.
Źródło:
Nukleonika; 2019, 64, 4; 123-129
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Shot Peening With Glass Microspheres on the Fatigue Behavior of a Low Carbon Steel
Autorzy:
de Lacerda, J. C.
Pereira, I. R.
Costa, J. M. G.
Pinto, J. S.
Souza, H. F. M.
Fonseca, M. A.
Powiązania:
https://bibliotekanauki.pl/articles/352156.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
fatigue
shot peening
Wöhler curve
low carbon steel
glass microspheres
Opis:
The present work has the objective of studying the effect of shot peening with glass microspheres on SAE 1020 steel in its resistance to fatigue. Fatigue tests were carried out by rotary bending with load control and loading on balance in specimens with and without shot peening. A rotation speed of approximately 750 rpm (12.5 Hz) was employed in the fatigue tests. Vickers microhardness tests were performed in order to verify the surface hardening produced by shot peening with glass microspheres. Analysis of the steel surface and fatigue fractures was performed using scanning electron microscopy (SEM). Fatigue tests were performed in order to obtain S-N curves (Wöhler curves). It was observed that shot peening with glass microspheres improved the fatigue strength of the steel at high cycle.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1513-1518
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Air-assistance in spray booms which have different spray volumes and nozzle types for chemically controlling Spodoptera frugiperda on corn
Autorzy:
Gimenes, M.J
Raetano, C.G.
Ferreira, M.H
Pereira-Prado, E.
Souza-Christovam, R.
Tourino-Rezende, D.
Almeida-Costa, S.I.
Powiązania:
https://bibliotekanauki.pl/articles/66410.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Opis:
The study aimed to evaluate the performance of air assistance in spray booms using different types of nozzles and spray volumes. We took into account spray deposits, fall armyworm control and crop corn performance in a narrow row cropping system. The experiment was carried out at the experimental area of Sao Paulo State University, Botucatu/SP, Brazil, during the 2008/2009 agricultural season, in randomized blocks with a factorial scheme (2×2+1) and four replications. Two spray nozzles (flat fan nozzle and hollow cone nozzle) were tested, combined with two air assistance levels in the spray boom (with and without air assistance) and a treatment control. In the experimental spraying, Spinosad insecticide was sprayed in amounts of 48 g active substance (a.s.)/ha. The air assistance in the spray boom increased the spray deposits in the V4 growth stage of the corn plants. Moreover, the application of this technology showed higher efficiency on fall armyworm control, reaching a 100% level 15 days after spraying, in the V10 growth stage of the plants. The hollow cone nozzle increased the spray deposit level on the corn plants compared with the flat fan nozzle, at growth stage V4. However, the flat fan nozzle, combined with air assistance technology, was more effective for controlling fall armyworm in the same growth stage (V4), although the hollow cone nozzle increased the deposit levels on the plants. All the technologies tested in the study promoted a reduction of plant damage from fall armyworm attack. Corn productivity is directly related to the control efficiency of fall armyworm.
Źródło:
Journal of Plant Protection Research; 2012, 52, 2
1427-4345
Pojawia się w:
Journal of Plant Protection Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Simulated nuclear contamination scenario, solid cancer risk assessment, and support to decision
Autorzy:
Lima, Sergio X.
Costa, Karolina P. S.
Lima, Zelmo R.
Rother, Fagner C.
Araujo, Olga M. O.
Vital, Helio C.
Brum, Tercio
Junior, Wilson F. R. S.
Amorim, Jose Carlos C.
Healy, Matthew J. F.
Andrade, Edson R.
Powiązania:
https://bibliotekanauki.pl/articles/146554.pdf
Data publikacji:
2019
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
improvised nuclear device
IND
induced cancer
risk assessment
decision
ocena ryzyka
decyzja
Opis:
The detonation of an (hypothetical) improvised nuclear device (IND) can generate atmospheric release of radioactive material in the form of particles and dust that ultimately contaminate the soil. In this study, the detonation of an IND in an urban area was simulated, and its effects on humans were determined. The risk of solid cancer development due to radiation was calculated by taking into account prompt radiation and whole-body exposure of individuals near the detonation site up to 10 km. The excess relative risk (ERR) of developing solid cancer was evaluated by using the mathematical relationships from the Radiation Effects Research Foundation (RERF) studies and those from the HotSpot code. The methodology consists of using output data obtained from simulations performed with the HotSpot health physics code plugging in such numbers into a specific given equation used by RERF to evaluate the resulting impact. Such a preliminary procedure is expected to facilitate the decision-making process significantly.
Źródło:
Nukleonika; 2019, 64, 2; 41-48
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Development of an irradiation system for a small size continuous run multipurpose gamma irradiator
Autorzy:
Calvo, W. A. P.
Rela, P. R.
Napolitano, C. M.
Kodama, Y.
Omi, N. M.
da Costa, F.
de Andrade e Silva, L. G.
Powiązania:
https://bibliotekanauki.pl/articles/148041.pdf
Data publikacji:
2009
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
multipurpose irradiator
gamma irradiator
compact irradiator
cobalt-60 irradiator
gamma facility
Opis:
The Radiation Technology Center from IPEN-CNEN/SP, Brazil, developed a revolutionary design and national technology, a small-sized continuous run and multipurpose industrial gamma irradiator, to be used as a demonstration facility for manufacturers and contract service companies, which need economical and logistical in-house irradiation system alternatives. Also, to be useful for supporting the local scientific community on development of products and process using gamma radiation, assisting the traditional and potential users on process validation, training and qualification of operators and radioprotection officers. The developed technology for this facility consists of a continuous tote box transport system, comprising a single concrete vault, where the automated transport system of products inside and outside of the irradiator utilizes a rotating door, integrated with the shielding, avoiding the traditional maze configuration. Covering 76 m2 of floor area, the irradiator design is a product overlap sources and the maximum capacity of cobalt-60 wet sources is 37 PBq. The performed qualification program of this multipurpose irradiator was based on AAMI/ISO 11137 standard, which recommends the inclusion of the following elements: installation and process qualification. The initial load of the multipurpose irradiator was 3.4 PBq with 13 cobalt-60 sources model C-188, supplied by MDS Nordion – Canada. For irradiator dose optimization, the source distribution was done using the software Cadgamma developed by IPEN-CNEN/SP. The polymethylmetacrylate (PMMA) dosimeter system, certified by the International Dose Assurance Service (IDAS) of the International Atomic Energy Agency (IAEA) was used for irradiator dose mapping. The economic analysis, performance concerning with dose uniformity and cobalt-60 utilization efficiency were calculated and compared with other commercial gamma irradiators available on the market.
Źródło:
Nukleonika; 2009, 54, 2; 93-97
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, characterization and catalytic properties of SAPO-11 molecular sieve synthesized in hydrothermal media using di-isopropylamine as template
Autorzy:
Chellappa, T.
Costa, M. J. F.
Nascimento, W. A.
Ferreira De Lima, L.
Bassan, I. A.
Tavares, M.
Fernandes, V. J.
Menezes, A.
Guilherme Meira, L.
Telesforo Nóbrega De Medeiros, J.
Maribondo Do Nascimento, R.
Powiązania:
https://bibliotekanauki.pl/articles/200372.pdf
Data publikacji:
2014
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
microporous materials
SAPO-11
characterization
catalytic activity
molecular sieves
Opis:
A microporous SAPO-11 Molecular sieve was successfully synthesized by the hydrothermal method, using a single agent, as an organic template: di-isopropylamine (DIPA). The obtained solid was calcined at 550C for three hours, after which the flow of nitrogen was exchanged for that of synthetic air and submitted for another ten hours of calcination, so as to remove the single agent: di-isopropylamine, which after the removal of the template could be observed by the high crystallization of the sample. Furthermore, the molecular sieve was characterized by XRD, SEM, TG-DTG and N2 adsorption desorption (BET analysis). The obtained catalyst proved to have a high potential catalytic activity and selectivity, through the obtained characterization results, exhibiting good hydrothermal stability. The catalytic performance of SAPO-11 was tested by the deactivation/regenerability of the coked sample, furthered by cracking of n-hexane reaction and high olefins selectivity was obtained.
Źródło:
Bulletin of the Polish Academy of Sciences. Technical Sciences; 2014, 62, 3; 481-488
0239-7528
Pojawia się w:
Bulletin of the Polish Academy of Sciences. Technical Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
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