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Wyświetlanie 1-15 z 15
Tytuł:
Boundary value problems for n-th order differential inclusions with four-point integral boundary conditions
Autorzy:
Ahmad, B.
Ntouyas, S. K.
Powiązania:
https://bibliotekanauki.pl/articles/255975.pdf
Data publikacji:
2012
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Wydawnictwo AGH
Tematy:
differential inclusions
four-point integral boundary conditions
existence
nonlinear alternative of Leray Schauder type
fixed-point theorems
Opis:
In this paper, we discuss the existence of solutions for a four-point integral boundary value problem of n-th order differential inclusions involving convex and non-convex multivalued maps. The existence results are obtained by applying the nonlinear alternative of Leray Schauder type and some suitable theorems of fixed point theory.
Źródło:
Opuscula Mathematica; 2012, 32, 2; 205-226
1232-9274
2300-6919
Pojawia się w:
Opuscula Mathematica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and properties of vinylpyrrolidone/ (trimethoxysilyl)propyl methacrylate gels containing different amounts of crosslinking agent
Synteza i właściwości żelu N-winylopirolidon/metakrylan3-(trimetoksysililo)propylu z różną zawartością czynnika sieciującego
Autorzy:
Mohammed, A. H.
Ahmad, M. B.
Ibrahim, N. A.
Zainuddin, N.
Powiązania:
https://bibliotekanauki.pl/articles/947044.pdf
Data publikacji:
2018
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
high conversion copolymers
swelling parameters
mechanical properties
oxygen permeability
crosslinking density
kopolimery o wysokim stopniu konwersji
parametry pęcznienia
właściwości mechaniczne
przepuszczalność tlenu
gęstość sieciowania
Opis:
High conversion copolymers containing 90 wt % of N-vinylpyrrolidone (NVP) and 10 wt % of 3-(trimethoxysilyl)propyl methacrylate (TMSPM) with 0, 1, 2, 3 and 4 wt % (in conversion to mass of NVP/TMSPM) of ethylene glycol dimethacrylate (EGDMA) as crosslinker have been successfully synthesized. Proton nuclear magnetic resonance (1H NMR) and Fourier transform infrared spectroscopy (FT-IR) were employed to characterize the resulting copolymers. The effect of EGDMA amount on the mechanical and thermal properties, swelling parameters, clarity, and oxygen permeability of the prepared xerogels and hydrogels were studied. 3 wt % of EGDMA is required to obtain clear xerogels and hydrogels. The water content (EWC), volume fraction of polymer (φ2) and weight loss during swelling decrease with increasing EGDMA content. Young’s and shear modulus (E and G) increase as EGDMA content increases, the values of E and G are 0.570–3.531 MPa and 0.217–1.359 MPa, respectively. The hydrogels were characterized in terms of modulus crosslinking density (ve and vt) and polymer-solvent interaction parameters (χ). The results are 0.220–0.613 mol/dm3 for ve, 0.105–0.441 mol/dm3 for vt, and 0.595–0.822 for χ. Thermal properties enhance by adding EGDMA whereas the oxygen permeability (P) of hydrogels decreases from 48.6 to 44.3 as water content decrease from 70.3 to 55.1.
Kopolimery zawierające 90 % mas. N-winylopirolidonu (NVP) i 10 % masmetakrylanu 3-(trimetoksysililo)propylu (TMSPM) z udziałem 0, 1, 2, 3 i 4 % mas. (w przeliczeniu na masę NVP/TMSPM) dimetakrylanu glikolu etylenowego (EGDMA) jako środka sieciującego zsyntetyzowano z wysokim stopniem konwersji. Otrzymane kopolimery charakteryzowano metodami protonowego rezonansu jądrowego (H1 NMR) i spektroskopii w podczerwieni (FT-IR). Badano wpływ udziału środka sieciującego na właściwości mechaniczne i termiczne, parametry pęcznienia, klarowność i przepuszczalność tlenu wytworzonych hydro- i kserożeli. Stwierdzono, że dodatek już 3 % mas. EGDMA wystarcza do uzyskania klarownego żelu, a w miarę zwiększania zawartości EGDMA zmniejsza się zawartość wody (EWC), ułamek objętości polimeru (φ2) oraz strata masy w procesie pęcznienia żelu NVP/TMSPM. Wartość modułu zarówno Younga (E), jak i ścinania (G) zwiększa się (E = 0,570–3,531 MPa, G = 0,217–1,359 MPa) wraz ze wzrostem udziału EGDMA w kompozycji. Wytworzone hydrożele charakteryzowano za pomocą modułów gęstości sieciowania (ve = 0,220–0,613 mol/dm3, vt = 0,105–0,441 mol/dm3) i parametru oddziaływania polimer-rozpuszczalnik (χ = 0,595–0,822). Właściwości termiczne otrzymanych hydrożeli zawierających EGDMA poprawiły się wraz ze zmniejszeniem zawartości wody (70,3–55,1), natomiast przepuszczalność tlenu się pogorszyła (P = 48,6–44,3).
Źródło:
Polimery; 2018, 63, 9; 577-585
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and monomer reactivity ratios of acrylamide with 3-(trimethoxysilyl)propyl methacrylate and tris(methoxyethoxy)vinylsilane copolymers
Współczynniki reaktywności monomerów w syntezie kopolimerów akryloamidu, metakrylanu 3-(trimetoksysililo)propylu i tris(metoksyetoksy)-winylosilanu
Autorzy:
Mohammed, A. H.
Ahmad, M. B.
Ibrahim, N. A.
Zainuddin, N.
Powiązania:
https://bibliotekanauki.pl/articles/947173.pdf
Data publikacji:
2016
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
vinylsilane monomers
acrylamide
reactivity ratios
sequence distribution
sekwencja monomerów
Opis:
Copolymers of acrylamide (AM) with 3-(trimethoxysilyl)propyl methacrylate (TMSPMA) and tris(methoxyethoxy)vinylsilane (TMEVS) with different compositions were synthesized at low conversion by free radical polymerization in dimethylformamide (DMF) using benzoyl peroxide (BPO) as an initiator. The copolymers were characterized by Fourier transform infrared spectroscopy (FT-IR), and their thermal properties were studied by differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA). The copolymers composition was determined by elemental analysis. The monomer reactivity ratios were estimated by linearization methods proposed by Fineman-Ross and Kelen-Tudos, the intersection method proposed by Mayo-Lewis and nonlinear method proposed by curve fitting procedure. The derived reactivity ratios (r1, r2) are: 1.87, 0.80 for TMSPMA-co-AM and 0.22, 1.21 for TMEVS-co-AM. Both copolymers formed blocks of one of the monomer units. The microstructure of copolymers and sequence distribution of monomers in the copolymers were calculated by statistical method based on the average reactivity ratios and found that these values are in agreement with the derived reactivity ratios.
Kopolimery akryloamidu (AM) z metakrylanem 3-(trimetoksysililo)propylu (TMSPMA) itris(metoksyetoksy)winylosilanem (TMEVS), o różnych składach, zsyntetyzowano w warunkach małej konwersji metodą wolnorodnikowej polimeryzacji w dimetyloformamidzie (DMF), z zastosowaniem nadtlenku benzoilu (BPO) jako inicjatora. Otrzymane kopolimery charakteryzowano za pomocą spektroskopii w podczerwieni z transformacją Fouriera (FT-IR), różnicowej kalorymetrii skaningowej (DSC) oraz analizy termograwimetrycznej (TGA). Skład kopolimerów ustalono metodą analizy elementarnej. Współczynniki reaktywności monomerów oszacowano metodami linearyzacji zaproponowanymi przez: Finemana-Rossa, Kelena-Tudosa, Mayo-Lewisa i metodą nieliniową z zastosowaniem procedury dopasowania krzywej. Otrzymane współczynniki reaktywności (r1, r2) wynosiły: 1,87 i 0,80 dla TMSPMA-co-AM oraz 1,21 i 0,22 dla TMEVS-co-AM. Oba kopolimery miały budowę złożoną zbloków utworzonych z jednostek monomerów składowych. Mikrostrukturę oraz sekwencję monomerów w kopolimerach wyznaczono metodą statystyczną na podstawie średnich współczynników reaktywności. Stwierdzono zgodność obliczeń z wartościami otrzymanymi doświadczalnie.
Źródło:
Polimery; 2016, 61, 11-12; 758-765
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, characterization and thermal polymerization of new 3,4-dihydro-2H-1,3-naphthoxazine monomers
Synteza, charakterystyka i polimeryzacja termiczna nowych monomerów 3,4-dihydro-2H-1,3-naftoksazynowych
Autorzy:
Gabbas, A. U. G.
Ahmad, M. B. H.
Zainuddin, N.
Ibrahim, N. A.
Powiązania:
https://bibliotekanauki.pl/articles/946991.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Chemii Przemysłowej
Tematy:
1,3-naphthoxazine
polynaphthoxazine
thermal polymerization
thermal properties
1,3-naftoksazyna
polinaftoksazyna
polimeryzacja termiczna
właściwości termiczne
Opis:
Two new 1,3-naphthoxazine monomers (M-A and M-B) were synthesized via a modified stepwise procedure in which methylene bromide was used for the ring-closure reaction. Condensation of 2-hydroxy-1-naphthaldehyde with 1,6-hexamethylenediamine or 1,4-phenylenediamine gives imine compounds, which were converted to 2-hydroxynaphthylamines by reduction with NaBH4 in methanol. Ring-closure reaction between the 2-hydroxynaphthylamines and methylene bromide results in the formation of 1,3-naphthoxazine monomers M-A or M-B with good yields. The structures of the synthesized monomers were confirmed using different spectroscopic techniques (including FT-IR, 1H NMR and 13C NMR), mass spectrometry, and elemental analysis. Thermal polymerization of the monomers was investigated by FT-IR and differential scanning calorimetry (DSC). Both the 1,3-naphthoxazine monomers undergo ring-opening polymerization, leading to the formation of the corresponding polynaphthoxazines [P(M-A) and P(M-B)]. The thermal stability of the polynaphthoxazines was thereafter studied by thermogravimetric analysis (TGA).
Za pomocą zmodyfikowanej trójetapowej syntezy, w której do reakcji zamknięcia pierścienia zastosowano bromek metylenu, otrzymano dwa nowe monomery 1,3-naftoksazyny (M-A i M-B). Kondensacja 2-hydroksy-1-naftaldehydu z 1,6-heksametylenodiaminą lub 1,4-fenylenodiaminą pozwala na wytworzenie związków iminowych, które następnie przez redukcję NaBH4 w metanolu są przekształcane w 2-hydroksynaftylaminy. Reakcja zamknięcia pierścienia pomiędzy 2-hydroksynaftylaminą i bromkiem metylenu prowadzi do utworzenia z dobrymi wydajnościami monomerów 1,3-naftoksazyny M-A i M-B. Struktury zsyntetyzowanych monomerów potwierdzono stosując różne techniki spektroskopowe, spektroskopię masową oraz analizę elementarną. Polimeryzację termiczną monomerów badano za pomącą spektroskopii w podczerwieni z transformatą Fouriera (FT-IR) i różnicowej kalorymetrii skaningowej (DSC). Oba monomery 1,3-naftoksazyny uległy polimeryzacji z otwarciem pierścienia dając odpowiednie polinaftoksazyny [P(M-A) i P(M-B)]. Za pomocą analizy termograwimetrycznej (TGA) zbadano stabilność termiczną otrzymanych polinaftoksazyn.
Źródło:
Polimery; 2017, 62, 2; 86-92
0032-2725
Pojawia się w:
Polimery
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Controllability Analysis of Reactive Magnetron Sputtering Process
Autorzy:
Ahmad, Z.
Abdallah, B.
Powiązania:
https://bibliotekanauki.pl/articles/1400186.pdf
Data publikacji:
2013-01
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
02.30.Yy
68.55.-a
Opis:
Reactive magnetron sputtering deposition is one of the major established techniques for deposition of both metallic and nonmetallic thin films on various substrates; it is a very nonlinear process, and exhibits hysteresis behavior with respect to the reactive gas flow. This nonlinearity is characterized by a sudden change in sputtering rate and fraction of compound formation. Most of the problems encountered in the preparation of compound films by reactive sputtering are due to the hysteresis effect. The industrial applications request high rate deposition processes. To meet this demand, it is necessary to have a very good control system of such processes and to ensure a stable sputtering in the transition mode by using closed loop reactive gas control. Therefore, the controllability analysis is an important issue. The aim of this paper is to study the controllability of reactive sputtering process, especially in the transition region; a simple mathematical model based on Berg's original proposal is used. Analysis results show that the reactive magnetron sputtering process shows unstable behavior in the transition region and it is a controllable process.
Źródło:
Acta Physica Polonica A; 2013, 123, 1; 3-6
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optimality conditions in multiobjective programming problems with interval valued objective functions
Autorzy:
Ahmad, I.
Singh, D.
Dar, B. A.
Powiązania:
https://bibliotekanauki.pl/articles/206566.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Instytut Badań Systemowych PAN
Tematy:
interval valued functions
gH-differentiablity
Pareto optimal solutions
pseudoconvexity
KKT optimality conditions
Opis:
We devote this paper to study of multiobjective programming problems with interval valued objective functions. For this, we consider two order relations LU and LS on the set of all closed intervals and propose several concepts of Pareto optimal solutions and generalized convexity. Based on generalized convexity (viz. LU and LS-pseudoconvexity) and generalized differentiability (viz. gHdifferentiablity) of interval valued functions, the KKT optimality conditions for aforesaid problems are obtained. The theoretical development is illustrated by suitable examples.
Źródło:
Control and Cybernetics; 2015, 44, 1; 19-45
0324-8569
Pojawia się w:
Control and Cybernetics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Distribution and relative density of trees species in Kainji Lake National Park, Nigeria
Autorzy:
Akande, O. A.
Ahmad, Y. A.
Shuaib, A. B.
Jeje, C. A.
Powiązania:
https://bibliotekanauki.pl/articles/1077871.pdf
Data publikacji:
2019
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Distribution
Kainji Lake National Park
relative density
species
trees
Opis:
The importance of trees in the environment cannot be overemphasized. This present study, therefore, deals with the distribution and relative density of trees species in Kainji Lake National Park. Data were collected using plot sampling techniques. Therein, a 50 by 50 m2 plot was randomly laid. Within each sample plot, data on all trees ≥ 10 cm in diameter at breast height were enumerated. The data were analyzed using descriptive statistics. The result shows that different types of plants species were enumerated in the selected plots. This included six families of trees: Fabiaceae, Caesalpiniaceae, Rubiaceae, Maliaceae, Annonaceae and Mimosaceae. The percentage score of tree species in the four plots reveals that Afzelia africana recorded the highest with a total number of 60 species, followed by Detarium macrocarpium with 47 species, while Anogeissus leiocarpus and Azadirachta indica recorded 31 and 17 species, respectively. Gardenia aqualla was the least species recorded. The density and relative density of Afzelia africana recorded the highest, with 1.2ha and 26.9%, followed by Detarium microcarpiuum with 0.94ha and 21.1%, respectively, while Gardenia aqualla was the least with 0.02 ha and 0.4%. In terms of mean height, Daniela oliveri recorded the highest, with 28.1m, followed by Afzelia africana with 21.8%, while Azadirachta indica was the least with 5.8%. The mean DBH of Entada africana and Anogeissus leiocarpus recorded was 28.7cm and 28.1cm, while Prosopis africana and Accacia gournmaensis recorded 14.0 and 13.4, respectively, which were the least. The Types of wild animal species that are associated with the tree species includes Baboon, Kob, Grim duiker, Francolin, Patas monkey etc. Relative abundance of the animal species shows that Papio anubis recorded the highest with 40.5 individuals, while Erythrocebus patas recorded the least with 2.5 individuals.
Źródło:
World News of Natural Sciences; 2019, 22; 52-61
2543-5426
Pojawia się w:
World News of Natural Sciences
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Deposition of a polymeric porous superhydrophobic thin layer on the surface of poly(vinylidenefluoride) hollow fiber membrane
Autorzy:
Ahmad, A. L.
Mohammed, H. N.
Ooi, B. S.
Leo, C. P.
Powiązania:
https://bibliotekanauki.pl/articles/778912.pdf
Data publikacji:
2013
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
Superhydrophobic layer
PVDF
Gas-liquid contactor
CO2
porous
Opis:
Porous superhydrophobic layer of low-density polyethylene (LDPE) was created by a simple approach on the Poly(vinylidenefluoride) (PVDF) hollow fiber membranes. Acetone and ethanol mixtures with different volume ratios were used as the non-solvent on the coating surface. A 5:1 (v/v) acetone/ethanol ratio provided a porous surface with a 152° ± 3.2 water contact angle. The high contact angle could reduce membrane wettability for better carbon dioxide capture when the membrane was used as gas-liquid contactor in absorption processes. To assess the effect of the created superhydrophobic layer, the pristine and modified membranes were tested in a CO2 absorption system for ten days. The results revealed that the absorption flux in the modified membrane was higher than that of pristine membrane.
Źródło:
Polish Journal of Chemical Technology; 2013, 15, 3; 1-6
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Site Preference Analysis and Ordering Characteristics of Ternary Cu0.5(Zn1–xMx)0.5 (M = Transition Metals) Alloys
Autorzy:
Ahmad, N.
Ziya, A. B.
Atiq, S.
Saifullah, K.
Hashim, M.
Saleem, M.
Powiązania:
https://bibliotekanauki.pl/articles/352693.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
ternary alloy systems
order-disorder transformations
site occupancy
ab-initio calculations
ordering energies
Opis:
The site preference of some transition metals during B2-type ordering has been investigated in the ternary Cu0.5 (Zn1-x Mx )0.5 alloys with M = Ti, V, Ag, Au, Cr, Mn, Fe, Co, Ni, Nb, Mo, Hf, Ta, W, Re or Pt (x ≤ 0.01). The statistic-o-thermodynamical theory combined with the electronic theory of alloys has been used to calculate the partial ordering energies, partial short range order parameters and the order-disorder transformation temperatures. The values of partial short range order parameters have been used to determine the site preference of the metal M. The analysis shows that the metals M can be divided into two groups with regard to lattice site occupancy. One group comprising of Cr, Mn, Fe, Co, Ni, Nb, Mo, Hf, Ta, W, Re or Pt was found to prefer Zn sublattice sites, while the second group of Ti, V, Ag or Au atoms prefer Cu sublattice sites. It is found that order-disorder transformation temperature and the site preference of metal M both depend strongly on the partial ordering energies and ternary alloying addition of metal M.
Źródło:
Archives of Metallurgy and Materials; 2018, 63, 3; 1531-1535
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Impact of membrane pore structure on protein detection sensitivity of affinity-based immunoassay
Autorzy:
Ahmad, A. L.
Ideris, N.
Ooi, B.S.
Low, S.C.
Ismail, A.
Powiązania:
https://bibliotekanauki.pl/articles/777927.pdf
Data publikacji:
2016
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
morphology
PVDF membrane
protein immobilization
Opis:
Understanding a membrane’s morphology is important for controlling its final performance during protein immobilization. Porous, symmetric membranes were prepared from a polyvinylidene fluoride/N-methyl-2-pyrrolidinone solution by phase inversion process, to obtain membrane with various microsized pores. The concentration and surface area of aprotein dotted on the membrane surface were measured by staining with Ponceau S dye. The dotted protein was further scanned and analysed to perform quantitative measurements for relative comparison. The intensity of the red protein spot and its surface area varied depending on the membrane pore size, demonstrating the dependence of protein immobilization on this factor. The membrane with the smallest pore size (M3) showed the highest protein spot intensity and surface area when examined at different protein concentrations. An increase in the applied protein volume showed a linearity proportional trend to the total surface area, and an uneven round dot shape was observed at a large applied volume of protein solution.
Źródło:
Polish Journal of Chemical Technology; 2016, 18, 2; 97-103
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Statistical Estimation and Mathematical Modelling of Tropospheric Radio Refractivity Based on Meteorological Data
Autorzy:
Alimgeer, K. S.
Awais, M.
Ijaz, B.
Khan, S. A.
Subhan, F.
Ahmad, N.
Powiązania:
https://bibliotekanauki.pl/articles/221069.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
radio refractivity
statistical estimation
ITU
mathematical modelling
Opis:
To obtain optimal performance, estimation of radio refractivity is essential in planning and design of radio links/systems. The dependence of radio refractivity on different climatic parameters such as temperature, pressure, humidity and scale height is studied. The method proposed by International Telecommunication Union (ITU) is used in calculation of tropospheric radio refractivity. The main objective of this work is to formulate a mathematical equation/expression which can be used to predict/estimate the value of radio refractivity for an arbitrary day of any year, with a low error of estimation, in a local environment. Sensitivity of radio refractivity to temperature, pressure and humidity has been evaluated for a period of 5 years from 2008 to 2012, in a particular area under consideration. The results presented for tropospheric radio refractivity take into consideration both the location height and scale height parameters. The results are analysed in terms of statistical measures such as the moving averages, probability density function, monthly mean values, and their corresponding standard deviations. Finally, a mathematical model is formulated to calculate the radio refractivity for any day of a whole year. Reliability of error analysis in respect to accuracy is also shown. It was implemented in the industrial enterprise.
Źródło:
Metrology and Measurement Systems; 2018, 25, 1; 115-128
0860-8229
Pojawia się w:
Metrology and Measurement Systems
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
X-ray diffraction and vibrational spectroscopic studies of the intermolecular interactions on the grinding and compaction behaviours of lopinavir and ritonavir crystals
Autorzy:
Ainurofiq, Ahmad
Setianto, Arif B.
Nugraha, Yuda P.
Suendo, Veinardi
Uekusa, Hidehiro
Soewandhi, Sundani N.
Powiązania:
https://bibliotekanauki.pl/articles/895537.pdf
Data publikacji:
2020-04-29
Wydawca:
Polskie Towarzystwo Farmaceutyczne
Tematy:
compression
grinding
Vibrational spectroscopy
Ritonavir
intermolecular interactions lopinavir
crystal behaviour
Opis:
Lopinavir (LPV) and ritonavir (RTV) are anti-viral drugs used in combination and commonly prepared through hot-melt extrusion techniques. Mechanical processes are greatly involved, including blending and milling. Therefore, the crystal behaviour of LPV and RTV under the mechanical process is an interesting study. Here, the LPV, RTV, and their mixtures were processed by two different treatments: grinding and compression processes. The solid-state properties of the drugs were evaluated by powder x-ray diffraction (PXRD), differential scanning calorimetry (DSC), Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy, and scanning electron microscopy (SEM). Single-crystal XRD analysis was also carried out to confirm the packing structure in the crystal lattice. It was observed that LPV was very sensitive to the grinding process, where it tends to form an amorphous solid in both the pure and mixture forms. On the other hand, RTV has a very stable crystalline structure and was able to retain its crystallinity even under grinding. Both LPV and RTV were observed to be quite stable under compression, where both retained their crystalline form with only slight changes in their d-spacing values. This study highlighted the molecular origin of LPV and RTV crystal behaviour after grinding and compression processes.
Źródło:
Acta Poloniae Pharmaceutica - Drug Research; 2020, 77, 2; 259-269
0001-6837
2353-5288
Pojawia się w:
Acta Poloniae Pharmaceutica - Drug Research
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effectiveness of fMRI Data when Combined with Polygraph Data
Эффективность сочетания данных фМРТ с данными полиграфа
Autorzy:
Gordon, Nathan J.
Mohamed, Feroze B.
Platek, Steven M.
Ahmad, Harris
Williams, J. Michael
Faro, Scott H.
Powiązania:
https://bibliotekanauki.pl/articles/523470.pdf
Data publikacji:
2018
Wydawca:
Krakowska Akademia im. Andrzeja Frycza Modrzewskiego
Tematy:
Integrated Zone Comparison Technique
Polygraph
ASIT PolySuite Scoring Algorithm
Horizontal Scoring System
fMRI
Pneumo
Electro-dermal Response
Cardio
Opis:
The Integrated Zone Comparison Technique (IZCT) was utilized with computerized polygraph instrumentation and the Academy for Scientific Investigative Training’s Horizontal Scoring System ASIT PolySuite algorithm, as part of a blind study in the detection of deception. This paper represents a synergy analysis of combining fMRI only deception data with each of the three individual physiological parameters that are used in polygraph. They include the electro-dermal response (EDR), pneumo, and cardio measurements. In addition, we compared the detection accuracy analysis using each single parameter by itself. The fMRI score and each individual polygraph parameter score on individual subjects were averaged to establish an overall score.
Źródło:
European Polygraph; 2018, 12, 1(43); 19-25
1898-5238
2380-0550
Pojawia się w:
European Polygraph
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Introducing key advantages of intensified flotation cells over conventionally used mechanical and column cells
Autorzy:
Hassanzadeh, Ahmad
Safari, Mehdi
Khoshdast, Hamid
Güner, Mustafa K.
Hoang, Duong H.
Sambrook, Tim
Kowalczuk, Przemyslaw B.
Powiązania:
https://bibliotekanauki.pl/articles/2146874.pdf
Data publikacji:
2022
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
pneumatic flotation cells
energy input
mean particle retention time
fine particles
bubble size distribution
Opis:
The present paper introduces the key advantages of ImhoflotTM, JamesonTM, and RefluxTM flotation cells over the conventionally used mechanical and column cells from different perspectives. The impact of slurry mean retention time, bubble size distribution, and energy input was studied for all cell types. The mean retention time of laboratory scale ImhoflotTM (V030-cell) and RefluxTM flotation cells (RFC100) were measured experimentally using KCl as a tracer. Also, initially a statistical and practical overview of previously installed ImhoflotTM, and JamesonTM cells was presented in this work. It was found that more industrial data is available for the JamesonTM cell. The diagnostic results showed that RefluxTM, JamesonTM, and ImhoflotTM functionally operate similarly based on providing intensive turbulence in the downcomer. They were initially applied to the Australian and the UK coal industries and installed in the cleaning stage of flotation circuits, while there are now more applications in a wide variety of minerals across the world in different flotation stages. First pilot trials on a Russian gold ore were reported operating both JamesonTM and ImhoflotTM cells at the rougher-scalper and cleaner stages providing superior results using the ImhoflotTM cell as rougher-scalper and the JamesonTM at the cleaner. Formation of sub-micron and micron-sized bubbles, effective hydrodynamic characteristics, and low capital and operating costs were reported as major advantages of intensified flotation cells over the conventionally used ones in improving the recoverability of ultra-fine particles. Literature data showed that these cells provide greater gas-hold-up values (40-60%) over the mechanical (5-20%) and column cells (5-25%) with substantially lower power inputs. It was indicated that low mean slurry retention time could lead to a potential enhancement in their throughputs, but further industrial measurements are required to prove this statement. The RefluxTM cell showed a plug-flow mixing regime, while ImhoflotTM V-Cell followed the trend of perfect mixing and plug-flow dispersion regimes.
Źródło:
Physicochemical Problems of Mineral Processing; 2022, 58, 5; art. no. 155101
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
An alternative and indirect statistical modeling method for viscosity estimation and its experimental validation for low styrene content polyester resin
Autorzy:
Nawaz, A.
Islam, B.
Ijaz, M. Z.
Saleem, U.
Khattak, M. S.
Ahmad, S. N.
Maqsood, N.
Ali, L.
Powiązania:
https://bibliotekanauki.pl/articles/778495.pdf
Data publikacji:
2018
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
indirect method
polyester resin
statistical relation
Ford viscosity cup
Opis:
We propose an indirect method of ASTM D-1200 for measurement of viscosity from 0.1 to 30 stokes (St) using Ford cup 5 (range 2~ 12 St) by developing a statistical relation. General purpose low styrene content polyester resin (without adding initiator, hardener and accelerator) was used for viscosity measurement. In existing ASTM D 1200 standard, ford cups (1-4) are used to measure the viscosity up to 2 St, while fifth cup is used for measurement from 2 to 12 St. Viscosity above 12 St is not estimated using existing ASTM D- 1200 method. In contrast, our method and statistical relation proposed in this paper estimates viscosity in the flexible range of 0.1 to 30 St by using Ford cup 5 only. The estimated values were confirmed by existing ASTM D-1200 (0.1 to 12 St) and by using Ubbelohde viscometer (12 to 30 St). Values estimated above 12 St are from the proposed model are also in good conformance (percentage error ~ 5% or less) with experimental results. The satisfaction level of the estimated values with the experiments suggests that the model has also the potential for application to paints, polymer and oil industry.
Źródło:
Polish Journal of Chemical Technology; 2018, 20, 4; 60-65
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
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