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    Wyświetlanie 1-4 z 4
    Tytuł:
    Production of High-Purity Tantalum Metal Powder for Capacitors Using Self-Propagating High-Temperature Synthesis
    Autorzy:
    Lee, Yong-Kwan
    Sim, Jae-Jin
    Byeon, Jong-Soo
    Lee, Yong-Tak
    Cho, Yeong-Woo
    Kim, Hyun-Chul
    Heo, Sung-Gue
    Lee, Kee-Ahn
    Seo, Seok-Jun
    Park, Kyoung-Tae
    Powiązania:
    https://bibliotekanauki.pl/articles/2049150.pdf
    Data publikacji:
    2021
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    tantalum
    self-propagating high-temperature synthesis
    tantalum oxide
    magnesium
    capacitor
    Opis:
    In this study, high-purity tantalum metal powder was manufactured via self-propagating high-temperature synthesis. During the process, Ta2O5 and Mg were used as the raw material powder and the reducing agent, respectively, and given that combustion rate and reaction temperature are important factors that influence the success of this process, these factors were controlled by adding an excessive mass of the reducing agent (Mg) i.e., above the chemical equivalent, rather than by using a separate diluent. It was confirmed that Ta metal powder manufactured after the process was ultimately manufactured 99.98% high purity Ta metal powder with 0.5 μm particle size. Thus, it was observed that adding the reducing reagent in excess favored the manufacture of high-purity Ta powder that can be applied in capacitors.
    Źródło:
    Archives of Metallurgy and Materials; 2021, 66, 4; 935-939
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Development of wear-resistant coatings for automotive parts after processing in SHS conditions
    Autorzy:
    Sereda, Borys
    Kruglyak, Irina
    Sereda, Dmytro
    Gaydaenko, Alex
    Kruglyak, Dmytro
    Powiązania:
    https://bibliotekanauki.pl/articles/2141006.pdf
    Data publikacji:
    2019
    Wydawca:
    Fundacja Centrum Badań Socjologicznych
    Tematy:
    automotive parts
    transport
    protective coatings
    wear resistance
    self propagating high-temperature synthesis
    steel
    Opis:
    Methods of obtaining chromium-coated coatings are considered and technology for the formation of boron, silicon and titanium protected layers on steels under conditions of self-propagating high-temperature synthesis is presented. Using the methods of mathematical modeling, when obtaining wear-resistant coatings on machine parts in conditions of self-propagating high-temperature synthesis, optimal compositions of SHS mixtures have been developed. When tested in sliding friction conditions, the best abrasion resistance, among the coatings under consideration, are chromoaluminium-coated coatings. Their wear resistance is 4.8-5 times higher than in uncoated samples, chromoaluminosilicated and chromoalumotated in 2.1-3.5. The gas-transport method of coating with the help of SHS makes it possible to obtain steel 50 and U8A with increased physical and mechanical properties, without requiring high energy costs and time.
    Źródło:
    Journal of Sustainable Development of Transport and Logistics; 2019, 4, 1; 25-30
    2520-2979
    Pojawia się w:
    Journal of Sustainable Development of Transport and Logistics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of Fe-TiB2 Nanocomposites by Spark-Plasma Sintering of a (FeB, TiH2) Powder Mixture
    Autorzy:
    Huynh, X.-K.
    Kim, B.-W.
    Kim, J.-S.
    Powiązania:
    https://bibliotekanauki.pl/articles/351368.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    Fe-TiB2 nanocomposite
    mechanical activation
    spark plasma sintering
    self-propagating high-temperature synthesis reaction
    Opis:
    Fe-40wt% TiB2 nanocomposites were fabricated by mechanical activation and spark-plasma sintering of a powder mixture of iron boride (FeB) and titanium hydride (TiH2). The powder mixture of (FeB, TiH2) was prepared by high-energy ball milling in a planetary ball mill at 700 rpm for 3 h followed by spark-plasma sintering (SPS) at various conditions. Analysis of the change in relative sintered density and densification rate during sintering showed that a self-propagating high-temperature synthesis reaction occurs to form TiB2 from FeB and Ti. A sintered body with relative density higher than 98% was obtained after sintering at 1150°C for 5 and 15 min. The microstructural observation of sintered compacts with the use of FE-SEM and TEM revealed that ultrafine particulates with approximately 5 nm were evenly distributed in an Fe-matrix. A hardness value of 83 HRC was obtained, which is equivalent to that of conventional WC-20 Co systems.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 2; 1043-1047
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermoelectric properties of bismuth-doped magnesium silicide obtained by the self-propagating high-temperature synthesis
    Autorzy:
    Bucholc, Bartosz
    Kaszyca, Kamil
    Śpiewak, Piotr
    Mars, Krzysztof
    Kruszewski, Mirosław J.
    Ciupiński, Łukasz
    Kowiorski, Krystian
    Zybała, Rafał
    Powiązania:
    https://bibliotekanauki.pl/articles/2173670.pdf
    Data publikacji:
    2022
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    thermoelectric materials
    magnesium silicide
    bismuth doping
    SHS
    self-propagating high-temperature synthesis
    spark plasma sintering
    materiały termoelektryczne
    krzemek magnezu
    doping bizmutem
    samorozwijająca się wysokotemperaturowa synteza
    iskrowe spiekanie plazmowe
    Opis:
    Doping is one of the possible ways to significantly increase the thermoelectric properties of many different materials. It has been confirmed that by introducing bismuth atoms into Mg sites in the Mg2Si compound, it is possible to increase career concentration and intensify the effect of phonon scattering, which results in remarkable enhancement in the figure of merit (ZT) value. Magnesium silicide has gained scientists’ attention due to its nontoxicity, low density, and inexpensiveness. This paper reports on our latest attempt to employ ultrafast self-propagating high-temperature synthesis (SHS) followed by the spark plasma sintering (SPS) as a synthesis process of doped Mg2Si. Materials with varied bismuth doping were fabricated and then thoroughly analyzed with the laser flash method (LFA), X-ray diffraction (XRD), scanning electron microscopy (SEM) with an integrated energy-dispersive spectrometer (EDS). For density measurement, the Archimedes method was used. The electrical conductivity was measured using a standard four-probe method. The Seebeck coefficient was calculated from measured Seebeck voltage in the sample subjected to a temperature gradient. The structural analyses showed the Mg2Si phase as dominant and Bi2Mg3 located at grain boundaries. Bismuth doping enhanced ZT for every dopant concentration. ZT = 0.44 and ZT=0.38 were obtained for 3wt% and 2wt% at 770 K, respectively.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2022, 70, 3; art. no. e141007
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-4 z 4

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