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Tytuł:
Influence of granular bed parameters on emulsion flow and elution process of oil-in-water emulsion
Autorzy:
Błaszczyk, M.
Pacholski, P.
Przybysz, Ł.
Sęk, J.
Powiązania:
https://bibliotekanauki.pl/articles/298006.pdf
Data publikacji:
2016
Wydawca:
Uniwersytet Warmińsko-Mazurski w Olsztynie
Tematy:
porous media
oil-in-water emulsion
elution
Opis:
Emulsion flow through porous structure is used in many processes in the field of chemical engineering. Good examples of practical applications are Enhanced Oil Recovery (EOR) techniques, soil remediation and treatment of oily wastewater. The emulsion transport in through porous media is not easy to describe, due to rheological behavior of emulsions and porous structure properties. In case of emulsified system flow through porous bed it is possible to observe the retention of oil on porous structure, and reduction of permeability of bed. In the presented study, we tried to investigate the influence of porous bed parameters on oil-in-water emulsion behavior during its flow and elution from porous structure. In experiments we used porous beds with varied particle size range and with different lengths. We measured pressure drop and related permeability changes in time. The turbidimetric and microscopic analysis that we conducted allowed us to check how concentration of emulsion changed during its flow and elution from porous structure.
Źródło:
Technical Sciences / University of Warmia and Mazury in Olsztyn; 2016, 19(4); 325-337
1505-4675
2083-4527
Pojawia się w:
Technical Sciences / University of Warmia and Mazury in Olsztyn
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The investigation of crude oil derivatives elution from porous structure
Autorzy:
Pacholski, Piotr
Sęk, Jerzy
Błaszczyk, Mariola
Przybysz, Łukasz
Powiązania:
https://bibliotekanauki.pl/articles/1179645.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
emulsion elution
oil-in-water transport
porous media
Opis:
Crude oil and its derivatives migration in porous structure are important aspects of chemical engineering, since they are vital for processes such as oil extraction and soil remediation. Understanding the multiphase flow in porous rocks is necessary for Enhanced Oil Recovery (EOR) and can lead to this process intensification. In methods of oil extraction such as water flooding or polymer flooding liquids are pumped with high pressure to increase the sweeping efficiency of medium. Thus, the knowledge in this field is important for all people engaged in this process. Oil and its derivatives transport in porous structure occurs also during ground leaching techniques used in soil remediation after emergency release of these liquids. Therefore the research in field of transport in porous media are necessary to conduct this process efficiently. The aim of the experiment was to check the sweeping ratio of paraffin from porous structure for different volumetric flow of leaching liquid. We also measured pressure at the inlet to bed, which allowed us to follow the stages during elution process. To analyze concentration in obtained samples we used TurbiscanLab® device.
Źródło:
World Scientific News; 2017, 72; 86-93
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Experimental investigation into influence of oil-in-water emulsions flow on permeability of porous bed
Autorzy:
Błaszczyk, Mariola
Sęk, Jerzy
Przybysz, Łukasz
Pacholski, Piotr
Powiązania:
https://bibliotekanauki.pl/articles/1178549.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
emulsions
multiphase flow
oil-in-water
porous bed permeability
Opis:
Emulsions are interesting dispersed systems that are necessary for a number of technological processes. Their flow through porous structures have many applications in the field of chemical engineering. Enhanced Oil Recovery (EOR) techniques, soil remediation and various treatment methods of oily wastewater are good examples of emulsion flow in porous structure. The phenomenon of dispersed system flow through porous media is not easy to describe, mainly because of rheological behavior of emulsions and porous structure properties. During two phase flow of oil and water through porous bed it is possible to observe the interception of oil to porous structure, as well as filtration of oil in pores. In this study, we tried to examine the influence of the fraction size as well as migration process history on permeability of porous bed.
Źródło:
World Scientific News; 2017, 70, 2; 241-251
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spectrum of light absorption as the indicator of lubricate oil dispsersed in the natural water
Autorzy:
Baszanowska, E.
Otremba, Z.
Powiązania:
https://bibliotekanauki.pl/articles/247346.pdf
Data publikacji:
2016
Wydawca:
Instytut Techniczny Wojsk Lotniczych
Tematy:
lubricate oil
absorption
absorption spectra of dispersed oil oil-in-water emulsion
Opis:
Oil pollutants in the natural water masses – especially in the seawater column – can be found in two forms, namely as dissolved oil or as dispersed one. With a broad set of methods, for studying the complex structure of petroleum products, due to the ability of petroleum products to absorb UV-light, absorbance spectra could be a relevant indicator to oil identification in aquatic environment and could support methods provided by the fluorescence technique. The intention of the study described in this article is to characterise the absorption properties of lubricate oil possible to found in the marine environment. Two types of oil as the representative of lubricate oils using in the ship engines are considered. One form of oil possible to found in the marine environment – oil-in-water emulsion was taken into account for analysis. Dispersed in water lubricate oil samples were prepared for several oil concentration for each type of oil. Spectrofluorometer Aqualog Horiba was used to register the absorbance spectra of oils. Based on the Lambert-Beer law the absorbance spectra were derived and specific parameter – absorption coefficient – for each wavelength of excitation, in the range 240-600 nm, was determined. Obtained results indicate decreasing of the oil absorbance value when excitation wavelength increases. Moreover, basing on the absorbance spectra it could be concluded that the main maximum for this kind of oils is located below 240 nm. However, in the considered range of excitation wavelength small flat peak, centred about 265 nm for both types of oils, was detected. Therefore one could conclude that absorbance of oils could be used as the indicator to detect of oil pollution in the natural environment omitting the labour intensive chemical methodology.
Źródło:
Journal of KONES; 2016, 23, 1; 61-66
1231-4005
2354-0133
Pojawia się w:
Journal of KONES
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Light absorption properties of ‘Petrobaltic’ oil-in-water emulsion present in seawater
Autorzy:
Baszanowska, E.
Otremba, Z.
Powiązania:
https://bibliotekanauki.pl/articles/246640.pdf
Data publikacji:
2018
Wydawca:
Instytut Techniczny Wojsk Lotniczych
Tematy:
crude oil, absorbance
absorption spectra of dispersed oil
absorption coefficient
oil-in-water emulsion
Opis:
In the article, the characteristic of crude oil ‘Petrobaltic’ potentially present in the Baltic Sea water masses is considered in relation to the protection of marine environment. The main spectroscopic method to characterize various oils (crudes and refinery products like fuels and lubricating oils) is fluorescence. However, the absorbance measurements of oils are necessary due to the partial overlapping the spectra of natural seawater components and oil substances. Therefore, properties of crude oil are considered to expand the basis of spectroscopic properties of oils – typical marine organic pollutants – based on absorption measurements. Oils potentially found in the marine environment are, in addition to surface forms, also in-depth ones as oil-in-water emulsion. Therefore, in the article crude oil as oil-in-water emulsion form is considered. As a solvent demineralised water with salinity, corresponding to Baltic Sea salinity was used. Several concentrations of dispersed crude oil were prepared. The absorbance spectra in the UV and visual range of the light in the range from 240 to 600 nm, for each prepared samples are discussed. Based on the Lambert-Beer law for each wavelength of excitation, in the range 240-600 nm, the specific parameter absorption coefficient was determined. Obtained results indicate the rapid decreasing of the absorbance for this kind of oil in the wavelength range from 240 nm to 420 nm. However, in the shape of absorbance spectra is observed the characteristic wide and flat peak located at 260 nm for excitation wavelength, which could be a specific point for this kind of oil.
Źródło:
Journal of KONES; 2018, 25, 3; 59-64
1231-4005
2354-0133
Pojawia się w:
Journal of KONES
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Modelling of seawater polluted by light and heavy crude oil droplets
Autorzy:
Rudź, K.
Darecki, M.
Toczek, H.
Powiązania:
https://bibliotekanauki.pl/articles/246668.pdf
Data publikacji:
2012
Wydawca:
Instytut Techniczny Wojsk Lotniczych
Tematy:
oil pollution
remote sensing reflectance
Monte Carlo simulation
radiative transfer
oil-in-water emulsion
Opis:
Significant amounts of crude oil transported from offshore fields to the refineries using tankers or pipelines, demand increased control of seawater pollution. Tanker accidents resulting in oil spills drive much attention, as they influence local marine life and coastal industry. However, the most significant annual amount of crude oil enters the sea in the form of oilin- water emulsion as a result of standard tanker operations, offshore oil extraction and daily work of refineries. Many branches of science are challenged to provide new methods for oil detection, less expensive, more sensitive and more accurate. Remote satellite or airborne detection of large oil spills is possible using joint techniques as microwave radars, ultraviolet laser fluorosensors and infrared radars. Some methods are capable to deal with oil streaks detection and estimation of oil thickness. Although there is currently, no method to detect small concentration of oil droplets dispersed in seawater. Oil droplets become additional absorbents and attenuators in water body. They significantly change seawater inherent optical properties, which imply the change of apparent optical properties, detectable using remote sensing techniques. To enable remote optical detection of oil-in-water emulsion, a study of optical properties of two types of crude oil was conducted. Radiative transfer theory was applied to quantify the contribution of oil emulsion to remote sensing reflectance (Rrs). Spectra of Rrs from in situ measurements in Baltic Sea were compared to Rrs spectra of seawater polluted by 1 ppm of crude oil emulsion, collected using radiative transfer simulation. The light crude oil caused a 9-10% increase of Rrs while the heavy one reduced Rrs up to 30% (model accuracy stayed within 5% for considered spectral range). Results are discussed concerning their application to shipboard and offshore oil content detection.
Źródło:
Journal of KONES; 2012, 19, 2; 473-480
1231-4005
2354-0133
Pojawia się w:
Journal of KONES
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Emulsified fuels of machine origin in seawater - a contribute to remote detection
Autorzy:
Rudz, K.
Powiązania:
https://bibliotekanauki.pl/articles/246040.pdf
Data publikacji:
2011
Wydawca:
Instytut Techniczny Wojsk Lotniczych
Tematy:
oil pollution
remote sensing reflectance
Monte Carlo simulation
radiative transfer
oil-in-water emulsion
Opis:
Development of industry and trade in the last few decades caused a huge increase in the pollution of the world's oceans. Substantial contributors to marine pollution come with the rivers from land-based sources including the by products of industry, run-off from agriculture activities such as biocides as well as effluents from urban areas. Moreover, a significant amount of marine pollution is caused by shipping and maritime activities. The operation of ship plants gives a real possibility for engine oils and fuels to reach the marine environment. Discharge waters contain a certain amount of petroleum derivatives in the form of dispersed droplets (oil-in-water emulsion). The presence of oil emulsion cause measurable changes in the optical properties of seawater. It is conceptually possible to detect these changes using a standard radiance or irradiance reflectance meter. Hence, a set of radiative transfer simulation has been carried out. This paper presents a computed photon trace simulation based on the Monte Carlo code, applied to the marine environment. The results are presented as reflectance spectra for the models of Baltic Sea and ocean water both pure and polluted by oil emulsion. It is shown that even small amounts of petroleum pollution raise the values of irradiance reflectance and cause a spectral shift by certain conditions. A possibility for remote evaluation of oil pollution is discussed as well as the perspective for improving the interpretation of shipboard and offshore light field analyses.
Źródło:
Journal of KONES; 2011, 18, 3; 375-381
1231-4005
2354-0133
Pojawia się w:
Journal of KONES
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Emulsified fuels of machine origin in seawater - a contribute to remote detection
Autorzy:
Rudz, K.
Powiązania:
https://bibliotekanauki.pl/articles/242232.pdf
Data publikacji:
2011
Wydawca:
Instytut Techniczny Wojsk Lotniczych
Tematy:
oil pollution
remote sensing reflectance
Monte Carlo simulation
radiative transfer
oil-in-water emulsion
Opis:
Development of industry and trade in the last few decades caused a huge increase in the pollution of the world's oceans. Substantial contributors to marine pollution come with the rivers from land-based sources including the by-products of industry, run-off from agriculture activities such as biocides as well as effluents from urban areas. Moreover, a significant amount of marine pollution is caused by shipping and maritime activities. The operation of ship plants gives a real possibility for engine oils and fuels to reach the marine environment. Discharge waters contain a certain amount of petroleum derivatives in the form of dispersed droplets (oil-in-water emulsion). The presence of oil emulsion cause measurable changes in the optical properties of seawater. It is conceptually possible to detect these changes using a standard radiance or irradiance reflectance meter. Hence, a set of radiative transfer simulation has been carried out. This paper presents a computed photon trace simulation based on the Monte Carlo code, applied to the marine environment. The results are presented as reflectance spectra for the models of Baltic Sea and ocean water both pure and polluted by oil emulsion. It is shown that even small amounts of petroleum pollution rise the values of irradiance reflectance and cause a spectral shift by certain conditions. A possibility for remote evaluation of oil pollution is discussed as well as the perspective for improving the interpretation of shipboard and offshore light field analyses.
Źródło:
Journal of KONES; 2011, 18, 2; 385-390
1231-4005
2354-0133
Pojawia się w:
Journal of KONES
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Physical stability of model emulsions based on ethyl cellulose oleogels
Autorzy:
Szymańska, I.
Żbikowska, A.
Kowalska, M.
Powiązania:
https://bibliotekanauki.pl/articles/2082906.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Instytut Agrofizyki PAN
Tematy:
oleogels
ethyl cellulose
oil-in-water emulsions
MS-DWS method
storage test
CSA method
Opis:
The purpose of this study was the evaluation of the physical stability of low-fat oil-in-water model emulsions containing oleogels based on ethyl cellulose), compared to emulsions with anhydrous milk fat. The oleogels were prepared using rapeseed oil with ethyl cellulose at the level of 4.5, 5.0, 5.5 or 6.0% w/w. The O/W emulsions (30/70 w/w) were stabilized by guar gum (0.6% w/w) and soy lecithin (5.0% w/w). The physical properties of oleogels and anhydrous milk fat (centrifugal stability, spreadability/penetration test), rheology and the physical stability of the emulsions (MS-DWS method, centrifugal/thermal stability) were determined, a storage test of the emulsions (CSA method, LUMiSizer) was also conducted. It was demonstrated that ethyl cellulose is an effective edible oil structuring agent. The increase in ethyl cellulose content enhanced the centrifugal stability and hardness of the oleogels. As a result of a microrheology analysis, it was found that the emulsion with anhydrous milk fat had the most elastic strength, macroscopic viscosity and the highest solids content. All emulsions demonstrated high centrifugal/ thermal stability. A higher temperature and extended storage time caused a reduction in the stability of all emulsions and increased the velocity of particle migrations. The ethyl cellulose-oleogels are potential fat phases for stable O/W emulsions, which could be used as a vegan alternative to traditional products based on animal components.
Źródło:
International Agrophysics; 2020, 34, 3; 289-300
0236-8722
Pojawia się w:
International Agrophysics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wybrane zagadnienia modelowania procesu elektrokoagulacji w zastosowaniu do rozdziału emulsji olejowo-wodnych
Selected modeling aspects of electrocoagulation process applied in oil-in-water emulsion breaking
Autorzy:
Janczewski, Ł.
Dyląg, M.
Powiązania:
https://bibliotekanauki.pl/articles/2073405.pdf
Data publikacji:
2014
Wydawca:
Stowarzyszenie Inżynierów i Techników Mechaników Polskich
Tematy:
elektrokoagulacja
flotacja
koagulacja
modelowanie
emulsje O/W
electrocoagulation
flotation
coagulation
modeling
oil-in-water emulsions
Opis:
Przedstawiono istotę metody elektrokoagulacji w zastosowaniu do rozdziału emulsji O/W. Wykorzystano możliwości diagramu Venna, wskazując na złożoność możliwych interakcji mechanizmów procesów składowych. Skoncentrowano się na analizie i ocenie stanu wiedzy w zakresie modelowania elektrokoagulacji - stwierdzając brak liczbowego zachowania proporcji pomiędzy modelami deterministycznymi oraz stochastycznymi. W konkluzji wskazano na konieczność dalszych badań wykorzystujących podstawy systematyki modelowania matematycznego, ze szczególnym uwzględnieniem potencjału środowiska MOSAIC.
Bases of electrocoagulation method applied in oil-in-water emulsion breaking are presented in the paper. The Venn diagram was used in the presentation of constituent processes interactions. The state-of-the-art in the field of electrocoagulation modeling was analyzed and evaluated. A lack of proportion between deterministic and stochastic modeling was ascertained. A necessity of further investigations with the application of systematic mathematical modelling was indicated, especially with the use of MOSAIC environment.
Źródło:
Inżynieria i Aparatura Chemiczna; 2014, 2; 76--80
0368-0827
Pojawia się w:
Inżynieria i Aparatura Chemiczna
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Optimizing manufacturing conditions of polymer microspheres as cell carriers for modular tissue engineering
Autorzy:
Mielan, Bartosz
Pamuła, Elżbieta
Powiązania:
https://bibliotekanauki.pl/articles/1844978.pdf
Data publikacji:
2020
Wydawca:
Akademia Górniczo-Hutnicza im. Stanisława Staszica w Krakowie. Polskie Towarzystwo Biominerałów
Tematy:
modular tissue engineering
microspheres
cell culture
oil-in-water emulsification
poly(L-lactide-co-glycolide) (PLGA)
Opis:
Microspheres (MS) made of biostable polymer, namely polystyrene, have been used as substrates for cell culture enabling rapid cell expansion in dynamic conditions. However, due to non-resorbability, polystyrene (PS) MS when repopulated with cells cannot be directly used in tissue engineering. Our concept was to produce MS from resorbable polymer – poly(L-lactide- -co-glycolide) (PLGA) as a support for adherent cells, e.g. osteoblasts. We hypothesize that such MS can be applied to the injured site to act as cell carriers or as modules for modular tissue engineering (MTE). In this article, we present the results of optimizing the PLGA MS manufacturing conditions via oil-in-water emulsification. Due to such a technique, MS with the required size, size distribution and properties suitable for cell culturing can be obtained. Three parameters of the oil-in-water emulsification were examined: the stirring speed of a water phase during MS manufacturing, the surfactant concentration, i.e. poly(vinyl alcohol) (PVA) in a water phase and concentration of PLGA in dichloromethane (DCM) as an oil phase. The results proved that the 7.5% PLGA concentration in DCM solution as an oil phase, the 0.5-2% concentration of PVA solution as a water phase and the stirring speed of water phase of 1000 rpm provided MS with the 160 μm mean diameter, which is suitable for cell culture. Moreover, the developed sieving and cleaning procedures were efficient to collect MS with the mean diameter of 280 μm, the more coherent size distribution and the ability to sink in the cell culture medium. The presence on the bottom of cell culture wells is crucial for MTE.
Źródło:
Engineering of Biomaterials; 2020, 23, 156; 2-9
1429-7248
Pojawia się w:
Engineering of Biomaterials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Hydrocyklony do rozdziału układu ciecz - ciecz
Hydrocyclones for liquid - liquid separation
Autorzy:
Gutteter-Grudziński, J.M.
Powiązania:
https://bibliotekanauki.pl/articles/2070688.pdf
Data publikacji:
2009
Wydawca:
Stowarzyszenie Inżynierów i Techników Mechaników Polskich
Tematy:
hydrocyklon
separacja emulsji o/w
wielkość kropel
hydrocyclone
separation of oil-in-water emulsions
droplet size
Opis:
Hydrocyklony powszechnie stosowane są do zagęszczania cząstek stałych np. mułów. W ostatnim czasie podjęto próby rozdziału emulsji O/W np. na platformach wiertniczych. W artykule przedstawiono oryginalne wyniki badań autora nad rozdziałem emulsji olejowo-wodnej. Przedstawiono teorię sedymentacji kropel oleju w hydrocyklonie oraz wyniki obliczeń i pomiarów średnicy kropel oleju miernikiem firmy Malvern.
Hydrocyclones are commonly used for compacting solid particles, e.g. sediments. Recent attempts to separate homogenous phases from oil/water emulsions have an environmental background, as relevant oil-water separation installations seem to have various applications, e.g. in oil platforms during uncontrolled spills. This article presents original results of author's own research on the separation of oil and water from emulsions. The concept of oil droplets" sedimentation in a hydrocyclone is discussed and the results of calculations and measurements of oil droplet diameter using the Malvern particle analyzer are shown.
Źródło:
Inżynieria i Aparatura Chemiczna; 2009, 5; 34-35
0368-0827
Pojawia się w:
Inżynieria i Aparatura Chemiczna
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Badanie skuteczności odolejania na nowych koalescencyjnych przegrodach filtracyjnych
The Results of Research on the Efficiency of Oil Separation in New Coalescence Filter Barriers
Autorzy:
Grudziński, J. M.
Powiązania:
https://bibliotekanauki.pl/articles/360227.pdf
Data publikacji:
2004
Wydawca:
Akademia Morska w Szczecinie. Wydawnictwo AMSz
Tematy:
przegroda filtracyjna koalescencyjna
emulsja olejowo-wodna
odolejanie wód zęzowych
EXPLO-SHIP 2004
oil-in-water emulsion
coalescence filter barrier
bilge water oil separation
Opis:
Analizowano zjawiska zachodzące w trakcie procesu filtracji emulsji olejowo-wodnej w filtrze koalescencyjnym włókninowym. Dla zadanego przepływu mieszaniny oleju w wodzie przez przegrodę włóknistą, określono skuteczność filtracji ?F i rozkład wielkości cząstek oleju do wykorzystując miernik Malvern. Uzyskane wyniki przedstawione na rysunkach i w tabelach należy uznać za zadowalające i spełniające normy IMO.
The article presents the results of an analysis of the phenomena that take place during the process of filtration of the oil-in-water emulsion (oil droplet diameter <5mm) in the coalescence unwoven fabric filter. The flow of the oil-water mixture through the unwoven fabric filter barrier has been analyzed. Moreover, the effectiveness of the filtration and the size of oil droplets have been examined. The research results have been presented graphically. The distribution of oil particle sizes and filtration effectiveness have been determined with the use of a Malvern instrument.
Źródło:
Zeszyty Naukowe Akademii Morskiej w Szczecinie; 2004, 1 (73); 221-232
1733-8670
2392-0378
Pojawia się w:
Zeszyty Naukowe Akademii Morskiej w Szczecinie
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oily wastewater treatment using a zirconia ceramic membrane : a literature review
Oczyszczanie ścieków olejowych przy zastosowaniu membran ceramicznych zawierających tlenek cyrkonu : przegląd literaturowy
Autorzy:
Kwaśny, J. A.
Kryłów, M.
Balcerzak, W.
Powiązania:
https://bibliotekanauki.pl/articles/205420.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
wastewater treatment
sol-gel method
ultrafiltration
microfiltration
oil-in-water emulsion
oczyszczanie ścieków
metoda zol-żel
ultrafiltracja
mikrofiltracja
emulsja olej-woda
Opis:
The goal of this article was to review the literature which discusses the problem of oily wastewater purification by membrane filtration. The authors focused on membranes containing zirconium compounds, mainly ZrO2, used in pressure driven membrane processes. The efficiency of the oil removal processes for various membranes (ceramic and composite), usually above 95% for the oil contaminated sewage, was compared. The influence of zirconium compounds on the properties of ceramic membranes was also discussed. The methods of producing ceramic membranes have been briefly characterized as well. Ceramic membranes are usually obtained by sol-gel technique but also by isostatic compression, reverse phase technique, or hydrothermal crystallization. Ceramic membranes are formed with zirconia, which cause an increase in filtration efficiency by improvement of hydrophilic properties of the membrane. Moreover, the addition of ZrO2 results in increased chemical and hydrothermal membrane stability. The efficiency of the filtration processes using the presented membranes was high, suggesting that membrane filtration processes are highly effective purification methods.
Artykuł stanowi przegląd literatury, w którym omówiono problem oczyszczania ścieków olejowych w oparciu o filtrację membranową. Skupiono się na membranach ciśnieniowych zawierających związki cyrkonu, głównie ZrO2. Porównano skuteczność procesów oczyszczania dla różnych membran (ceramicznych i kompozytowych). Omówiono wpływ związków cyrkonu na właściwości użytkowe membran ciśnieniowych. Membrany ceramiczne są zwykle uzyskiwane za pomocą techniki zol-żel, ale również przez prasowanie izostatyczne, technikę odwróconej fazy lub krystalizację hydrotermiczną. Membrany ceramiczne są formowane z tlenkiem cyrkonu, co skutkuje wzrostem skuteczności filtracji.
Źródło:
Archives of Environmental Protection; 2018, 44, 3; 3-10
2083-4772
2083-4810
Pojawia się w:
Archives of Environmental Protection
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Badania laboratoryjne nad opracowaniem emulsyjnych zaczynów cementowych typu woda w oleju
Laboratory tests on the development of water-in-oil emulsion based cement slurries
Autorzy:
Kut, Łukasz
Powiązania:
https://bibliotekanauki.pl/articles/1835020.pdf
Data publikacji:
2019
Wydawca:
Instytut Nafty i Gazu - Państwowy Instytut Badawczy
Tematy:
zaczyn cementowy
zaczyn emulsyjny
emulsja typu O/W i W/O
płuczka olejowa
płuczka inwersyjna
kamień cementowy
parametry mechaniczne
parametry technologiczne
cement slurry
emulsion slurry
oil-in-water emulsion
water-in-oil emulsion
oil mud
invert emulsion drilling mud
cement stone
mechanical parameters
technological parameters
Opis:
Dotychczas w Polsce żadne laboratorium nie prowadziło szczegółowych badań nad opracowaniem zaczynów cementowych sporządzonych na bazie płynu olej w wodzie, jak i woda w oleju. W przemyśle naftowym coraz częściej otwory wiertnicze wykonywane są przy użyciu płuczki inwersyjnej. Zastosowanie tego typu płuczki ma wiele pozytywnych aspektów, jednak zdarzają się też te negatywne. Jedną z niedogodności jest pozostawianie na ścianach otworu wiertniczego trudnego do usunięcia osadu, co w konsekwencji może wpływać na nieskuteczne uszczelnienie kolumny rur okładzinowych. Celem badań laboratoryjnych było więc opracowanie zaczynów cementowych sporządzonych na bazie różnych spoiw wiążących do uszczelniania kolumn rur okładzinowych po zastosowaniu płuczki inwersyjnej. Obecność oleju w składzie zaczynu cementowego może wpłynąć na jego większą kompatybilność z pozostawionymi na ścianach otworu osadami, a co za tym idzie – na skuteczniejsze uszczelnienie przestrzeni pierścieniowej. Jako cieczy zarobowej użyto wody wodociągowej, do której dodawano kolejno upłynniacz, środek powierzchniowo czynny (SPC) oraz cement. Po ujednorodnieniu mieszaniny dodawano do niej olej wymieszany z emulgatorem. Po połączeniu wszystkich składników zaczyn cementowy mieszano przez 30 minut, a następnie wykonywano pomiary laboratoryjne, takie jak: gęstość; parametry reologiczne; filtracja; czas wiązania; elektryczna stabilność emulsyjna. Z wybranych zaczynów sporządzono próbki kamieni cementowych. Próbki te utwardzano i przetrzymywano w dwóch różnych temperaturach: 25°C oraz 120°C. Otrzymane kamienie poddano badaniu: wytrzymałości kamienia cementowego na ściskanie; przyczepności kamienia cementowego do rur stalowych. Przeprowadzone badania wykazały, że pod względem parametrów reologicznych zaczynów cementowych lepszy okazał się cement glinowo-wapniowy od cementów portlandzkich. Zastosowanie tego cementu wpłynęło na obniżenie filtracji oraz znaczny wzrost elektrycznej stabilności emulsyjnej zaczynów cementowych. Ujednorodnienie mieszaniny oraz wspólne łączenie się poszczególnych dodatków nie stwarzało większych trudności. Jedynym mankamentem były niskie wartości otrzymanych parametrów kamieni cementowych, dlatego też istotne jest prowadzenie dalszych badań nad doborem odpowiednich receptur (Dębińska, 2012; Kremieniewski, 2012, 2013; Vipulanandan i Krishnamoorti, 2013).
So far, no laboratory in Poland, has conducted detailed research on the development of oil-in-water and water-in-oil cement slurries. In the oil industry, more and more boreholes are often drilled using an inversion mud. The use of this type of mud has many advantages and benefits, however, there are also negative aspects. One of the disadvantages is the difficulty to remove mud cake from the walls of the borehole, which may affect the sealing of the casing column. The aim of the research being presented, was to develop cement slurries, prepared based on various binders, used to seal the casing columns after the use of an invert emulsion drilling mud. The presence of oil in the composition of the cement slurry may affect its greater compatibility with the mud cake on the walls of the borehole and more effective sealing of the annular space. Sweet water played the role of the slurry. The dispersant, surfactant and cement were then added. After homogenizing the mixture, the oil mixed with the emulsifier was added. After combining all the components, the cement slurry was mixed for 30 minutes and the technological parameters such as density, rheological parameters, filtration, setting time and electrical stability were examined. Cement stone test samples were prepared from selected cement slurries. These samples were cured and hydrated at two different temperatures: 25°C and 120°C. The compressive strength and adhesion to steel pipes tests were performed for obtained cement stones. The conducted tests showed that better rheological parameters were obtained for aluminium-calcium cement in comparison to Portland. The use of this cement reduced the filtration and resulted in a significant increase in the electric emulsion stability of cement slurries. The homogeneity of the mixture and the combination of additives did not pose major difficulties. Parameters of the obtained cement stones were low, therefore it is important to conduct further research on the selection of appropriate recipes (Dębińska, 2012; Kremieniewski, 2012, 2013; Vipulanandan i Krishnamoorti, 2013).
Źródło:
Nafta-Gaz; 2019, 75, 4; 214-221
0867-8871
Pojawia się w:
Nafta-Gaz
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 27

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