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Wyszukujesz frazę "crystal size" wg kryterium: Temat


Wyświetlanie 1-5 z 5
Tytuł:
Enhancing filtration rate of new valley oxidized phosphate concentrate with additives
Autorzy:
Abdel-Aal, E.-S.
Abdel Rahman, E.
Kandil, A.-H.
Powiązania:
https://bibliotekanauki.pl/articles/110175.pdf
Data publikacji:
2016
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
New Valley phosphate concentrate
surfactant
filtration rate
gypsum morphology
crystal size distribution
Opis:
Phosphoric acid is utilized for production of fertilizers. It is mainly produced by wet processes, in which phosphate concentrate, produce by several operations including crushing, scrubbing, classification, attritioning, and desliming, is leached with sulfuric acid with coproduction of calcium sulfate dihydrate (phosphogypsum). The New Valley oxidized phosphate concentrate was processed for phosphoric acid production by addition of certain additives to improve gypsum filtration through modifying its morphology and particle size distribution. The additives used were cetylpyridinium chloride (CPC) as a cationic surfactant, sodium dodecyl sulfate (SDS) as an anionic surfactant and sulfonic acid (SA). The applied dosages ranged from 0.25 to 2.5 kg additive/Mg P2O5 in the phosphate concentrate. The filtration rate of the New Valley oxidized phosphate concentrate is 3.6 Mg P2O5 /m2day without additives. The filtration rate was increased by 33% and 31% with 1 and 0.8 kg/Mg P2O5 doses of CPC surfactant and sulfonic acid (SA), respectively. On the other hand, the filtration rate was decreased by 33% with addition of 1 kg/Mg P2O5 dose of SDS. The aspect ratios of gypsum crystals were 6:1, 3:1, 3:1 and 12:1 without additive, with CPC, SA and SDS surfactant, respectively. Reaction efficiencies without and with 0.8 kg/Mg P2O5 of CPC, SA and SDS dose of additives were 95.0%, 97.9%, 97.9% and 94.7%, respectively. The P2O5 recoveries without and with 0.8 kg/Mg P2O5 of CPC, SA and SDS dose of additives were 92.6%, 95.5%, 95.8% and 90.8%, respectively.
Źródło:
Physicochemical Problems of Mineral Processing; 2016, 52, 1; 124-135
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Friction Sensitivity of the ε-CL-20 Crystals Obtained in Precipitation Process
Autorzy:
Szczygielska, J.
Chlebna, S.
Maksimowski, P.
Skupiński, W.
Powiązania:
https://bibliotekanauki.pl/articles/358476.pdf
Data publikacji:
2011
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
CL-20
crystallization
friction sensitivity
shape and size of crystal
Opis:
The purpose of this work was to obtain samples of CL-20 by precipitation process in a solvent/nonsolvent system, under variable process parameters such as: antisolvent kind, time of nonsolvent addition, stirrer speed, mass of seeded crystals of ε-CL-20. Received samples were studied in the aspect of their sensitivity to friction. As the results of the crystallization processes were prepared crystals of different sizes and shapes depend on applied parameters. It was affirmed, that applied antisolvent has essential influence on type of received crystals. CL-20 crystals of cuboid shape and sizes of 80-200 μm were obtained by recrystallization from ethyl acetate/chloroform. As the result of the recrystallization from ethyl acetate/xylene crystals with rounded edges were obtained. Crystals, from both samples, were mostly single and showed the lowest sensitivity to friction. Also, the crystals of irregular shape and sharp-edged agglomerates were obtained from systems with n-heptane, isooctane, cyclohexane and toluene, which revealed the highest friction sensitivities.
Źródło:
Central European Journal of Energetic Materials; 2011, 8, 2; 117-130
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Reaction crystallization of struvite in a continuous DTM type crystallizer with a compressed air driven jet pump
Autorzy:
Matynia, A.
Mazieńczuk, A.
Piotrowski, K.
Wierzbowska, B.
Hutnik, N.
Kozik, A.
Powiązania:
https://bibliotekanauki.pl/articles/779281.pdf
Data publikacji:
2011
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
krystalizator DTM
strumienica
sprężone powietrze
krystalizacja
usuwanie fosforanów
struwit
rozkład miarowy kryształów
model kinetyczny
continuous DTM crystallizer
jet pump
compressed air
reaction crystallization
phosphates(V) removal
struvite
crystal size distribution
SIG kinetic model
Opis:
Experimental tests covering the production of struvite MgNH4PO4ź6H2O from water solutions containing 1.0 mass % of phosphate(V) ions using magnesium and ammonium ions in stoichiometric proportions were carried out in a crystallizer of 1.2 dm3 working volume. The process temperature was 298 K. Struvite crystals of mean size Lm from ca. 14 to ca. 38 µm were produced depending on the process environment's pH (9-11) and the mean residence time of suspension in a crystallizer, τ (900-3600 s). In such defined process conditions the linear growth rate of struvite crystals changed from 1.45ź10-8 m/s (pH 9, τ 900 s) to 2.06ź10-9 m/s (pH 11, τ 3600 s) while the nucleation rate from 5.1ź10^7 to 3.2ź10^9 1/(sm3). Crystal product of the most advantageous granular characteristics was produced at pH 9 and the mean residence time 3600 s. Within this product population the largest sizes reached above 200 µm while the number of crystals smaller than 3 mm was kept below 6%.
Źródło:
Polish Journal of Chemical Technology; 2011, 13, 2; 46-53
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Relationship between the Monomer Chain Length and the Electro-Optical Properties of Polymer Dispersed Liquid Crystals
Autorzy:
Liu, J.
Ozga, K.
Liu, X.
Zhen, Z.
Plucinski, K. J.
Szota, M.
Kityk, I. V.
Powiązania:
https://bibliotekanauki.pl/articles/958219.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
liquid crystal
electro-optical property
polymer dispersed
mesh size
response time
Opis:
Five polymers dispersed liquid crystalline (LC) films were fabricated using photo-polymerizable monomers with different lengths of carbon chains. These LC films have shown different electro-optical (EO) properties. Through their SEM pictures, the relationship between the linear electro-optical effect and the mesh size of the polymer network was explored. With the increase of number of photo-polymerizable monomers, the mesh size of the polymer network would become larger. So the liquid crystal molecules would be easily oriented in the electric field and therefore, the threshold voltage and saturation voltage would decrease. The open state response times were also reduced and the off state response times would be extended. The DFT simulations have shown principal role of the ground state dipole moments in the observed electro-optical efficiency.
Źródło:
Archives of Metallurgy and Materials; 2016, 61, 1; 457-460
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Powder Size on the Microstructure and Magnetic Properties of Nd-Fe-B Magnet Alloy
Autorzy:
Cho, Ju-Young
Abbas, Sardar Farhat
Choa, Yong-Ho
Kim, Taek-Soo
Powiązania:
https://bibliotekanauki.pl/articles/353634.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Nd-Fe-B
gas atomization
powder size
crystal orientation
hot deformation
Opis:
Rare earth Nd-Fe-B, a widely used magnet composition, was synthesized in a shape of powders using gas atomization, a rapid solidification based process. The microstructure and properties were investigated in accordance with solidification rate and densification. Detailed microstructural characterization was performed by using scanning electron microscope (SEM) and the structural properties were measured by using X-ray diffraction. Iron in the form of α-Fe phase was observed in powder of about 30 μm. It was expected that fraction of Nd2 Fe14 B phase increased rapidly with decrease in powder size, on the other hand that of α-Fe phase was decreased. Nd-rich phase diffused from grain boundary to particle boundary after hot deformation due to capillary action. The coercivity of the alloy decreased with increase in powder size. After hot deformation, Nd2 Fe14 B phase tend to align to c-axis.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 2; 623-626
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-5 z 5

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