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Wyszukujesz frazę "X-ray analysis," wg kryterium: Temat


Tytuł:
Identification of sandstone-related rocks composition using the X-ray analysis
Autorzy:
Kosuth, M.
Powiązania:
https://bibliotekanauki.pl/articles/344037.pdf
Data publikacji:
2013
Wydawca:
nakł. Maciej Pawlikowski
Tematy:
X-ray analysis
mineral composition
sandstones
siltstones
calcite
dolomite
Opis:
The article presents knowledge based on investigation of sandstones or siltstones composition from the Paleogene flysch terrains in North-East Slovakia. Samples of frequently crumbling clastic rocks were commonly considered to be close to sandstones, composed by predominant quartz. The set of such samples, belonging to Dukla Unit Sandstones were analyzed using the XRD analyses. Beside of quartz the diffraction patterns gave the evidence in significant carbonate share with some minor to minute feldspars, mica and chlorite contents. Among majority of analyzed samples we distinguish three groups of sandstones: (1) with the abundant calcite admixture, (2) the sandstones which contain meaning dolomite portion. The group (3) is representing the samples is formed the same by quartz as by both of carbonates, each of them could form important up to prevailed mineral component. Comparison of analyzed samples mineral composition shows remarkable trend of higher calcite and dolomite contents in younger clastic sediments.
Źródło:
Auxiliary Sciences in Archaeology, Preservation of Relics and Environmental Engineering; 2013, 16; 1-7
1689-6742
Pojawia się w:
Auxiliary Sciences in Archaeology, Preservation of Relics and Environmental Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structure, physical properties and fractal character of surface topography of CVD coatings
Autorzy:
Kwaśny, W.
Powiązania:
https://bibliotekanauki.pl/articles/100107.pdf
Data publikacji:
2011
Wydawca:
Wrocławska Rada Federacji Stowarzyszeń Naukowo-Technicznych
Tematy:
CVD coatings
fractal geometry
multifractal geometry
X-ray analysis
Opis:
The aim of the presented study is to establish a methodology elaboration, giving a possibility to predict properties of coatings reached in CVD process on tool materials, based on fractal quantities describing their surface. Coatings' topography and its structure which has an impact on a shape of analysed objects' surface were characterised in a comprehensive way. Influence of a type of process and conditions of deposition over structure and shape of topography as well as mechanical and operational properties of the acquired coatings were determined.
Źródło:
Journal of Machine Engineering; 2011, 11, No. 1-2; 134-151
1895-7595
2391-8071
Pojawia się w:
Journal of Machine Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Influence of Ceramic Coating on Mechanical Properties of Stainless Steel
Autorzy:
Czekaj, D.
Lisińska-Czekaj, A.
Krzysztofowicz, K.
Powiązania:
https://bibliotekanauki.pl/articles/353220.pdf
Data publikacji:
2020
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
stainless steel
X-ray analysis
microhardness
sol-gel ceramic coating
Opis:
Crystal structure and phase composition of stainless steel substrates (AISI 304 type) was studied and it was found that they adopted the cubic symmetry. The calculated elementary cell parameter for the mayor Fe-Ni phase (weight fraction 99%) was a = 3.593 Å, whereas the mean grain size was = 2932 Å. Morphology of the stainless steel substrate surface was studied with profilometry. Mechanical properties of the stainless steel substrates and stainless steel substrates coated with ceramic layer of barium strontium titanate were studied with microhardness tester. For measurements performed according to the Vickers method the average microhardness was found HV = 189 or HV = 186 for the “in-line” and “mapping” measurement pattern, respectively. The sol-gel method was used to coat the surface of the stainless steel substrate with a thin ceramic layer of the chemical composition Ba0.6 Sr0.4 TiO3 . It was found that the stainless steel substrate covered with sol-gel deposited ceramic coating exhibited the average hardness within the range HV = 217 up to HV = 235 for loading force F = 98 mN and F = 0.98 N, respectively. The Knopp method was also used and it was found that the stainless steel substrate with Ba0.6 Sr0.4 TiO3 coating exhibited hardness HK = 386.
Źródło:
Archives of Metallurgy and Materials; 2020, 65, 2; 911-916
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
N-N Bond Lengths and Initiation Reactivity of Nitramines
Autorzy:
Zeman, Svatopluk
Atalar, Taner
Růžička, Aleš
Powiązania:
https://bibliotekanauki.pl/articles/358441.pdf
Data publikacji:
2020
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
bond length
impact sensitivity
nitramines
reactivity
thermal decomposition
X-ray analysis
Opis:
For the 16 selected nitramines, it is shown that an increase in the energy content of these molecules (represented by enthalpies of formation) is connected with an increase in the lengths of the longest N–N bonds in the molecules. These lengths are directly proportional to the activation energies of the low-temperature thermal decomposition of the pure nitramines in all states of matter for this reaction. Raising the energy content also leads to reductions in the rate constants of thermal decomposition. Both of these facts are in contrast to expectations and also with similar published findings concerning thermal decomposition of nitramines in solution, which can be explained by the solvation effect and termination of the emerging aza-radicals in solutions. The calculated dissociation energies of the weakest N–N bonds yielded a relatively good reciprocal conformity with the lengths of the longest N–N bonds of the nitramines studied, especially when using the UB3LYP/6-31G* method. The relationship between the impact sensitivity of these nitramines and the lengths of their longest N–N bond is not completely clear. Such lengths cannot be a measure of impact reactivity, because the longest N–N bond might be stabilized in some cases by suitable intermolecular interactions with adjacent molecules in the crystal lattice.
Źródło:
Central European Journal of Energetic Materials; 2020, 17, 2; 169-200
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of X-ray fluorescence techniques for the determination of hazardous and essential trace elements in environmental and biological materials
Autorzy:
Bamford, S.
Wegrzynek, D.
Chinea-Cano, E.
Markowicz, A.
Powiązania:
https://bibliotekanauki.pl/articles/147255.pdf
Data publikacji:
2004
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
biological material
environmental materials
X-ray fluorescence analysis
Opis:
The utilization of X-ray fluorescence technique for the determination of trace element concentrations in environmental and biological samples is presented. The analytical methods used include energy dispersive X-ray fluorescence with polarizing secondary targets, total reflection X-ray fluorescence, direct in-situ X-ray fluorescence, and micro-beam X-ray fluorescence spectrometry. These methods were applied to analysis of different samples including soil, water, plant material and airborne particulate matter collected on polycarbonate filters. The performance and achieved detection limits of elements for different techniques, established by measuring appropriate reference standards, are presented. Also described is the utilization of micro-beam X-ray fluorescence technique for studying element distribution in heterogeneous samples and investigating the 2D- and 3D-morphology of minute samples by means of computerized X-ray absorption and X-ray fluorescence tomography. The different X-ray techniques have their unique advantages. The micro-beam X-ray fluorescence set-up has an advantage of producing very well collimated primary X-ray beam (about 15 mm in diameter), in front of which the analyzed sample can be precisely positioned, providing local information about the sample composition. The energy dispersive X-ray fluorescence with secondary targets offers rapid analysis of broad range of elements (Na–U) combined with a simple sample preparation method. Total reflection X-ray fluorescence technique, characterized by the lowest detection limits of elements, has its leading edge in analysis of liquid samples, and dealing with particle size effects in air particulates collected on filter papers. In-situ X-ray fluorescence spectrometers are truly portable and enable on the spot, in field analysis. It is shown that the combination of several XRF methods
Źródło:
Nukleonika; 2004, 49, 3; 87-95
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Metallurgical analysis of the causes of failure of the hardening furnace conveyor belt
Autorzy:
Merda, A.
Klimaszewska, K.
Sroka, M.
Golański, G.
Powiązania:
https://bibliotekanauki.pl/articles/378641.pdf
Data publikacji:
2019
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
microstructure
X-ray phase analysis
precipitates
failure
mikrostruktura
rentgenowska analiza fazowa
osady
niepowodzenie
Opis:
Purpose: The aim of the tests was to analyze the microstructure and mechanical properties of a section of the hardening furnace conveyor belt serviced at the temperature of 880-920°C in the carburizing atmosphere, in the context of determining the probable causes of its failure. Design/methodology/approach: The scope of performed tests included: chemical composition analysis of the steel and particles, microstructure investigated using optical and scanning electron microscopy, X-ray phase analysis. Findings: The analysis of the chemical composition showed that the examined material was austenitic steel X15CrNiSi25-21 (S310). Performed metallurgical tests showed that after the service the examined steel was characterized by austenitic structure with numerous precipitates of diverse morphology. In the structure the sigma phase particles and probably the M23C6 carbides precipitates were observed. The continuous grid of precipitates on the boundaries of grains (mainly the sigma phase) and the influence of the cyclic changing heat loads (or thermo-mechanical loads) were the main causes of failure of the analysed detail. Research limitations/implications: The aim of the work was to determine the probable causes of damage of the material used for a conveyor belt of a hardening furnace. Practical implications: The results of investigation and analysis of the metallographic of het-resisting austenitic steel X15CrNiSi25-21 (S310) after service at the temperature of 880-920°C are presented. Originality/value: The paper presents the results of research on the microstructure and mechanical properties of the section of hardening furnace conveyor belt made of creepresisting austenitic steel. The aim of the performed tests was to determine the probable causes of damage of the analysed detail.
Źródło:
Archives of Materials Science and Engineering; 2019, 98, 2; 68-73
1897-2764
Pojawia się w:
Archives of Materials Science and Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Mechanical behaviour and phase transition mechanisms of a shape memory alloy by means of a novel analytical model
Autorzy:
Carpinteri, A.
Di Cocco, V.
Fortese, G.
Ronchei, C.
Scorza, D.
Vantadori, S.
Zanichelli, A.
Iacoviello, F.
Natali, S.
Powiązania:
https://bibliotekanauki.pl/articles/386617.pdf
Data publikacji:
2018
Wydawca:
Politechnika Białostocka. Oficyna Wydawnicza Politechniki Białostockiej
Tematy:
fatigue behaviour
phase transition mechanisms
shape memory alloy
tensile cyclic test
x-ray diffraction analysis
Opis:
The aim of the present paper is to examine both the fatigue behaviour and the phase transition mechanisms of an equiatomic pseudo-elastic NiTi Shape Memory Alloy through cyclic tests (up to 100 loading cycles). More precisely, miniaturised dog-bone specimens are tested by using a customised testing machine and the contents of both austenite and martensite phase are experimentally measured by means of X-Ray diffraction (XRD) analyses. On the basis of such experimental results in terms of martensite content, an analytical model is here formulated to correlate the stress-strain relationship to the phase transition mechanisms. Finally, a validation of the present model by means of experimental data pertaining the stress-strain relationship is performed.
Źródło:
Acta Mechanica et Automatica; 2018, 12, 2; 105-108
1898-4088
2300-5319
Pojawia się w:
Acta Mechanica et Automatica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Wear resistance of aluminized steel plates
Odporność na scieranie aluminiowanych taśm stalowych
Autorzy:
Żaba, K.
Powiązania:
https://bibliotekanauki.pl/articles/352691.pdf
Data publikacji:
2011
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminiowana taśma stalowa
odporność na ścieranie
powłoki
chropowatość
aluminized steel plate
abrasion resistance
coatings
roughness
X-ray phase analysis
Opis:
The results of the abrasion resistance measurements of aluminized steel strips are presented in the hereby paper. Steel strips of DX52D+AS120 grade, before and after a heat treatment at temperatures of 200-1000 C for 1 – 5760 minutes, were tested. Tests of the abrasion resistance were carried on in a specially built device: rotating disk – sample performing a plane-rotary motion, with an application of a lubricating medium. Examinations of the abrasion resistance were also performed by means of the block-on-ring tester. Estimations of a coating mass loss, roughness and thickness changes were carried on. The obtained results are illustrated by diagrams and macro- and micro-observations. Phase analysis investigations were also performed on samples selected after the abrasibility testing. The range of the heat treatment parameters – after which the Al-Si coating increased its abrasion resistance – was estimated.
W artykule przedstawiono wyniki badan odpornosci na ścieranie aluminiowanych tasm stalowych. Badaniom poddano taśmy stalowe z gatunku DX52D+AS120 przed i po obróbce cieplnej w temperaturze 200-1000 C w czasie 1min-5760min. Wykonano badania odporności na ścieranie w specjalnie przygotowanym urzadzeniu typu obracająca się tarcza – próbka, wykonujaca ruch posuwisto-zwrotny, przy zastosowaniu środka smarujacego Zrealizowano także badania odporności na zużycie cierne za pomocą testera typu rolka-klocek. Dokonano oceny ubytku masy, zmian chropowatoąci i grubości powłoki. Wyniki badan zobrazowano za pomocą wykresów oraz makro i mikro obserwacji. Przeprowadzono także badania analizy fazowej na próbkach wytypowanych po badaniach ścieralności. Określono taki zakres parametrów obróbki cieplnej, po której następuje wzrost odporności na ścieranie powłoki Al-Si.
Źródło:
Archives of Metallurgy and Materials; 2011, 56, 4; 871-882
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
X-Ray Phase Analysis of Nitrided Layers of X2CrNiMo17-12-2 Austenitic Steel
Rentgenowska analiza fazowa warstw azotowanych stali austenitycznej X2CrNiMo17-12-2
Autorzy:
Frączek, T.
Olejnik, M.
Pilarska, M.
Powiązania:
https://bibliotekanauki.pl/articles/354335.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
X-ray phase analysis
nitrided layers
stal austeniczna X2CrNiMo17-12-2
rentgenowska analiza fazowa
warstwy azotowane
stal austenityczna X2CrNiMo17-12-2
Opis:
This work presents the results of diffraction analyses carried out using X-ray phase analyses (XRD and GIXRD) of nitrided layers of X2CrNiMo17-12-2 austenitic steel. Plasma nitriding process was c arried out in the temperature range of 325 ÷ 400 °C and time of 2 ÷ 4 h. Hydrogen-nitrogen plasma was used as reactive atmosphere (H2 75% + N2 25%) with pressure of 150 Pa. On the basis of the X-ray analyses it was stated that the obtained nitrided layers consisted of a subsurface layer of chromium nitrides and a zone of nitrogen saturated austenite.
W pracy zaprezentowano wyniki badań strukturalnych metodą rentgenowskiej analizy fazowej (XRD i GIXRD) warstw azotowanych na podłożu stali austenitycznej X2CrNiMo17-12-2. Proces azotowania jarzeniowego przeprowadzono w zakresie temperatur 325 ÷ 400 °C i czasu 2 ÷ 4 h. Atmosferę reaktywną stanowiła plazma wodorowo-azotowa (H2 75% + N2 25%) o ciśnieniu 150 Pa. Na podstawie badań rentgenowskich stwierdzono, że otrzymane warstwy azotowane składają się z przypowierzchniowej warstwy azotków chromu oraz strefy austenitu przesyconego azotem. Zastosowanie ekranu aktywnego spowodowało wzrost głębokości dyfuzji azotu w głąb azotowanej powierzchni oraz zwiększyło jego koncentrację w fazie austenitu przesyconego azotem.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 3A; 2005-2012
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Characterisation of Mg-Zn-Ca-Y powders manufactured by mechanical milling
Autorzy:
Lesz, S.
Tański, T.
Hrapkowicz, B.
Karolus, M.
Popis, J.
Wiechniak, K.
Powiązania:
https://bibliotekanauki.pl/articles/1818808.pdf
Data publikacji:
2020
Wydawca:
Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
Tematy:
Mg-based alloys
scanning electron microscopy
X-ray diffraction analysis
mechanical alloying
stopy magnezu
skaningowa mikroskopia elektronowa
rentgenowska analiza dyfrakcyjna
mechaniczna synteza
Opis:
Purpose: This paper explains mechanical synthesis which uses powders or material chunks in order to obtain phases and alloys. It is based on an example of magnesium powders with various additives, such as zinc, calcium and yttrium. Design/methodology/approach: The following experimental techniques were used: X-ray diffraction (XRD) method, scanning electron microscopy (SEM), determining particle size distributions with laser measuring, Vickers microhardness. Findings: The particle-size of a powder and microhardness value depend on the milling time. Research limitations/implications: Magnesium gained its largest application area by creating alloys in combination with other elements. Magnesium alloys used in various industry contain various elements e.g. rare-earth elements (REE). Magnesium alloys are generally made by casting processes. Consequently, the search for new methods of obtaining materials such as mechanical alloying (MA) offers new opportunities. The MA allows for the production of materials with completely new physico-chemical properties. Originality/value: Thanks to powder engineering it is possible to manufacture materials with specific chemical composition. These materials are characterized by very high purity, specified porosity, fine-grain structure, complicated designs. These are impossible to obtain with traditional methods. Moreover it is possible to refine the process even further minimalizing the need for finishing or machining, making the material losses very small or negligible. Furthermore material manufactured in such a way can be thermally or chemically processed without any problems.
Źródło:
Journal of Achievements in Materials and Manufacturing Engineering; 2020, 103, 2; 49--59
1734-8412
Pojawia się w:
Journal of Achievements in Materials and Manufacturing Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Clay minerals as palaeoenvironmental indicators in the Bathonian (Middle Jurassic) ore-bearing clays from Gnaszyn, Kraków-Silesia Homocline
Autorzy:
Dudek, T.
Powiązania:
https://bibliotekanauki.pl/articles/139440.pdf
Data publikacji:
2012
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
analiza ilościowa
chloryn
dyfrakcja rentgenowska
glaukonit
illit
iły
kaolin
Skład minerałów
chlorite
clays
glauconite
illite
kaolinite
Mineral assemblage
X-ray diffraction quantitative analysis
Opis:
This paper reports the results of X-ray diffraction quantitative mineralogical studies of the clay-rich Middle Jurassic sedimentary rocks from Gnaszyn, central Poland and their palaeoenvironmental interpretation. The palaeoenvironmental interpretation is aided by the fact that the sediments have not been significantly altered by diagenesis. The mineral composition is uniform throughout the succession: quartz, K-feldspar, plagioclase, calcite, gypsum, anhydrite, pyrite, illite, kaolinite, chlorite, and glauconite. The clay assemblage is dominated by illite, which alone accounts for about 20 wt% of the total mineral content. Kaolinite amounts usually <10 wt% and chlorite and glauconite occur in subordinate quantities. The clay mineral assemblage is largely of detrital origin and indicates rather cool and/or dry climatic conditions favouring mechanical erosion of the source rocks.
Źródło:
Acta Geologica Polonica; 2012, 62, 3; 297-305
0001-5709
Pojawia się w:
Acta Geologica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Study of phase and chemical composition of Bi1-xNdxFeO3 powders derived by pressureless sintering
Badanie składu fazowego oraz chemicznego proszków Bi1-xNdxFeO3 spiekanych swobodnie
Autorzy:
Dzik, J.
Lisińska-Czekaj, A.
Zarycka, A.
Czekaj, D.
Powiązania:
https://bibliotekanauki.pl/articles/353066.pdf
Data publikacji:
2013
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
BiFeO3 ceramics
Nd3+ doping
X-ray phase and structural analysis
ceramika BiFeO3
rentgenowska analiza fazowa i strukturalna
Opis:
In the present paper studies on Bi1-xNdxFeO3 for x =0.1-0.4 are reported. The mixed oxide method followed with pressureless sintering was employed for ceramics fabrication. Thermal behavior of stoichiometric mixtures of simple oxide powders, viz. Bi2O3, Nd2O3 and Fe2O3 was studied by simultaneous thermal analysis. It was found that with an increase in neodymium content the weight loss increased from 0.75% to 3.16% for x =0.1 and x =0.4, respectively. It was found that weight loss took place mainly within two temperature ranges, namely ΔT1 ≈(300-400)0C and ΔT2 ≈(600-800)°C. Bi1-xNdxFeO3 ceramics was studied in terms of its phase composition (X-ray phase analysis) and chemical composition (EDS method) at room temperature. It was found that Bi1-xNdxFeO3 suffered structural phase transition from rhombohedral to orthorhombic symmetry with an increase in neodymium concentration x within the range x =(0.2-0.3).
W niniejszej pracy zaprezentowano wyniki badań ceramiki Bi1-xNdxFeO3 dla x =0,1-0,4. Do wytworzenia ceramiki zastosowano metodę reakcji w fazie stałej z mieszaniny tlenków wyjściowych Bi2O3, Nd2O3 i Fe2O3 spiekanej swobodnie w atmosferze powietrza. Analiza termiczna stechiometrycznej mieszaniny proszków wykazała wzrost ubytku masy proszku przy wzroście zawartości (x) neodymu w mieszaninie (od 0,75% do 3,16% dla x =0,1 i x =0,4 odpowiednio). Stwierdzono, że ubytek masy zachodzi głównie w dwóch zakresach temperatury, a mianowicie ΔT1 ≈ (300-400)°C i ΔT2 ≈ (600-800)°C. Ceramika Bi1-xNdxFeO3 została poddana charakterystyce składu fazowego (rentgenowska analiza fazowa) oraz składu chemicznego (metoda EDS) w temperaturze pokojowej. Stwierdzono, że Bi1-xNdxFeO3 przejawia strukturalną przemianę fazową z fazy romboedrycznej do rombowej przy wzroście koncentracji neodymu w zakresie x =(0.2-0.3).
Źródło:
Archives of Metallurgy and Materials; 2013, 58, 4; 1371-1376
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of X-Ray Diffraction to Analyse Phase Composition of Aluminium Alloys for Plastic Working
Autorzy:
Pachut, K.
Żelechowski, J.
Boczkal, S.
Powiązania:
https://bibliotekanauki.pl/articles/354144.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
aluminium alloys
X-ray diffraction
qualitative phase analysis
Opis:
An attempt was made to determine phase composition of commercial aluminium alloys using X-ray diffraction. Samples for phase composition analysis were selected from the group of aluminium alloys covered by the EN 573-3:2013 standard [1]. Representative samples were taken from eight groups of alloys with different chemical composition (at least one sample from each group). The diffraction intensity was measured with a standard X-ray diffractometer in Bragg-Brentano geometry in a way that allowed identification of the weakest diffraction peaks. As a results of the performed research it has been shown that X-ray phase analysis can be used to identify the matrix of aluminium alloys, Si and crystalline intermetallic phases such as Mg2Si, Al93.38Cu6.02Fe24Si16.27, Al4.01MnSi0.74, MgZn2, Al17 (Fe3.2Mn0.8)Si2, Al65Cu20Fe15, and Cu3Mn2Al. The detectability limit of the above-mentioned phases is better than 0.5%. The research has also shown that X-ray phase analysis is applicable in the investigation of phase transformations taking place in aluminium alloys.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 4; 1315-1319
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Computer system for analysis of X-ray images of wheat grains
Autorzy:
Strumillo, A.
Niewczas, J.
Szczypinski, P.
Makowski, P.
Wozniak, W.
Powiązania:
https://bibliotekanauki.pl/articles/24261.pdf
Data publikacji:
1999
Wydawca:
Polska Akademia Nauk. Instytut Agrofizyki PAN
Tematy:
wheat
grain
computer system
X-ray image
image analysis
Źródło:
International Agrophysics; 1999, 13, 1
0236-8722
Pojawia się w:
International Agrophysics
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Thermal decomposition characterization of supergene potassium-jarosite and sodium-jarosite minerals from the northern Tibetan Plateau, China
Autorzy:
Chen, L.
Powiązania:
https://bibliotekanauki.pl/articles/949691.pdf
Data publikacji:
2018
Wydawca:
Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
Tematy:
potassium-jarosite
sodium-jarosite
thermogravimetric analysis
X-ray diffraction
Opis:
The thermal decomposition of supergene potassium-jarosite and sodium-jarosite samples from the weathering profiles of sulfide deposits in the northern Tibetan Plateau, China, was investigated. Electron microprobe, scanning electron microscopy, and X-ray diffraction analyses indicated the presence of nearly pure potassium-jarosite and sodium-jarosite. Thermogravimetric analysis of the potassium-jarosite sample revealed mass losses of 11.39 wt% at 443.0 °C, 20.99 wt% at 688.3 °C, and 3.18 wt% at 779.3 °C. The thermogravimetric analysis of sodium-jarosite revealed mass losses of 11.72 wt% at 447.5 °C, 21.32 wt% at 682.6 °C, and 3.70 wt% at 716.5 °C. The results provide no evidence for water-molecule loss below 400 °C, as has been reported previously for natural potassium-jarosite and sodium-jarosite. Thermal-decomposition mechanisms have been proposed for potassium-jarosite and sodium-jarosite based on X-ray diffraction analyses of samples obtained at distinct points along the respective thermal decomposition processes. A comparison of the thermal analysis patterns of potassium-jarosite and sodium-jarosite indicates that sodium-jarosite undergoes the initiation of lattice destruction at a higher temperature.
Źródło:
Physicochemical Problems of Mineral Processing; 2018, 54, 2; 459-466
1643-1049
2084-4735
Pojawia się w:
Physicochemical Problems of Mineral Processing
Dostawca treści:
Biblioteka Nauki
Artykuł

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