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    Wyświetlanie 1-3 z 3
    Tytuł:
    Characterization of magnesia-doped yttria-stabilized zirconia powders for dental technology applications
    Autorzy:
    Nakonieczny, D.
    Walke, W.
    Majewska, J.
    Paszenda, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/307056.pdf
    Data publikacji:
    2014
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    stomatologia
    protetyka
    materiały protetyczne
    metoda zol-żel
    full ceramic restorations
    prosthetic dentistry
    sol-gel method
    Zirconium Oxide
    Opis:
    Purpose: This paper is focused on the works concerning on preparing zirconium oxide ceramic blocks recommended for CAD/CAM systems used in prosthetic dentistry for manufacturing fixed prosthetic restorations. Methods: Zirconium-yttrium-magnesium mixed ceramic oxides were prepared by sol-gel method via hydrolysis and condensation of zirconium alkoxide precursor (zirconium (IV) propoxide) with yttrium and magnesium nitrates diluted in 2-propanol. The aim of this work it was to obtain 2% mol yttria stabilized zirconia ceramic powders with magnesium as an additional tetragonal ZrO2 phase stabilizer in amount between 2÷6% mol (with 2% variable). Prepared gels were dried (24 h in 65°C). Obtained powders were mixed with binder (carboxymethyl cellulose) and uniaxial pressed in to a specimens with diameter 38 x 22 x 6 mm. Afterwards green bodies were sintered in range of temperature between 1350-1550°C. Powders and blocks were characterized by Scanning Electron Microscopy, Fourier Transform Infrared Spectroscopy, Specific Area Measurement. Results: Highly homogeneous powders with a low open porosity, was obtained. Prepared blocks after sintering showed numerous cracks. Nevertheless blocks was fine grained and show quite reproducible chemical composition. Conclusion: A sol gel wet chemical route of powder synthesis allow to obtain high homogenous ceramic materials with inconsiderable amount of pores with low variation in a diameter. In spite of a reproducible synthesis methods of a ceramic powders, applied to prepare green bodies procedure and sintering manner do not allowed to obtain free from cracks zirconia ceramics blocks.
    Źródło:
    Acta of Bioengineering and Biomechanics; 2014, 16, 4; 99-106
    1509-409X
    2450-6303
    Pojawia się w:
    Acta of Bioengineering and Biomechanics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    ZrO2-CeO2 ceramic powders obtained from a sol-gel process using acetylacetone as a chelating agent for potential application in prosthetic dentistry
    Autorzy:
    Nakonieczny, D.
    Paszenda, Z.
    Drewniak, S.
    Radko, T.
    Lis, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/306436.pdf
    Data publikacji:
    2016
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    proces zol-żel
    metody rentgenowskie
    analiza termiczna
    ZrO2
    protetyka
    sol-gel process
    X-ray Methods
    Thermal Analysis
    Prosthetic Dentistry
    Opis:
    Purpose: The main objective of this study was to obtain single-phase β-ZrO2 powders with so-called soft agglomerates reproducibile morphology with acetyl-acetone as a chelating-agent. To the best of our knowledge there is no avaiable data which determine the effect of acetyl acetone on the phase composition and morphology of ceria-doped ZrO2 powders for biomedical applications. Methods: Twenty variants of powders with different water to zirconia precursor and acetylacetone to zirconia precursor molar ratios were prepared. 0.9ZrO20.1CeO2 powders were obtained by a hydrolysis and condensation and further calcination of zirconium n-propoxide in a simple one-step sol-gel process. Influence of acetyloacetone to zirconia precursor on the phase composition ratio and water to zirconia precursor was investigated. Samples have been characterized by X-ray diffraction (XRD), Raman spectroscopy (RS), thermal analysis (TGA/DTA) and scanning electron microscopy (SEM) measurements. Results: Ceramic powders prepared by sol-gel process, according to the various concentration of chelating agent and water show different morphology and phase composition. Conclusions: Higher molar ratios of AcAc in range with smaller amounts of water cause hard agglomerates, obtained powders are characterized by highly thermally stable behaviour and various phase composition. With higher molar ratios of water to zirconium-n-propoxide so-called soft agglomerates and one phase powders are obtained.
    Źródło:
    Acta of Bioengineering and Biomechanics; 2016, 18, 3; 53-60
    1509-409X
    2450-6303
    Pojawia się w:
    Acta of Bioengineering and Biomechanics
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Application of polymer impression masses for the obtaining of dental working models for the stereolithographic 3D printing
    Autorzy:
    Dobrzański, L. B.
    Achtelik-Franczak, A.
    Dobrzańska, J.
    Pietrucha, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/378584.pdf
    Data publikacji:
    2019
    Wydawca:
    Stowarzyszenie Komputerowej Nauki o Materiałach i Inżynierii Powierzchni w Gliwicach
    Tematy:
    polyvinyl siloxane impression material
    alignate impression material
    CAD/CAM in dentistry
    digital prosthetic working models
    materiał wyciskowy poliwinylosiloksanowy
    materiał wyciskowy alginianowy
    CAD/CAM w stomatologii
    Opis:
    Purpose: The aim of the work is to execute measurements of digital dental models taken by scanning prosthetic impressions using the engineering CAD software and finding dimensional differences and scale factor for precise reproduction of patient tooth dimensions. Design/methodology/approach: Tests were carried out involving the execution of 3 series of impressions for selected impression materials, which were then scanned using two types of prosthetic scanners. Gypsum models based on mentioned impressions were scanned and dimensionally compared with impression-based digital models. Benchmark impressions were also performed in order to verify the obtained results and determine the correction factor for dimensions. The dimensional differences between impression groups were calculated by using Engineering CAD software. Findings: It was found, that compared to the base model, the digital model has a smaller volume than the object being mapped, the digital models based directly on the impression should be 0.09 - 0.12% rescaled to match the dimensions of the base model. Research limitations/implications: It is necessary to perform a practical verification of the results achieved and apply the determined coefficient in practice by creating working models using precise devices such as a 3D SLA printer and verify their results with intraoral scanner based models. Practical implications: This test will allow making precise working models using a 3D printer, allowing finally to perform, for example, implant-based bridges directly from the level of implants, using the masses described in the study. Originality/value: The comparative studies of polyvinyl siloxane and alignate impression materials were carried out in order to measure dimensional differences between working models made directly from the impression and gypsum models and compared with pattern, which allowed to determine the expansion coefficient, which will allow to work in 3D printing technology with close representation of real situation in the patient's oral cavity, which is particularly important when performing full arch bridges and extensive work on implants, including direct implants. The work has practical applications for both dental engineers and dentists performing advanced prosthetic work.
    Źródło:
    Archives of Materials Science and Engineering; 2019, 95, 1; 31-40
    1897-2764
    Pojawia się w:
    Archives of Materials Science and Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-3 z 3

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