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    Wyświetlanie 1-8 z 8
    Tytuł:
    Copper deposition on stainless steel sheets in copper nitrate solution
    Autorzy:
    Kekki, A.
    Aromaa, J.
    Forsen, O.
    Powiązania:
    https://bibliotekanauki.pl/articles/110678.pdf
    Data publikacji:
    2015
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    copper nitrate
    electrorefining
    high purity copper
    hydrometallurgy
    Opis:
    The aim of this study was to examine factors that influence copper nitrate based electrorefining of copper and to search the best process parameters for high-purity copper deposition on AISI 316L steel blanks. Considering impurities, the most important goal was to minimize sulfur content in a copper cathode. The effect of Cu2+ concentration, current density, temperature and pH were studied. The best parameters for the best copper purity were sorted out. The most important factors for quality copper deposition are sufficiently low Cu2+ concentration, low current density, right zone and careful control of pH. Active nitrate ion reduction reactions catalyzed by copper ions are suggested to affect detrimentally both copper deposition current efficiency and purity. Furthermore, nitrate ion reactions seem to elevate an electrolyte pH so that the deposition appears to be dark brow copper oxide. The 6N purity for copper was not reached with this cell construction and it felled behind about 7 ppm (99.9993% Cu). Both, sulfur and silver concentration were slightly above 1 - 2 ppm. To minimize the impurities, electrolyte circulation and filtration are needed. Also, either a separate silver cementation cell or cementation membrane is needed.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2015, 51, 1; 247-256
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    A method of proppant pack permeability assessment
    Autorzy:
    Lutynski, M. A.
    Powiązania:
    https://bibliotekanauki.pl/articles/110881.pdf
    Data publikacji:
    2015
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    copper nitrate
    electrorefining
    high purity copper
    hydrometallurgy
    Opis:
    Hydraulic fracturing methods used for low permeability reservoirs such as shale gas or tight gas require the use of proppants. The current standard used for proppant assessment does not take into account its interaction with the rock and the embedment effect. In this paper a new method of proppant pack permeability assessment is proposed where proppant is placed into a rock sample with induced fracture. Three types of proppant were assessed to verify the method i.e. offshore sand, onshore sand and ceramic proppant. The rock sample was a Tumlin sandstone. As the flowing medium supercritical carbon dioxide was used. Tests were performed with 300-500 μm size proppants at flowing pressure of 3 MPa and confining pressure of 5 MPa. Additional test was conducted with 1–2 mm sand proppant at two confining pressure, i.e. 5 MPa and 16 MPa. Proppant were characterized in accordance with the Krumbein/Sloss diagram. Similar values of permeability for the proppant concentration of 0.5 kg/m2 were obtained ranging from 2.3 to 3.3 D although the highest permeability was achieved with Baltic sand proppant and ceramic proppant. For the larger size of proppant (1 – 2 mm) the initial permeability with confining pressure of 5 MPa was initially larger but when the confining pressure was increased it declined by 37%. This proves that in the proposed method we can observe changes in the permeability of the fracture with change in confining pressure apply subjected to the sample.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2015, 51, 1; 325-334
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Fabrication of 4N5 Grade Tantalum Wire from Tantalum Scrap by EBM and Drawing
    Autorzy:
    Yu, Ji-Won
    Choi, Sang-Hoon
    Sim, Jae-Jin
    Lim, Jae-Hong
    Seo, Kyoung-Deok
    Hyun, Soong-Keon
    Kim, Tae-Youb
    Gu, Bon-Woo
    Park, Kyoung-Tae
    Powiązania:
    https://bibliotekanauki.pl/articles/353005.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    electron beam melting
    drawing
    tantalum scrap
    recycling
    high purity
    Opis:
    Electron beam melting(EBM) is a useful technique to obtain high-purity metal ingots. It is also used for melting refractory metals such as tantalum, which require melting techniques employing a high-energy heat source. Drawing is a method which is used to convert the ingot into a wire shape. The required thickness of the wire is achieved by drawing the ingot from a drawing die with a hole of similar size. This process is used to achieve high purity tantalum springs, which are an essential component of lithography lamp in semiconductor manufacturing process. Moreover, high-purity tantalum is used in other applications such as sputtering targets for semiconductors. Studies related to recycling of tantalum from these components have not been carried outuntil now. The recycling of tantalum is vital for environmental and economic reasons. In order to obtain high-purity tantalum ingot, in this study impurities contained in the scrap were removed by electron beam melting after pre-treatment using aqua regia. The purity of the ingot was then analyzed to be more than 4N5 (99.995%). Subsequently, drawing was performed using the rod melted by electron beam melting. Owing to continuous drawing, the diameter of the tantalum wire decreased to 0.5 mm from 9 mm. The hardness and oxygen concentration of the tantalum ingot were 149 Hv and less than 300 ppm, respectively, whereas the hardness of the tantalum wire was 232.12 Hv. In conclusion, 4N5 grade tantalum wire was successfully fabricated from tantalum scrap by EBM and drawing techniques. Furthermore, procedure to successfully recycle Tantalum from scraps was established.
    Źródło:
    Archives of Metallurgy and Materials; 2019, 64, 3; 935-941
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Biodiesel Production from Crude Palm Oil Using Kapok Skin KOH (Ceiba Pentandra) Catalyst as Solid Green Catalyst
    Autorzy:
    Jalaluddin
    Ginting, Zainuddin
    Maliki, Syariful
    Setiawan, Arif
    Zulfa
    Powiązania:
    https://bibliotekanauki.pl/articles/2086431.pdf
    Data publikacji:
    2022
    Wydawca:
    Polskie Towarzystwo Inżynierii Ekologicznej
    Tematy:
    biodiesel
    crude palm oil
    high purity
    Ceiba Pentandra
    THF
    tetrahydrofuran
    Opis:
    Biodiesel is one type of renewable alternative energy that has great potential to be developed. Biodiesel is a fuel consisting of a mixture of mono-alkyl esters of long-chain fatty acids made from renewable sources, such as vegetable oils or animal fats, one of which is crude palm oil (CPO). Crude palm oil contains free fatty acids in high levels, so treatment is needed to reduce free fatty acids by a reaction known as the esterification reaction. Then, the transesterification process is carried out to produce biodiesel (methyl ester). The purpose of this study was to analyze the effect of catalyst mass, a mole ratio of CPO to moles of methanol and the effect of adding THF co-solvent to biodiesel purity. The catalyst used is a heterogeneous catalyst from kapok fruit peel waste. Kapok fruit rind was calcined at 700°C for 8 hours. The independent variable varied the mole ratio of oil to methanol in a 1:4 ratio; 1:6; 1:8; and 1:10 with a catalyst weight variation of 3 and 4%. Meanwhile, for the addition of co-solvent, variations of THF: methanol v/v 1:1 and 2:1, were carried out. The biodiesel properties such as density, viscosity, water content and acid number, were evaluated and compared with the Indonesian National Standard. The results showed that the transesterification reaction with the addition of co-solvent resulted in a higher methyl ester content than that without the addition of co-solvent. The highest yield of methyl ester without the addition of co-solvent was 79.16%, while the yield of the methyl ester with the addition of THF co-solvent with a ratio of 1:1 and 2:1 v/v to methanol was 90.09 and 94.09%, respectively. The highest methyl ester content (94.09%) was achieved by the addition of THF: methanol = 2:1, CPO: methanol molar ratio = 1:6 and 4 wt% catalyst weight. The results obtained in this study indicate that a green catalyst made from kapok skin can be used to produce biodiesel and also the addition of co-solvent can increase the yield of methyl esters, so that high purity is obtained.
    Źródło:
    Journal of Ecological Engineering; 2022, 23, 5; 286--292
    2299-8993
    Pojawia się w:
    Journal of Ecological Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preparation and Up-conversion Luminescence of Yb3+/Er3+/GZO Ceramics
    Autorzy:
    Li, G.
    Wang, B.
    Wang, R.
    Liu, H.
    Powiązania:
    https://bibliotekanauki.pl/articles/779137.pdf
    Data publikacji:
    2018
    Wydawca:
    Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
    Tematy:
    Up-conversion
    Yb3+/Er3+/GZO
    Ceramics
    High purity
    Luminescence
    Opis:
    Yb3+/Er3+/GZO ceramics have been synthesized with high temperature solid-state method. The phase and structure of the Yb3+/Er3+/GZO ceramics were characterized by X-ray diffraction (XRD). The XRD pattern that following ions Yb3+, Er3+ and Ga3+ were well doped into the ZnO lattice. Effi cient visible up-conversion (UC) red and green emission were observed under 980 nm excitation. The mechanism of the UC luminescence is investigated on the basis of the UC luminescence emission spectra, the power curve and energy level diagram. The infl uence of doping ions to the intensity ratio of red to green is analyzed and high purity of red light (red/green = 29.9) is fi nally obtained.
    Źródło:
    Polish Journal of Chemical Technology; 2018, 20, 3; 15-19
    1509-8117
    1899-4741
    Pojawia się w:
    Polish Journal of Chemical Technology
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Study On The Electro-Refining Of Tin In Acid Solution From Electronic Waste
    Badanie elektrorafinacji cyny w roztworze kwasu z e-odpadów
    Autorzy:
    Son, S. H.
    Park, S. C.
    Kim, J. H.
    Kim, Y. H.
    Lee, M. S.
    Ahn, J.-W.
    Powiązania:
    https://bibliotekanauki.pl/articles/352665.pdf
    Data publikacji:
    2015
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    electrorefining
    tin
    electronic waste
    recycling
    high purity
    elektrorafinacja
    cyna
    odpady elektroniczne
    recykling
    Opis:
    The tin metal could be retractable from wasted tin scrap, sludge, and wasted electroplated solution hydrometallurgical treatment, and purification process. In order to be used as resource of electronic devices, the retracted crude metal should be purified to the extent of higher than 99.9%. In this study, tin electro-refining process was performed to purify the casted tin crude metal at various experimental conditions: at the current density of 3, 5A/dm2, and in various electrolytes such as hydrochloric acid, sulfuric acid and methansulfonic acid. Additional experiment was conducted using Rotating Disk Electrode (RDE) in order to investigate the rate determining step of tin electro-refining process. The current efficiency, 65.6%, was achievable at the condition of current density, 5A/dm2, and in the electrolyte of Hydrochloric acid. During tin electro-refining process, impurity dissolved from tin crude metal into the electrolyte was analyzed using Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), and the result showed the concentration of impurity metal gradually increased. Quantitative analysis on casted tin crude metal showed that it consists of tin with 93.9 wt.% and several impurity metals of Ag, Bi, Pb, Cu, and etc. After tin electro-refining process, the purity of tin increased up to 99.985 wt.%.
    Źródło:
    Archives of Metallurgy and Materials; 2015, 60, 2B; 1217-1220
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Theoretical Foundations and Technological Capabilities of Hydrocarbonyl Process while Recovering Copper from Technogenic Wastes
    Autorzy:
    Fedoseev, I. V.
    Barkan, M. S.
    Kornev, A. B.
    Danilov, A. S.
    Powiązania:
    https://bibliotekanauki.pl/articles/123296.pdf
    Data publikacji:
    2018
    Wydawca:
    Polskie Towarzystwo Inżynierii Ekologicznej
    Tematy:
    polymetallic sulphide ores
    high purity copper
    hydrocarbonyl process
    reduction ratio
    producer gas
    Opis:
    Secondary processing of waste from metallurgical and other industries becomes an urgent issue in the face of increasing anthropogenic pressure and a shortage of sources of materials. The paper shows the results of chemical and technological studies of processes, executing in the Cu(II) – Cu(I) – Cl- – CO – H2О system. The processing technology of copper-bearing intermediate products multicomponent leaching solutions, permitting high purity copper production at the least economic cost, is proposed.
    Źródło:
    Journal of Ecological Engineering; 2018, 19, 5; 33-37
    2299-8993
    Pojawia się w:
    Journal of Ecological Engineering
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Mechanical strength and fracture toughness of brittle monocrystalline and ceramic materials
    Wytrzymałość mechaniczna i odporność na pękanie kruchych materiałów monokrystalicznych i ceramicznych
    Autorzy:
    Boniecki, M.
    Kamiński, P.
    Wesołowski, W.
    Krzyżak, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/192433.pdf
    Data publikacji:
    2016
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Technologii Materiałów Elektronicznych
    Tematy:
    Y2O3 ceramics
    high-purity silicon
    fracture toughness
    bending strength
    ceramika Y2O3
    krzem
    odporność na pękanie
    wytrzymałość na zginanie
    Opis:
    The article compares the mechanical properties of a n-type silicon single crystal with an orientation <100> and resistivity ~ 2000 Ωcm, obtained by the floating zone (FZ) method, with the mechanical properties of Y2O3 ceramics. Both materials are characterized by a high value of transmission coefficient of electromagnetic radiation in the wavelength range from 2 μm to 8 μm and they can be used as optical windows in a near infrared range. However, the choice of a material type for the specific applications may depend on their mechanical properties. these properties have been determined both at room temperature and at elevated temperature, i.e. 700°C for si and 800°C for Y2O3 ceramics. We have found that at room temperature the fracture toughness of the Si single crystal KIc = 1.3 ± 0.1 MPam1/2 and the four-point bending strength σc = 289 ± 61 MPa. For Y2O3 ceramics these parameters are 1.8 ± 0.2 MPam1/2 and 184 ± 20 MPa, respectively. At 700°C the mechanical parameters for the Si single crystal are: KIc = 20 ± 3 MPam1/2 and σc = 592 ± 86 MPa. for Y2O3 ceramics at 800°C, KIc = 1.7 ± 0.1 MPam1/2 and σc = 230 ± 23 MPa. The presented data show that at elevated temperatures both fracture toughness and bending strength of the Si single crystal are significantly greater than the values of those parameters found for Y2O3 ceramics.
    W artykule porównano właściwości mechaniczne monokrystalicznego krzemu typu n o orientacji <100> i rezystywności ~ 2000 Ωcm, otrzymanego metodą beztyglową, z właściwościami mechanicznymi ceramiki Y2O3. Oba materiały charakteryzują się dużym współczynnikiem transmisji promieniowania elektromagnetycznego w zakresie długości fali od 2 μm do 8 μm i mogą być stosowane jako okna optyczne w zakresie bliskiej podczerwieni. Wybór rodzaju materiału dla konkretnych zastosowań może być jednak uzależniony od ich właściwości mechanicznych. Właściwości te określano zarówno w temperaturze pokojowej, jak i w temperaturze podwyższonej do 700°C w przypadku Si oraz do 800°C w przypadku ceramiki Y2O3. Stwierdzono, że dla Si w temperaturze pokojowej odporność na pękanie KIc = 1,3 ± 0,1 MPam1/2,a wytrzymałość na zginanie czteropunktowe σc = 289 ± 61 MPa. Dla Y2O3 parametry KIc i σc przyjmują wartości wynoszące w tej temperaturze odpowiednio 1,8 ± 0,2 MPam1/2 i 184 ± 20 MPa. W temperaturze 700°C wartości parametrów KIc i σc dla Si są równe odpowiednio 20 ± 3 MPam1/2 oraz 592 ± 86 MPa, zaś dla ceramiki Y2O3 w 800°C KIc = 1,7 ± 0,1MPam1/2 i σc = 230 ± 23 MPa. Prezentowane dane wskazują, że w temperaturze pokojowej wytrzymałość na zginanie czteropunktowe monokrystalicznego Si jest znacząco większa niż ceramiki Y2O3. W podwyższonych temperaturach zarówno odporność na pękanie, jak i wytrzymałość na zginanie monokrystalicznego Si jest wielokrotnie większa niż w przypadku ceramiki Y2O3.
    Źródło:
    Materiały Elektroniczne; 2016, T. 44, nr 4, 4; 8-16
    0209-0058
    Pojawia się w:
    Materiały Elektroniczne
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-8 z 8

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