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Tytuł:
Current Trends in the Development of FTIR Imaging for the Quantitative Analysis of Biological Samples
Autorzy:
Petibois, C.
Wehbe, K.
Belbachir, K.
Noreen, R.
Déléris, G.
Powiązania:
https://bibliotekanauki.pl/articles/1808575.pdf
Data publikacji:
2009-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
82.80.-d
Opis:
Fourier transform infrared imaging instrumentation has come of age for the rapid acquisition of biosample IR images, and thus now allows developing analytical methods based upon the molecular information of samples contents. For the biomedicine field, Fourier transform infrared imaging should be able to play a role in the molecular characterization of cells and tissues where no other analytical method provides quantitative information. Now, a compromise may be obtained between an acceptable acquisition time of IR images, which should never exceed a few tens of minutes, and the necessary spatial resolution (down to the diffraction limit, although limited for biology), spectral resolution (2 to 8 $cm^{-1}$ for biosample analyses), and signal-to-noise ratio level, to provide a diagnostic answer to clinicians during the surgery time. Here, we will discuss the potential of Fourier transform infrared imaging in face to major pathologies (myopathies, brain tumors, metabolic diseases) for which current imaging methods remain unable to provide sufficient information for a precise diagnosis. Quantitative molecular information may be extracted from infrared images of samples as soon as samples volume/thickness is controlled as well as absorption and absorptivity of the molecules to analyze may be isolated from other absorbing compounds. In this context, metabolic parameters appear as the main targets for providing critical information about the physiological status of a biosample due to their characteristic infrared spectra. As examples, it will be shown how to isolate and quantify glucose, lactic-acid, urea, etc. absorptions from complex biosample infrared images.
Źródło:
Acta Physica Polonica A; 2009, 115, 2; 507-512
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Chemical Effects on the K$\text{}_{β}$/K$\text{}_{α}$ Intensity Ratios in First-Row Transition Element Compounds
Autorzy:
Küçükönder, A.
Büyükkasap, E.
Yilmaz, R.
Şahin, Y.
Powiązania:
https://bibliotekanauki.pl/articles/1994736.pdf
Data publikacji:
1999-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.-g
82.80.-d
Opis:
Chemical Effects on the K$\text{}_{β}$/K$\text{}_{α}$ X-ray Intensity Ratios for Some First-row Transition Element Compounds Were Studied Experimentally and Calculated. the Vacancies in the K Shell Were Created by 59.5 keV γ rays from an $\text{}^{241}$Am Radioactive Source and Characteristic X-ray Radiation from Sample Was Measured by Using Si(li) and Ge(li) Detectors. the Calculations Were Carried Out Using Brunner's Model. the Calculated Relative K$\text{}_{β}$/K$\text{}_{α}$ X-ray Intensity Ratios Are in Good Agreement with the Present and the Previously Published Experimental Data.
Źródło:
Acta Physica Polonica A; 1999, 95, 2; 243-250
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Zone-Plate Based Nanospectroscopy with Soft X-Rays at the SLS
Autorzy:
Fink, R.
Hub, C.
Tzvetkov, G.
Powiązania:
https://bibliotekanauki.pl/articles/1808308.pdf
Data publikacji:
2009-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
68.37.Yz
82.80.-d
82.80.Ej
07.85.Tt
Opis:
With the advance of nanostructuring techniques and the availability of third-generation synchrotron sources, Fresnel-type zone plate optics is widely used for nanospectroscopic investigations with resolutions of several 10 nm. Whereas hard X-rays commonly use diffraction or elemental contrast (e.g. using X-ray fluorescence), soft X-rays are favored to utilize the spectroscopic contrast in the near-edge region of the absorption edge. In particular, for soft materials, the relevant C-, N- and O 1s absorption edges show distinct resonances which allow fingerprint-type chemical identification, even in water surroundings. Few selected examples from modern material science will be discussed to demonstrate that the combination of X-ray absorption spectroscopy with high spatial resolution yields new insight into the nanoscale properties of these materials.
Źródło:
Acta Physica Polonica A; 2009, 115, 2; 462-466
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, Characterization of Novel Dinuclear Co(II)-Cu(II) Complexes and Investigation of Their Catecholase and Catalase-Like Activities
Autorzy:
Dede, B.
Cicek, E.
Karipcin, F.
Powiązania:
https://bibliotekanauki.pl/articles/1398819.pdf
Data publikacji:
2016-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Ka
82.80.-d
87.15.R-
Opis:
The purpose of this study is synthesis, characterization and enzyme activity functions of novel dinuclear metal complexes. Therefore two new dinuclear heterometallic cobat(II)-copper(II) complexes have been synthesized and structurally characterized by using Fourier transform infrared method, elemental analysis, inductively coupled plasma optical emission spectrometry, molar conductivity, magnetic moment measurements and thermal analysis. Spectroscopic and stoichiometric data of the metal complexes indicated that the metal:ligand ratio of the complexes were found to be 2:1. Both of the complexes are 1:2 electrolytes as shown by their molar conductivities and paramagnetism. The subnormal magnetic moment values of the dinuclear complexes were explained by an antiferromagnetic interaction. Additionally complexes were each tested both for their ability to oxidation reaction of 3,5-di-tert-butylcatechol to the 3,5-di-tert-butyl-o-benzoquinone presence of O₂ and catalyse the disproportionation of hydrogen peroxide in the presence of the added base imidazole. It was found that both of the complexes exhibited good catecholase and catalase-like enzyme activity.
Źródło:
Acta Physica Polonica A; 2016, 129, 2; 203-207
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Methodology for FTIR Imaging of Individual Cells
Autorzy:
Yao, Seydou
Cestelli Guidi, M.
Delugin, M.
Della-Ventura, G.
Marcelli, A.
Petibois, C.
Powiązania:
https://bibliotekanauki.pl/articles/1398831.pdf
Data publikacji:
2016-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
82.80.-d
87.85.Pq
87.64.-t
Opis:
FTIR imaging is a novel spectroscopic technique able to provide cell imaging, in vivo and in real-time. However, one key issue is developing methodologies for cell culture on IR-transparent substrates fitting cell biology requirements. In this work we tested different IR-transparent substrates in terms of biotoxicity, surface properties, and spectral image acquisition qualities. Only a few substrates, namely Si₃N₄, Ge, GLS, LaF₃, Si, SrF₂, ZnS/C, ZnS/F, were found to provide cell culture conditions comparable to those observed on usual polycarbonate Petri dishes, the main limiting parameter being the toxicity of the material (ZnS, GLS, PbF₂, PbCl₂) or a poor adhesiveness (notably diamond, AgCl, CaF₂, ZnS). From substrates eligible for a good-quality cell culture, the spectral acquisition quality is mainly affected by the refractive index value. Finally, the best compromise between cell culture quality and image spectral quality could be obtained using Si and Ge substrates. This rationalization of the available IR-transparent substrates for bioimaging is particularly relevant for live cell analyses, where cell culture conditions must remain unaffected by substrate properties.
Źródło:
Acta Physica Polonica A; 2016, 129, 2; 250-254
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Effect of Argon Plasma on the Float Glass Surface
Autorzy:
Tuleta, M.
Powiązania:
https://bibliotekanauki.pl/articles/1503946.pdf
Data publikacji:
2011-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Kf
52.77.-j
82.80.-d
Opis:
Both surfaces of a commercial float glass were treated simultaneously by a low-temperature argon plasma generated by an inductively coupled rf power supply. The effect of plasma processing on the outer surface composition of both sides of the glass was analysed by means of the ion scattering spectroscopy technique. The observed recomposition of the outer surface atoms was interpreted as a result of the action of the thermal and electric fields created by the plasma on particular glass constituents.
Źródło:
Acta Physica Polonica A; 2011, 120, 1; 91-93
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Application of HPLC-MS with Electrospray Ionization for the Qualitative and Quantitative Analysis of Antibiotics in Pharmaceutical Formulation
Autorzy:
Likhtarovich, A.
Luhin, V.
Sovastei, O.
Zukowski, P.
Dado, M.
Powiązania:
https://bibliotekanauki.pl/articles/1402227.pdf
Data publikacji:
2015-11
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
32.10.Bi
33.15.Ta
82.80.-d
Opis:
This study describes the application of electrospray ionization mass spectrometry in order to identify ten antibiotics (macrolides, penicillins, aminoglycosides). An optimum procedure was developed for determination of antibiotics of different grade. Positive ion spectra of most antibiotics are higher in intensity including an [M+H]⁺ ion and produce less fragmentation and are more informative compared to the negative ion spectra. The group of antibiotics exhibits the same characteristic fragmentation. The data base was developed for identification of antibiotics comparing of their molecular and fragment ions. The results of the study showed that the method with electrospray ionization is simple and quick which is useful in the routine determination of antibiotics and in their pharmaceutical dosage forms.
Źródło:
Acta Physica Polonica A; 2015, 128, 5; 901-904
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Identification and Fragmentation of Cefalosporins, Lincosamides, Levofloxacin, Doxycycline, Vancomycin by ESI-MS
Autorzy:
Sapon, A.
Luhin, V.
Sovastei, O.
Spanik, P.
Bondariev, V.
Powiązania:
https://bibliotekanauki.pl/articles/1030206.pdf
Data publikacji:
2017-08
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
32.10.Bi
33.15.Ta
82.80.-d
Opis:
The aim of the paper is the identification of the most frequently used antibiotics such as cefazolin, cefuroxime, cefotaxime, ceftriaxone, ceftazidime, lyncomycin, clindamycin, levofloxacin, doxycycline and vancomycin by electrospray ionization mass spectrometry interface in positive and negative modes. The fragmentation pathways of the group of antibiotics were colligated on the basis of the obtained ESI mass spectra. Generally, the positive ion spectra of antibiotics are higher in intensity including an [M+H]⁺ ion and producing less fragmentation as well as more informative compared to the negative ion spectra. Only ESI of levofloxacin in positive and negative modes with the chosen tune parameters leads to degradation of molecular ion, so the parent ion does not appear in the mass spectra. The group of antibiotics (cephalosporins and lincosamides) shows the same characteristic fragmentation. These setup parameters were successfully applied for the routine determination of antibiotics in their pharmaceutical dosage forms and other objects. Data base was developed for identification of antibiotics by comparison of their molecular and fragment ions.
Źródło:
Acta Physica Polonica A; 2017, 132, 2; 236-239
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Novel metal(II) complexes with bidentate Schiff base ligand: Synthesis, spectroscopic properties and dye decolorization functions
Autorzy:
Karakaya, C.
Dede, B.
Cicek, E.
Powiązania:
https://bibliotekanauki.pl/articles/1065151.pdf
Data publikacji:
2016-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Ka
82.80.-d
89.60.-k
Opis:
The bidentate Schiff base ligand 4-chloro-2-[1-(4-phenylphenyl)ethylideneamino]phenol and its mononuclear Co(II), Ni(II), Cu(II) and Zn(II) complexes have been synthesized. Ligand and metal complexes were characterized by elemental analyses, magnetic susceptibility, molar conductivity, ¹H- and ¹³C-NMR, the Fourier transform infrared, UV-Vis, inductively coupled plasma optical emission spectrometry, and thermogravimetric-differential thermogravimetric studies. The results suggest that the mononuclear complexes have a metal to ligand mole ratio of 1:2 and the metal(II) ions are coordinated with the phenolic oxygen and imine nitrogen atoms. Octahedral structures are proposed for the complexes of the Schiff base ligand. Furthermore, the complexes were checked for their efficiency to decolorize the dye methylene blue. In our experiments we found that metal(II) complexes had an acceptable decolorization efficiency against the dye methylene blue.
Źródło:
Acta Physica Polonica A; 2016, 129, 2; 208-212
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Surface Properties of Me/Si Structures Prepared by Means of Self-Ion Assisted Deposition
Autorzy:
Tashlykov, I.
Żukowski, P.
Mikhalkovich, O.
Baraishuk, S.
Powiązania:
https://bibliotekanauki.pl/articles/1198974.pdf
Data publikacji:
2014-06
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.72.uf
82.80.-d
62.20.Qp
Opis:
In this paper a composite structure, topography, wettability and nanohardness of a (100) Si surface modified by means of ion-assisted deposition of metal (Me) coatings in conditions of a self-irradiation are discussed.
Źródło:
Acta Physica Polonica A; 2014, 125, 6; 1306-1308
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Investigation of Sediments Causing Damage to Water Meters in a Large Drinking Water Distribution System
Autorzy:
Kopeć, M.
Roman, M.
Kąc, M.
Budziak, A.
Paluszkiewicz, C.
Zarzycki, A.
Kąc, S.
Dutkiewicz, E.
Cichoń, T.
Bochnia, T.
Kwiatek, W.
Powiązania:
https://bibliotekanauki.pl/articles/1030652.pdf
Data publikacji:
2018-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
89.60.-k
78.70.En
61.05.cp
82.80.-d
82.80.Gk
Opis:
Preliminary studies on the sediments collected from water meters of Krakow water supply system were performed in the cooperation with the Municipal Water Supply and Sewage. Creation and deposition of sediments on the measuring devices installed in the water supply system is a serious technological and economical problem for water companies, defectively operating for this reason water meters must be replaced. It is evident that knowledge of the chemical and phase composition of sediments is an important step towards resolving the problem of impurities in water supply systems. Four different samples of sediments, coming from water meters, were investigated using the proton-induced X-ray emission, the X-ray diffraction, the Fourier transform infrared and Raman spectroscopy. The X-ray methods revealed presence of amorphous and fine-crystalline phases as well as high content of iron-based compounds. As a crystalline phase, the most frequently appeared: goethite, lepidocrocite, iron oxides (hematite, maghemite, magnetite), calcium carbonate, and quartz. In one of the samples, the nanocrystalline phase was found and identified as hydrous iron oxyhydroxide ferrihydrite. Vibrational spectroscopy methods confirmed the composition of crystalline phases as well as enabled to estimate the abundance of amorphous phase in samples.
Źródło:
Acta Physica Polonica A; 2018, 133, 2; 296-301
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Anion Removal Potential of Complex Metal Oxides Estimated from Their Atomic Scale Structural Properties
Autorzy:
Chubar, N.
Gerda, V.
Mičušík, M.
Omastova, M.
Heister, K.
Man, P.
Yablokova, G.
Banerjee, D.
Fraissard, J.
Powiązania:
https://bibliotekanauki.pl/articles/1030882.pdf
Data publikacji:
2018-04
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.05.Je
81.05.Rm
68.43.-h
82.80.-d
Opis:
The main common idea of two conference papers delivered at OMEE-2017 was to demonstrate an importance of the speciation level knowledge in modern adsorption materials science. In order to prove this, two groups of adsorptive materials were used: three samples of Mg-Al-CO₃ layered double hydroxides produced by different synthesis methods and ten samples of Fe-Ce oxide-based composites with various ratios of Fe-to-Ce. In both cases of studies, it was not possible to find direct correlation between adsorptive performances of the materials and their structural properties obtained by conventional characterisation techniques. However, anion adsorptive removals of each group of inorganic composites correlated with their structural properties studied on the level of speciation. It was shown that strong anion removal potential of Mg-Al-CO₃ layered double hydroxides was associated with richness in speciation of chemical elements (Mg, Al) and interlayer anions (CO₃²¯) as well as with generous hydration. Adsorptive performances of inorganic anion exchangers based on Fe-Ce hydrous oxides were explained by simulation extended X-ray absorption fine structures simulation. The best anion removers were found to be those Fe/Ce oxide-based composites whose Fe outer shells were formed from backscattering oscillations from both O and Fe atoms.
Źródło:
Acta Physica Polonica A; 2018, 133, 4; 1091-1096
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Defect Transformations in Ion Bombarded InGaAsP
Autorzy:
Ratajczak, R.
Turos, A.
Stonert, A.
Nowicki, L.
Strupiński, W.
Powiązania:
https://bibliotekanauki.pl/articles/1504046.pdf
Data publikacji:
2011-07
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.-j
61.72.-y
81.05.-t
82.80.-d
85.40.-e
Opis:
Damage buildup and defect transformations at temperatures ranging from 15 K to 300 K in ion bombarded InGaAsP epitaxial layers on InP were studied by in situ Rutherford backscattering/channeling measurements using 1.4 MeV $\text{}^4He$ ions. Ion bombardment was performed using 150 keV N ions and 580 keV As ions to fluences ranging from 5 × $10^{12}$ to 6 × $10^{14}$ at./$cm^2$. Damage distributions were determined using the McChasy Monte Carlo simulation code assuming that they consist of randomly displaced lattice atoms and extended defects producing bending of atomic planes. Steep damage buildup up to amorphisation with increasing ion fluence was observed. Defect production rate increases with the ion mass and decreases with the implantation temperature. Parameters of damage buildup were evaluated in the frame of the multi-step damage accumulation model. Following ion bombardment at 15 K defect transformations upon warming up to 300 K have also been studied. Defect migration beginning above 100 K was revealed leading to a broad defect recovery stage with the activation energy of 0.1 eV for randomly displaced atoms and 0.15 eV for bent channels defects.
Źródło:
Acta Physica Polonica A; 2011, 120, 1; 136-139
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Parallel Mappings as a Key for Understanding the Bioinorganic Materials
Autorzy:
Kuczumow, A.
Nowak, J.
Chałas, R.
Powiązania:
https://bibliotekanauki.pl/articles/1808388.pdf
Data publikacji:
2009-02
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.En
87.64.Bx
87.64.Dz
87.59.-e
82.80.-d
Opis:
Important bioinorganic objects, both living and fossilized are as a rule characterized by a complex microscopic structure. For biological samples, the cell-like and laminar as well as growth ring structures are among most significant. Moreover, these objects belong to a now widely studied category of biominerals with composite, inorganic-organic structure. Such materials are composed of a limited number of inorganic compounds and several natural organic polymers. This apparently simple composition leads to an abnormal variety of constructions significant from the medical (repairs and implants), natural (ecological effectiveness) and material science (biomimetic synthesis) point of view. The analysis of an image obtained in an optical microscope, optionally in a scanning electron microscope is a topographical reference for further investigations. For the characterization of the distribution of chemical elements and compounds in a material, techniques such as X-ray, electron- or proton microprobes are applied. Essentially, elemental mappings are collected in this stage. The need for the application of an X-ray diffraction microprobe is obvious and our experience indicates on the necessity of using the synchrotron-based devices due to their better spatial resolution and good X-ray intensity. To examine the presence of the organic compounds, the Raman microprobe measurements are good options. They deliver information about the spatial distribution of functional groups and oscillating fragments of molecules. For the comprehensive investigation of bioinorganic material structural and chemical features, we propose the following sequence of methods: optical imaging, elemental mapping, crystallographic mapping, organic mapping and micromechanical mapping. The examples of such an approach are given for: petrified wood, human teeth, and an ammonite shell.
Źródło:
Acta Physica Polonica A; 2009, 115, 2; 482-488
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Formability Evaluation of Aluminium Alloys by FLD Diagrams
Autorzy:
Petroušek, P.
Kočiško, R.
Kvačkaj, T.
Bidulský, R.
Bidulská, J.
Fedoriková, A.
Sabol, P.
Powiązania:
https://bibliotekanauki.pl/articles/1032922.pdf
Data publikacji:
2017-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Hy
62.10.+s
62.20.M-
81.05.-t
82.80.-d
Opis:
The goal of the present work is evaluated mechanical properties and forming limit diagrams of ambient rolled aluminium alloy based on AlMgSi. Forming limit diagrams are convenient and often used as a tool for the classification of the formability and the evaluation of the forming process of sheet materials. Forming limits of sheet metal are represented in the forming limit diagrams occurring by various deformation states. The most widely used type is the Keeler-Goodwin diagram. Input data got from static tensile test are important for formability evaluating of the thin sheet by mathematical simulations, such as tensile strength, yield strength, elongation, and the strain hardening exponent. The result is a consideration of the suitability of the material for stamping technology.
Źródło:
Acta Physica Polonica A; 2017, 131, 5; 1344-1346
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
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