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Tytuł:
Trihalogenonitropropeny w reakcjach [4+2]-π-elektronowych cykloaddycji
Trihalonitropropenes in [4+2]-π-electron cycloaddition reactions
Autorzy:
Szczepanek, A.
Mróz, K.
Goliasz, G.
Jasiński, R.
Powiązania:
https://bibliotekanauki.pl/articles/1219978.pdf
Data publikacji:
2011
Wydawca:
Stowarzyszenie Inżynierów i Techników Przemysłu Chemicznego. Zakład Wydawniczy CHEMPRESS-SITPChem
Tematy:
[3+2] cykloaddycja
[4+2] cykloaddycja
nitroalkeny
[3+2] cycloaddition
[4+2] cycloaddition
nitroalkenes
Opis:
W pracy przeprowadzono krytyczną analizę danych literaturowych dotyczących reakcji [3+2] i [4+2] cykloaddycji z udziałem trihalogenonitropropenów.
The work is a critical review of available literature data concerning the reaction of [3+2] and [4+2] cycloaddition reactions of trihalonitropropenes.
Źródło:
Chemik; 2011, 65, 10; 1049-1054
0009-2886
Pojawia się w:
Chemik
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Technological aspects of the synthesis of 2,4-dichlorophenol
Autorzy:
Białek, A.
Moszczyński, W.
Powiązania:
https://bibliotekanauki.pl/articles/779182.pdf
Data publikacji:
2009
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
2,4-dichlorofenol
chlorowanie
katalizator
dioksyny
kwas 2,4-dichlorofenoksyoctowy
2,4-dichlorophenol
chlorination
catalyst
dioxine
2,4-dichlorophenoxyacetic acid
Opis:
The main factors influencing the selectivity of chlorophenols synthesis were described. The loss of raw materials and the composition of wastes obtained in a conventional technology of 2,4-D production based on 2,4-dichlorophenol (2,4-DCP) of the 89% purity were presented. The influence of some homogenous catalysts on the selectivity of 2,4-dichlorophenol obtained in phenol and chlorine reaction was examined. Using the combined catalyst enables to chlorinate selectively the monochlorophenols to 2,4-DCP without an undesirable increasing of the 2,6-dichlorophenol and 2,4,6-trichlorophenol contents. The catalyst transformations during the reaction of phenol chlorination were investigated and the method of its elimination after the reaction was elaborated.
Źródło:
Polish Journal of Chemical Technology; 2009, 11, 2; 21-30
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Modified Subformula Property for the Modal Logic S4.2
Autorzy:
Takano, Mitio
Powiązania:
https://bibliotekanauki.pl/articles/749870.pdf
Data publikacji:
2019
Wydawca:
Uniwersytet Łódzki. Wydawnictwo Uniwersytetu Łódzkiego
Tematy:
modal logic S4.2
sequent calculus
subformula property
Opis:
The modal logic S4.2 is S4 with the additional axiom ◊□A ⊃ □◊A. In this article, the sequent calculus GS4.2 for this logic is presented, and by imposing an appropriate restriction on the application of the cut-rule, it is shown that, every GS4.2-provable sequent S has a GS4.2-proof such that every formula occurring in it is either a subformula of some formula in S, or the formula □¬□B or ¬□B, where □B occurs in the scope of some occurrence of □ in some formula of S. These are just the K5-subformulas of some formula in S which were introduced by us to show the modied subformula property for the modal logics K5 and K5D (Bull Sect Logic 30(2): 115–122, 2001). Some corollaries including the interpolation property for S4.2 follow from this. By slightly modifying the proof, the finite model property also follows.
Źródło:
Bulletin of the Section of Logic; 2019, 48, 1
0138-0680
2449-836X
Pojawia się w:
Bulletin of the Section of Logic
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Architectural innovations influenced by climatic phenomena (4.2 ka event) in the late old kingdom (saqqara, egypt)
Autorzy:
Kuraszkiewicz, Kamil O.
Powiązania:
https://bibliotekanauki.pl/articles/2025727.pdf
Data publikacji:
2016
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
Saqqara
architecture
4.2 ka BP climate event
heavy rainfalls
Opis:
The work of the Polish-Egyptian Archaeological Mission at Saqqara revealed a cemetery of palace officials that was in use during the late Old Kingdom. The evidence found during the exploration of the tombs indicates that the tomb builders were aware of the problems resulting from torrential rains in last years of functioning of the cemetery and that architectural solutions have been invented against these problems. The discussed phenomena seem to be directly related to the 4.2 ka event.
Źródło:
Studia Quaternaria; 2016, 33; 27-34
1641-5558
2300-0384
Pojawia się w:
Studia Quaternaria
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ornamental swiss chard (Beta vulgaris var. cicla) response to daminozide and flurprimidol
Autorzy:
Zawadzińska, Agnieszka
Salachna, Piotr
Piechocki, Rafał
Powiązania:
https://bibliotekanauki.pl/articles/1178715.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
2-dimethylhydrazinyl)-4-oxobutanoic acid
2-methyl-1-pyrimidin-5-yl-1-[4-(trifluoromethoxy)phenyl]propan-1-ol
4-(2
chard
drenching
spraying
Opis:
The ornamental swiss chard (Beta vulgaris var. cicla) has the potential to produce ornamental potted plants becaused of the highly decorative foliage, characterized by intens color of leaves with large, ribbed blades and wide, grooved stalks arranged in a rosette. Depending on the cultivar, swiss chard may grow up to 60 cm in height. However to obtain compacts and attractive plants it is necessary to use plant growth regulation (PGRs). The aim of the study was to identify the most effective regulator and the method of its application to reduce the size and improve the habit of ornamental swiss chard grown in pots. In two years experiments two growth retardants were used, i.e. daminozide at 4250 mg•dm-3 and flurprimidol at 15 mg•dm-3. The retardants were applied four times at an interval of 10 days by spraying the plants with 20-25 ml of the solution on plants or drenching them with 150 ml of the solution per pot. Control plants were not treated with the retardants. Both the habit and proportions of potted swiss chard may be effectively controlled by drenching it four times with flurpirimidol at a dose of 2.25 mg/pot. Daminozide was not effective in controlling swiss chard habit, irrespective of the application method. Non negative effects or phytotoxicities were found in any drench or spray treatments of daminozide and flurprimidol.
Źródło:
World Scientific News; 2017, 61, 2; 86-97
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Estimations of the magnitude of the fourth-order electrooptic effect in KDP-type crystals
Próba wyznaczenia wielkości elektrooptycznego efektu czwartego rzędu w kryształach grupy KDP
Autorzy:
Ledzion, R.
Izdebski, M.
Górski, P.
Kucharczyk, W.
Powiązania:
https://bibliotekanauki.pl/articles/296609.pdf
Data publikacji:
2013
Wydawca:
Politechnika Łódzka. Wydawnictwo Politechniki Łódzkiej
Tematy:
fourth-order electrooptic effect
KH2PO4
NH4H2PO4
efekt elektrooptyczny czwartego rzędu
Opis:
An attempt to measure the fourth-order electrooptic effect in KH2PO4 (KDP) and NH4H2PO4 (ADP) is presented. Contrary to previously reported results of the order of magnitude 10-30 m4V-4, the fourth-order coefficient |g111111 - g221111| is found to be lower than 5 · 10-33 m4V-4 and 1 · 10-34 m4V-4, respectively. In addition, the effect of imperfect crystal cutting and alignment is investigated by means of calculations based on Jones calculus. It is found that even small inaccuracies may lead to an apparent fourth-order electrooptic effect comparable in magnitude to the previously reported values.
Wykorzystując dynamiczną metodę polaryzacyjno-optyczną przeprowadzono próbę pomiaru elektrooptycznego efektu czwartego rzędu w kryształach KH2PO4 (KDP) oraz NH4H2PO4 (ADP). W przeciwieństwie do zmierzonych wcześniej przy wykorzystaniu metody statycznej i prezentowanych w literaturze wielkości współczynnika |g111111 - g221111| rzędu 10-30 m4V-4 , otrzymane w pracy wyniki pozwalają stwierdzić, że współczynnik ten, odpowiednio dla kryształów KDP i ADP, jest mniejszy niż 5 · 10-33 m4v-4 oraz 1 · 10-34 m4V-4. Analizując przyczyny rozbieżności otrzymanych wyników i tych otrzymanych wcześniej, rozważono wpływ błędów w wycięciu i orientacji wykorzystanych próbek krystalicznych na wynik pomiarów. Wykorzystując rachunek Jonesa pokazano, że takie niedokładności mogą prowadzić do znaczących nieliniowości w odpowiedzi układu pomiarowego, sugerując istnienie pozornego efektu czwartego rzędu, który może być nawet o kilka rzędów wielkości większy niż efekt prawdziwy.
Źródło:
Scientific Bulletin. Physics / Technical University of Łódź; 2013, 34; 43-48
1505-1013
2449-982X
Pojawia się w:
Scientific Bulletin. Physics / Technical University of Łódź
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Nanocomposites graphene/CoFe2O4 and graphene/NiFe2O4 – preparation and characterization
Autorzy:
Jędrzejewska, A.
Sibera, D.
Pełech, R.
Jedrzejewski, R.
Narkiewicz, U.
Powiązania:
https://bibliotekanauki.pl/articles/352113.pdf
Data publikacji:
2019
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
graphene
nanocomposites
CoFe2O4
NiFe2O4
Opis:
A series of nanocomposite graphene/CoFe2 O4 and graphene/NiFe2 O4 hybrid materials was synthesized via facile, one-pot solvothermal route. The materials were obtained using two pressure methods: synthesis in the autoclave and synthesis in the microwave solvothermal reactor. The use of a microwave reactor enabled to significantly shorten the synthesis time up to 15 min. All the syntheses were carried out in a solution of ethanol. The effect of processing conditions and composite composition on the physicochemical properties and electric conductivity was studied. The specific surface area, density, morphology, phase composition, thermal properties and electric conductivity of the obtained composites were investigated. The results of studies of composites obtained in an autoclave and in a microwave reactor were compared.
Źródło:
Archives of Metallurgy and Materials; 2019, 64, 1; 103-112
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
High-Performance Ternary (4:2) Compressor Based on Capacitive Threshold Logic
Autorzy:
Mirzaee, R. F.
Reza, A.
Powiązania:
https://bibliotekanauki.pl/articles/225977.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
4:2 compressor
ternary logic
multiple-valued logic
CNFET
threshold logic
Opis:
This paper presents a ternary (4:2) compressor, which is an important component in multiplication. However, the structure differs from the binary counterpart since the ternary model does not require carry signals. The method of capacitive threshold logic (CTL) is used to achieve the output signals directly. Unlike the previously presented similar structure, the entire capacitor network is divided into two parts. This segregation results in higher reliability and robustness against unwanted process, voltage, and temperature (PVT) variations. Simulations are performed by HSPICE and 32nm CNFET technology. Simulation results demonstrate about 94% higher performance in terms of power-delay product (PDP) for the new design over the previous one.
Źródło:
International Journal of Electronics and Telecommunications; 2017, 63, 4; 355-361
2300-1933
Pojawia się w:
International Journal of Electronics and Telecommunications
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Induction of CMV-1 promoter by 4-hydroxy-2-nonenal in human embryonic kidney cells
Autorzy:
Jaganjac, Morana
Matijevic, Tanja
Cindric, Marina
Cipak, Ana
Mrakovcic, Lidija
Gubisch, Wolfgang
Zarkovic, Neven
Powiązania:
https://bibliotekanauki.pl/articles/1040401.pdf
Data publikacji:
2010
Wydawca:
Polskie Towarzystwo Biochemiczne
Tematy:
cytomegalovirus
4-hydroxy-2-nonenal
oxidative stress
Opis:
Oxidative stress, i.e., excessive production of oxygen free radicals and reactive oxygen species, leads to lipid peroxidation and to formation of reactive aldehydes which act as second messengers of free radicals. It has previously been shown that oxidative stress may be involved in the transcriptional regulation of cytomegalovirus (CMV) immediate early promoter, involved in viral reactivation from latency. In the current study we used a plasmid containing the yellow fluorescent protein (YFP) gene under the control of CMV-1 promoter to monitor the influence of hydrogen peroxide and reactive aldehydes, 4-hydroxy-2-nonenal (HNE) and acrolein, on CMV-1 promoter activation in human embryonic kidney cells (HEK293). While acrolein was ineffective, hydrogen peroxide slightly (50 %) stimulated the CMV promoter. In contrast, HNE had a strong, up to 3-fold, enhancing effect on the CMV-1 promoter within four as well as after 24h of treatment. The most effective was the treatment with 24 µM HNE. This effect of HNE suggests that stressful conditions associated with lipid peroxidation could lead to CMV activation.
Źródło:
Acta Biochimica Polonica; 2010, 57, 2; 179-183
0001-527X
Pojawia się w:
Acta Biochimica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Design Of A Bi-Functional α-Fe2O3/Zn2SiO4:Mn2+ By Layer-By-Layer Assembly Method
Projektowanie dwufunkcyjnych proszków α-Fe2O3/Zn2SiO4:Mn2+ metodą warstwa po warstwie
Autorzy:
Yu, R.
Yun, J.
Pee, J-H.
Kim, Y.
Powiązania:
https://bibliotekanauki.pl/articles/352623.pdf
Data publikacji:
2015
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
red pigment
α-Fe2O3
Zn2SiO4:Mn2+ layer
phosphor
bi-functional
czerwony pigment
Zn2SiO4: Mn2+
fosfor
proszki dwufunkcyjne
Opis:
This work describes the design of bi-functional α-Fe2O3/Zn2SiO4:Mn2+ using a two-step coating process. We propose a combination of pigments (α-Fe2O3) and phosphor (Zn2SiO4:Mn2+ ) glaze which is assembled using a layer-by-layer method. A silica-coated α-Fe2O3 pigment was obtained by a sol-gel method and a Zn2+ precursor was then added to the silica-coated α-Fe2O3 to create a ZnO layer. Finally, the Zn2SiO4:Mn2+ layer was prepared with the addition of Mn2+ ions to serve as a phosphor precursor in the multi-coated α-Fe2O3, followed by annealing at a temperature above 1000°C. Details of the phase structure, color and optical properties of the multi-functional α-Fe2O3/Zn2SiO4:Mn2+ were characterized by transmission electron microscopy and X-ray diffraction analyses.
Źródło:
Archives of Metallurgy and Materials; 2015, 60, 2B; 1165-1167
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
4-amine-2-mercaptopyrimidine modified silica gel applied in Cd(II) and Pb(II) extraction from an aqueous medium
Autorzy:
Pereira, A.S.
Ferreira, G.
Caetano, L.
Castro, R.S.D.
dos Santos, A.
Padilha, P.M.
Castro, G.R.
Powiązania:
https://bibliotekanauki.pl/articles/778413.pdf
Data publikacji:
2010
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
4-amino-2-merkaptopirymidyna
krzemionka
ekstrakcja metali
środowisko wodne
4-amine-2-mercaptopyrimidine
silica
metal extraction
aqueous medium
Opis:
This paper discusses silica surface modification by a process involving a two-step reaction: anchoring of a silylating agent, followed by an attachment of a 4-amino-2-mercaptopyrimidine molecule. The modified material (Si-BP) was successfully characterized by the FTIR spectra, which revealed amine absorption bands, and through 13C and 29Si NMR spectra, which confirm the proposed structure of the modified silica (Si-BP). Si-BP was used to extract cadmium and lead from an aqueous medium at 298 K. The Si-BP kinetics towards metal ions was very fast, i.e., about 10 minutes, although extraction was significantly impaired at pH 3. The series of adsorption isotherms were adjusted to a modified Langmuir equation and the maximum extraction capacity was 0.193 and 0.387 mmol g-1 for Cd(II) and Pb(II), respectively. An analysis of the Ř values lead to the inference that the resulting metal ligand complex was type 1:1.
Źródło:
Polish Journal of Chemical Technology; 2010, 12, 1; 7-11
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Structural properties of Mn-substituted hercynite
Autorzy:
Jastrzębska, I.
Bodnar, W.
Witte, K.
Burkel, E.
Stoch, P.
Szczerba, J.
Powiązania:
https://bibliotekanauki.pl/articles/147826.pdf
Data publikacji:
2017
Wydawca:
Instytut Chemii i Techniki Jądrowej
Tematy:
FeAl2O4
MnAl2O4
hercynite
spinel
galaxite
Mössbauer spectroscopy
Opis:
In this work spinel series with the general formula Fe1–xMnxAl2O4 (where x = 0, 0.3, 0.5 and 0.7) were synthesized and characterized with respect to their structure and microstructure. X-ray diffractometry (XRD) was used to identify the phase composition that revealed a single phase spinel material. Rietveld refinements of the XRD patterns were carried out in order to determine the lattice and oxygen positional parameters of the spinel compounds. Mössbauer effect measurements were performed at room temperature to determine the local chemical environment of the Fe ions, their valences, and degrees of spinels inversion. It was shown that an increase in the Mn content led to a decrease in the ratio of Fe2+ to Fe3+. The results obtained from Mössbauer spectroscopy (MS) were used to establish the chemical formulas of the synthesized spinels. Finally, the microstructure that was observed using scanning electron microscopy (SEM) showed a compact microstructure with an octahedral crystal habit.
Źródło:
Nukleonika; 2017, 62, 2; 95-100
0029-5922
1508-5791
Pojawia się w:
Nukleonika
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Detonation and Decomposition Characteristics of Dichlorate(VII) μ-Tris(4-amino-1,2,4-triazole)copper(II)
Autorzy:
Cudziło, S.
Trzciński, W. A.
Paszula, J.
Nita, M.
Powiązania:
https://bibliotekanauki.pl/articles/358059.pdf
Data publikacji:
2014
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
4-amino-1,2,4-triazole
complex copper compound
primary explosive
detonation parameters
Opis:
Dichlorate(VII) μ-tris(4-amino-1,2,4-triazole)copper(II) is an explosive with a performance close to that of lead azide. However, it is quite stable and has moderate sensitivity to thermal and mechanical stimuli. In order to fully characterize it as a primary explosive, its thermal decomposition kinetics were studied and some important detonation and explosion parameters (detonation heat and velocity, acceleration ability, water shock wave overpressure, and energy) were measured and/or calculated.
Źródło:
Central European Journal of Energetic Materials; 2014, 11, 4; 539-552
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, Characterization and Biological evaluation of 6-substituted-2-(substituted-phenyl)-quinoline derivatives bearing 4-amino-1,2,4-triazole-3-thiol ring at C-4 position
Autorzy:
Vaghasiya, R. G.
Ghodasara, H. B.
Vachharajani, P. R.
Shah, V. H.
Powiązania:
https://bibliotekanauki.pl/articles/412211.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Quinoline, 4-amino-1,2,4-triazole-3-thiol
therapeutic agents
antimicrobial assai
Opis:
Quinoline derivatives represent one of the most active classes of compounds possesses wide spectrum biodynamic activities and use as potent therapeutic agents. In this research work, a synthesis, characterization and biological evaluation of 6-substituted-2-(substituted-phenyl)-quinoline derivatives bearing 4-amino-1,2,4-triazole-3-thiol ring at C-4 position is described. The synthesis of quinoline derivatives is carried out by the reaction of substituted quinoline-4-carbohydrazides with a mixture of carbon disulphide and potassium hydroxide which further react with hydrazine hydrate to give final compounds. All of these compounds were screened for their in vitro antimicrobial assay against gram (+ve), gram (-ve) bacteria and fungi activity compared with standard drugs viz., Ampicilin, Chloramphenicol, Ciprofloxacin, Norfloxacin, Griseofulvin and Nystatin at different concentrations.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 8; 30-37
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Novel side reactions accompanying activation and aminolysis of N-benzoyl-2-alkylserines.
Autorzy:
Kamiński, Zbigniew
Woszczyna, Agnieszka
Kolesińska, Beata
Redliński, Adam
Powiązania:
https://bibliotekanauki.pl/articles/1044075.pdf
Data publikacji:
2001
Wydawca:
Polskie Towarzystwo Biochemiczne
Tematy:
side-reaction
4-alkyl-2-phenyl-4,5-dihydro-1,3-oxazole-5 carboxylic acids
2-alkylserines
Opis:
2-Phenyl-4-alkyl-4-hydroxymethyl-1,3-oxazolones (2a-d) have been identified as side products accompanying activation of N-benzoyl-2-alkylserines (1a-d). Oxazolones 2a-d in the presence of amine rearrange subsequently to corresponding 4-alkyl-2-phenyl-4,5-dihydro-1,3-oxazole-5 carboxylic acids (4a-d) at a 20-68% yield.
Źródło:
Acta Biochimica Polonica; 2001, 48, 4; 1175-1178
0001-527X
Pojawia się w:
Acta Biochimica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
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