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Tytuł:
Synthesis and Characterization of 1-(1-chlorocyclopropyl)-2-(1,2,4-triazol-1-yl)ethan-1-one
Autorzy:
Ji, H.
Niu, Y.
Liu, D.
Wang, W.
Dai, C.
Powiązania:
https://bibliotekanauki.pl/articles/778677.pdf
Data publikacji:
2017
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
prothioconazole
1,2,4-triazole
N-alkylation reaction
Opis:
A simple and efficient method to prepare 1-(1-chlorocyclopropyl)-2-(1,2,4-triazol-1-yl)ethan-1-one via nucleophilic substitution of 2-chloro-1-(1-chlorocyclopropyl)ethanone and 1,2,4-triazole is described. The title compound is the key intermediate required for the synthesis of prothioconazole, a promising agricultural fungicide. By exploring changes in the reaction time, temperature, ratio of starting reagents, acid binding agent, and the nature of phase transfer catalyst, the reaction conditions could be optimized to afford the desired N-alkylated material in near-quantitative yield. The ultimate yield of the product after recrystallization was 93%, with a purity of 99% based on its characterization by Gas Chromatography-Mass Spectrometer (GC-MS), Fourier Transform infrared spectroscopy (IR), Proton Magnetic Resonance (1H NMR), and Carbon-13 Nuclear Magnetic Resonance (13C NMR). The synthetic process is suitable for industrial application, with the advantages of high yield and facile preparation under mild operating conditions.
Źródło:
Polish Journal of Chemical Technology; 2017, 19, 1; 41-47
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and biological activity of 1,2,4-triazolo-[3,4-b]thiadiazole as antimicrobial agents
Autorzy:
Vekariya, P. B.
Pandya, J. R.
Goswami, V.
Joshi, H. S.
Powiązania:
https://bibliotekanauki.pl/articles/412334.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
6-Fluoro chroman
1,2,4-triazole
triazolothiadiazole
antimicrobial activity
Opis:
Some novel 6-fluoro chroman derivatives having 1,2,4-triazolo-[3,4-b]thiadiazole were synthesized and characterized by IR, NMR and mass spectral analysis. All synthesized compounds were screened for antimicrobial activity using broth dilution method. All the compounds showed good antimicrobial activity and compound 5e showed significant antibacterial activity.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 7; 45-52
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and antimicrobal activities of some novel triazolo[1,5-a]pyrimidine derivatives
Autorzy:
Gami, S. P.
Vilapara, K. V.
Khunt, H. R.
Babariya, J. S.
Naliapara, Y. T.
Powiązania:
https://bibliotekanauki.pl/articles/412170.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
5-amino-1,2,4-triazole
ketene dithioacetal
antimicrobial activity
triazolopyrimidine
Opis:
A convenient synthesis of substituted 1,2,4-triazolo[1,5-a]pyrimidine was carried out by the reaction of various ketene dithioacetals with 5-amino 1,2,4-triazole in methanol in presence of sodium methoxide. The newly synthesized compound were characterized by 1H NMR, 13C NMR, IR, MS, elemental analysis and screened for their antimicrobial activity against various strains of bacteria and fungi.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 11, 2; 127-134
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Acetylation of methyl 5-amino-1H-[1,2,4]triazole-3-carboxylate
Autorzy:
Dżygiel, Anetta
MAsiukiewicz, Elżbieta
Rzeszotarska, Barbara
Powiązania:
https://bibliotekanauki.pl/articles/1044073.pdf
Data publikacji:
2001
Wydawca:
Polskie Towarzystwo Biochemiczne
Tematy:
hetareneamino acid
5-amino-1H-[1,2,4]triazole-3-carboxylate
Opis:
Acetylation with acetic anhydride of methyl 5-amino-1H-[1,2,4]triazole-3-carboxylate, one of the hetareneamino acids, was studied using HPLC,1H NMR, FTIR and GC-MS. The compound has a significantly decreased susceptibility to acetylation compared to 5-amino-1H-[1,2,4]triazole itself. Two isomeric diacetylated products were found.
Źródło:
Acta Biochimica Polonica; 2001, 48, 4; 1169-1173
0001-527X
Pojawia się w:
Acta Biochimica Polonica
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Detonation and Decomposition Characteristics of Dichlorate(VII) μ-Tris(4-amino-1,2,4-triazole)copper(II)
Autorzy:
Cudziło, S.
Trzciński, W. A.
Paszula, J.
Nita, M.
Powiązania:
https://bibliotekanauki.pl/articles/358059.pdf
Data publikacji:
2014
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
4-amino-1,2,4-triazole
complex copper compound
primary explosive
detonation parameters
Opis:
Dichlorate(VII) μ-tris(4-amino-1,2,4-triazole)copper(II) is an explosive with a performance close to that of lead azide. However, it is quite stable and has moderate sensitivity to thermal and mechanical stimuli. In order to fully characterize it as a primary explosive, its thermal decomposition kinetics were studied and some important detonation and explosion parameters (detonation heat and velocity, acceleration ability, water shock wave overpressure, and energy) were measured and/or calculated.
Źródło:
Central European Journal of Energetic Materials; 2014, 11, 4; 539-552
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, Characterization and Biological evaluation of 6-substituted-2-(substituted-phenyl)-quinoline derivatives bearing 4-amino-1,2,4-triazole-3-thiol ring at C-4 position
Autorzy:
Vaghasiya, R. G.
Ghodasara, H. B.
Vachharajani, P. R.
Shah, V. H.
Powiązania:
https://bibliotekanauki.pl/articles/412211.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Quinoline, 4-amino-1,2,4-triazole-3-thiol
therapeutic agents
antimicrobial assai
Opis:
Quinoline derivatives represent one of the most active classes of compounds possesses wide spectrum biodynamic activities and use as potent therapeutic agents. In this research work, a synthesis, characterization and biological evaluation of 6-substituted-2-(substituted-phenyl)-quinoline derivatives bearing 4-amino-1,2,4-triazole-3-thiol ring at C-4 position is described. The synthesis of quinoline derivatives is carried out by the reaction of substituted quinoline-4-carbohydrazides with a mixture of carbon disulphide and potassium hydroxide which further react with hydrazine hydrate to give final compounds. All of these compounds were screened for their in vitro antimicrobial assay against gram (+ve), gram (-ve) bacteria and fungi activity compared with standard drugs viz., Ampicilin, Chloramphenicol, Ciprofloxacin, Norfloxacin, Griseofulvin and Nystatin at different concentrations.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 8; 30-37
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
An efficient solid phase one port synthesis of Novel triazolo[1,5-a]pyrimidine derivatives from 4-(4-aminophenyl)morpholin-3-one and evaluation of their antimicrobial activity
Autorzy:
Prajapati, D. R.
Vilapara, K. V.
Naliapara, Y. T.
Powiązania:
https://bibliotekanauki.pl/articles/412307.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
1,2,4-triazole
4-(4-aminophenyl)morpholin-3-one
antibacterial
antifungal
biological assai
Opis:
A series of novel triazolo[1,5-a]pyrimidine derivatives was synthesized from 5-amino-1,2,4-triazole and biologically active morpholinone amine in excellent yield as promising class of antimicrobial agents. The antimicrobial activities were investigated against Escherichia coli, Staphylococcus aureus, Pseudomonas aeruginosa, Staphylococcus pyogen, Candida albicans, Aspergillusniger, Aspergillusclavatus and compared with standard drugs Ampicillin, Chloramphenicol, Norfloxacin and Griseofulvin. All the synthesized compounds were characterized by IR, 1H NMR, 13C and mass spectroscopy. The result of antimicrobial activity data revealed that compound 4f,4g and 4i were found more active against bacterial species and compound 4c, 4d, 4g, 4i and 4jwere found more active against fungal strain, while other compounds shows moderate to law activity against microbes.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 14, 1; 12-21
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Characterization of Four Energetic Transition Metal Complexes of 3,4-Diamino-1,2,4-triazole
Autorzy:
Yin, X.
Jin, X.
Xu, C.-X.
He, P.
Wang, K.
Zhang, J.-G.
Powiązania:
https://bibliotekanauki.pl/articles/358716.pdf
Data publikacji:
2016
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
3,4-diamino-1,2,4-triazole
theoretic study
crystal structure
thermal stability
sensitivity
Opis:
Four complexes with the formula of [M5(DATr)12~14(H2O)6](ClO4)10 (M = Mn (1), Co (2), Ni (3), Zn (4)) about their synthesis, structures and some energetic properties (such as sensitivities tests) have been described, where the DATr here denotes 3,4-diamino-1,2,4-triazole. These four compounds are all light metallic complexes with good thermal stability. The structures of 2-4 were determined by single-crystal X-ray diffraction, and the crystal structures mainly consist of penta-nuclear units. All the structures have a common interesting property in which DATr plays a role of bi-dentate ligand. Besides, it is observed from the crystal structure of 4 that DATr can be also act as a mono-dentate ligand. Thermodynamic studies of their decomposition properties and kinetic parameters show that the four complexes have high thermal stabilities. Furthermore, tests of their impact and friction sensitivities show that complexes (2) and (3) can be potential candidates as primary explosives to replace toxic lead azide.
Źródło:
Central European Journal of Energetic Materials; 2016, 13, 2; 301-320
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Melt-cast Energetic Matrices with 3-Nitro-1,2,4-triazole Derivatives for Composite Explosives
Autorzy:
Komarova, Marina
Vakutin, Aleksey
Kazutin, Maxim
Kozyrev, Nikolai
Sukhanov, Gennady
Powiązania:
https://bibliotekanauki.pl/articles/1063044.pdf
Data publikacji:
2020
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
melt-cast energetic matrix
3-nitro-1,2,4-triazole
TNT
composite explosives
Opis:
Safety requirements for the manufacture, use and storage of high-energy materials and explosive substances necessitate a search for new insensitive components of fusible energetic matrices (propellant matrices) in order to completely or partially replace 2,4,6-trinitrotoluene (TNT). 3-Nitro-1,2,4-triazole derivatives and their melt-casts with TNT may be proposed as such replacements. Differential scanning calorimetry was employed to characterize the thermal behaviour of 1-methyl-3-nitro-1,2,4-triazole, 1-ethoxymethyl-3-nitro-1,2,4-triazole, t-butyl-3-nitro-1,2,4-triazole and their melt-casts with TNT. This study showed that 1-methyl-3-nitro-1,2,4-triazole and its melt-casts with TNT was the best for explosive systems based on 2,4,6,8,10,12-hexanitro-1,4,6,8,10,12-hexaazaisowurtzitane (HNIW), 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane (HMX) and guanylurea dinitramide (GUDN). The present article also presents data for the mechanical sensitivity of these explosives and their calculated detonation characteristics. The composite explosive based on HMX with 1-methyl-3-nitro-1,2,4-triazole has a calculated detonation velocity the same as HMX with TNT, but the sensitivity of HMX/TNT is 1.3-1.7 times higher.
Źródło:
Central European Journal of Energetic Materials; 2020, 17, 3; 344-361
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Preparation, Structure and Kinetic Analysis of the Thermal Behavior of Some Energetic Salts of 3-Hydrazino-4-amino-1,2,4-triazole
Autorzy:
Wu, J. T.
Zhang, J. G.
Sun, M.
Yin, X.
Zhang, T. L.
Powiązania:
https://bibliotekanauki.pl/articles/358073.pdf
Data publikacji:
2013
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
synthesis
crystal structure
thermal analysis
3-hydrazino-4-amino-1,2,4-triazole
energetic salts
Opis:
As a key research objective for low melting explosives and propellants, energetic salts have received worldwide attention. 3-Hydrazino-4-amino-1,2,4triazole (HATr) is an important high-nitrogen compound (73.65% N) with good stability. This paper focuses on the energetic salts which were formed between HATr and picric acid (PA) or 2,4,6-trinitroresorcinol (TNR). Single crystals of HATr·PA and HATr·TNR·H2O were grown and their crystal structures determined at low temperature. They both belong to the monoclinic system, P21/n space group. The thermal characteristics of the two target salts were investigated using DSC and TG-DTG. In addition, the non-isothermal decomposition kinetics, heats of combustion and sensitivity have also been investigated. The detonation pressures (P) and detonation velocities (D) of the salts have been calculated using the K-J equations. The results indicated that both salts have certain potential applications as gunpowder and propellant materials.
Źródło:
Central European Journal of Energetic Materials; 2013, 10, 4; 481-493
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Oxygen-containing Tetrazole Salts of 3-Hydrazino-4-amino-1,2,4-triazole (HATr): Nitrogen-rich Ionic Materials with High Thermal Stability
Autorzy:
Wu, J.-T.
Zhang, J.-G.
Yin, X.
Li, T.
Wu, L.
Zhang, Z.-B.
Powiązania:
https://bibliotekanauki.pl/articles/358927.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
energetic salts
thermal stability
oxygen-containing tetrazoles
3-hydrazino-4-amino-1,2,4-triazole
Opis:
Energetic salts of doubly-protonated 3-hydrazino-4-amino-1,2,4-triazole (2-4), and mono-protonated 3-hydrazino-4-amino-1,2,4-triazole (5-7), have been prepared in high yields from the corresponding oxygen-containing tetrazoles by (i) reaction of free acids and neutral 3-hydrazino-4-amino-1,2,4-triazole, or (ii) metathesis reactions of 3-hydrazinium-4-amino-1H-1,2,4-triazolium di-chloride with the silver salts of the corresponding oxygen-containing tetrazoles. All of these energetic salts were fully characterized by single-crystal X-ray diffraction, FT-IR and DSC measurements. All of the structures are dominated by extensive hydrogen bonds due to amino groups, hydrazino groups and oxygen atoms in the molecules. These salts exhibit good thermal stability, especially the salt 3-hydrazinium-4-amino-1H-1,2,4-triazolium 1H,1’H-5,5’-bitetrazole-1,1’-diolate (4), which exhibits a measured onset of decomposition temperature of 237 °C. Quantum chemical calculations, carried out using the Gaussian 03 suite of programs and based on the experimental densities were used to calculate the detonation pressures and velocities of all of the salts.
Źródło:
Central European Journal of Energetic Materials; 2017, 14, 1; 217-232
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and Theoretical Studies of a New Insensitive Explosive, 2’-Methyl-3-nitro-2’H-[1,3’-bi(1,2,4-triazole)]-5,5’-diamine
Autorzy:
Luo, J.
Liu, Y.
Wang, J.
Chai, T.
Yuan, J.
Chang, S.
Yu, Y.
Jing, S.
Ma, H.
Powiązania:
https://bibliotekanauki.pl/articles/358633.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
insensitive explosive
synthesis
theoretical studies
density functional theory
new 1,2,4-triazole derivative
Opis:
A new insensitive energetic material 2’-methyl-3-nitro-2’H-[1,3’-bi(1,2,4-triazole)]-5,5’-diamine (1) was prepared by a three-step synthesis from commercially available chemicals. The energetic title compound was comprehensively characterized by various means, including FT-IR, multinuclear (1H, 13C, 14N) NMR spectroscopy, elemental analysis, HPLC and thermal analysis. The sensitivities of the synthesized material towards various external stimuli (impact, friction) were determined according to the BAM method. The optimized structure and related thermodynamic parameters were obtained at the DFT-B3LYP/6-31+G** theoretical level. The detonation properties of the material were also predicted according to the Kamlet-Jacobs formulae and the Monte-Carlo method. The results show that the density, heat of formation, detonation velocity, detonation pressure, impact sensitivity and purity were 1.83 g/cm3, 369 kJ/mol, 7.52 km/s, 25.4 GPa, 82.3 J and 97.7%, respectively. In addition, the compound was an insensitive high explosive which could meet the requirements of high energetic materials.
Źródło:
Central European Journal of Energetic Materials; 2017, 14, 2; 269-280
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Correlation analysis of substituted 2-((phenyl amino)methyl)-1,2-dihydro-5-(3-methoxyphenyl)-1-phenyl-1,2,4-triazole-3-thiones
Autorzy:
Thirunarayanan, G.
Kamalkkannan, D.
Suresh, R.
Sakthinathan, S. P.
Sundararajan, R.
Arulkumara, R.
Manikandan, R.
Vanangamudi, G.
Sathiyendiran, V.
Powiązania:
https://bibliotekanauki.pl/articles/1194047.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
1-2-4-triazole
Hammett constants
IR spectral
NMR spectral
Swain-Lupton’s parameters
correlation
multi-regression analysis
Opis:
A series of substituted 2-((phenyl amino)methyl)-1,2-dihydro-5-(3-methoxyphenyl)-1-phenyl-1,2,4-triazole-3-thione compounds were synthesized and examined their purities as per the literature. The IR spectra of νC=N, νC=S, νNH and νCOC frequencies and NMR chemical shifts (ppm) of δNH, δOCH3, δCH2, δC=N, δC=S, δOCH3 and δCH2 are also assigned. The assigned IR and both 1H NMR and 13C NMR spectral data have been correlated with Hammett substituent constants and Swain-Lupton’s parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the above spectral data has been studied.
Źródło:
World Scientific News; 2015, 12; 24-43
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Physicochemical Properties and Laser Initiation of a Copper Perchlorate Complex with 3(5)-Hydrazino-4-amino-1,2,4-triazole (HATr) as a Ligand
Autorzy:
Ilyushin, M. A.
Tselinskiy, I. V.
Smirnov, A. V.
Shugalei, I. V.
Powiązania:
https://bibliotekanauki.pl/articles/358314.pdf
Data publikacji:
2012
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
IR-laser
pulse
ignition
3(5)-hydrazino-4-amino-1,2,4-triazole (HATr) as a ligand
light-sensitive explosives
Opis:
Several metal perchlorate complexes with 3(5)-hydrazino-4-amino- 1,2,4-triazole as a ligand were investigated. It was shown that the threshold of laser initiation of the copper complex changed under the influence of additives of optically transparent polymers, detonation nanodiamonds or nanotubes.
Źródło:
Central European Journal of Energetic Materials; 2012, 9, 1; 3-16
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
A Facile Synthesis of 3,3'-Dinitro-5,5'-diamino-bi-1,2,4-triazole and a Study of Its Thermal Decomposition
Autorzy:
Ma, Q.
Lu, H.
Qu, Y.
Liao, L.
Li, J.
Fan, G.
Chen, Y.
Powiązania:
https://bibliotekanauki.pl/articles/358272.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
3,3’-dinitro-5,5’-diamino-bi-1,2,4-triazole
facile synthesis
DSC-TG
RSFTIR
TG-IR
thermolysis
Opis:
3,3’-Dinitro-5,5’-diamino-bi-1,2,4-triazole (DABNT) was synthesized by a facile method and its crystalline density was determined as 1.839 g·cm−3 at 293(2) K by X-ray diffraction. Its thermal decomposition kinetics and mechanism were studied by means of differential scanning calorimetry-thermogravimetry (DCS-TG), in situ thermolysis by rapid-scan Fourier transform infrared spectroscopy (RSFTIR) and simultaneous TG-IR technology. The results showed that the apparent activation energies obtained by the Kissinger, Ozawa and Starink methods were 122.9 kJ·mol−1, 123.2 kJ·mol−1 and 123.5 kJ·mol−1, respectively. The thermodynamic parameters of ΔS≠, ΔH≠ and ΔG≠ were −37.5 J·K−1·mol−1, 118.4 kJ·mol−1 and 138.7 kJ·mol−1, respectively. The decomposition reaction process of DABNT starts with the transformation from a primary amine to a secondary amine and then the loss of one nitro-group from the DABNT structure. Gaseous products, such as N2O and H2O, were detected from decomposition in the range of 50-300 °C. Density functional theory (DFT) calculations were further employed to illustrate the decomposition mechanism. The above-mentioned information on the synthesis and thermal behaviour is quite useful for the scale-up and evaluation of the thermal safety of DABNT.
Źródło:
Central European Journal of Energetic Materials; 2017, 14, 2; 281-295
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
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