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    Wyświetlanie 1-13 z 13
    Tytuł:
    Preparation and Complex Characterization of Magnetic Nanoparticles in Magnetic Fluid
    Autorzy:
    Kubovčíková, M.
    Antal, I.
    Kováč, J.
    Závišová, V.
    Koneracká, M.
    Kopčanský, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1201928.pdf
    Data publikacji:
    2014-07
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.75.Fk
    78.67.Bf
    36.40.Cg
    47.65.Cb
    75.50.Mm
    75.30.Cr
    Opis:
    This paper deals with the preparation and complex characterization of magnetite nanoparticles (MNPs), stabilized with sodium oleate (SO), by the routine methods such as infrared spectroscopy (FTIR), magnetic measurements, scanning electron microscopy (SEM) and dynamic light scattering (DLS). The FTIR spectra showed that SO molecules were linked to MNPs through chemical bonding. Magnetic measurements proved that the MNPs are superparamagnetic in nature. Four different methods were used to determine the size and size distribution of the MNPs: SEM, DLS, differential centrifugal sedimentation (DCS) and magnetic measurements. SEM analysis showed a relatively narrow size distribution of roughly spherical MNPs with a mean diameter of 61 nm. DLS analysis confirmed monodispersed MNPs production with hydrodynamic diameter of 75 nm. The size distribution determined by DCS was found to be 69 nm. Finally, the calculated magnetic core diameter obtained from magnetization curve was 10 nm. The obtained results demonstrate that SO coated MNPs fulfil the requirements for a useful drug delivery system.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 1; 268-269
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal Analysis of Magnetic Polymer Nanospheres for Drug Targeting
    Autorzy:
    Juríková, A.
    Csach, K.
    Miškuf, J.
    Koneracká, M.
    Závišová, V.
    Kopčanský, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1535061.pdf
    Data publikacji:
    2010-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    47.65.Cb
    65.80.-g
    47.63.mh
    Opis:
    Poly(D,L-lactic-co-glycolic) acid (PLGA) polymer nanospheres loaded with different input amounts of anticancer drug taxol were prepared by the modified nanoprecipitation method. Magnetite was incorporated into the polymer nanospheres to impart them superparamagnetic properties. Thermal properties of the drug loaded magnetic polymer nanospheres were characterized using differential scanning calorimetry and thermogravimetric analysis. The solid state solubility of taxol in PLGA nanospheres and the influence of external magnetic field on their thermal stability were estimated. The investigations have revealed that the samples of dried taxol loaded magnetic PLGA nanospheres undergo mass loss at three stages during heating.
    Źródło:
    Acta Physica Polonica A; 2010, 118, 5; 990-992
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Magnetic Properties of Encapsulated Magnetite in PLGA Nanospheres
    Autorzy:
    Koneracká, M.
    Závišová, V.
    Timko, M.
    Kopčanský, P.
    Tomašovičová, N.
    Csach, K.
    Powiązania:
    https://bibliotekanauki.pl/articles/1813943.pdf
    Data publikacji:
    2008-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    71.20.Rv
    75.50.Mm
    87.83.+a
    Opis:
    In this study, the biocompatible magnetic fluid was encapsulated in biodegradable polymer PLGA (poly D, L/lactide-co-glycolide acid) by the nanoprecipitation method. We characterized these spheres in terms of morphology, magnetite content and magnetic properties. The results showed good encapsulation with magnetite content 22wt% and magnetization 3.4 mT. The transmission electron microscopy and scanning electron microscopy images showed that magnetic particles have almost a spherical shape with approximate size 250 nm. Infrared spectroscopy and thermogravimetric analysis measurements were used to confirm incorporation of magnetic particles into the PLGA polymer.
    Źródło:
    Acta Physica Polonica A; 2008, 113, 1; 595-598
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Structural Phase Transitions in 6CB-Based Ferronematics
    Autorzy:
    Tomašovičová, N.
    Koneracká, M.
    Kopčanský, P.
    Timko, M.
    Závišová, V.
    Tomčo, L.
    Jadżyn, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1810567.pdf
    Data publikacji:
    2009-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Mm
    61.30.Gd
    61.30.Hn
    Opis:
    The structural transitions in ferronematics based on the thermotropic nematic liquid crystal 4-cyano-4'-hexylbiphenyl were studied. The ferronematic samples were prepared by doping with magnetic suspension consisting of $Fe_3O_4$ particles (10 nm in diameter) coated with oleic acid as a surfactant with different volume concentrations of magnetic particles (from $10^{-5}$ to $10^{-3}$). Freedericksz transitions were studied in combined electric and magnetic fields. The experimental results indicated soft anchoring with perpendicular initial orientation between the magnetic moment of the magnetic particles and director.
    Źródło:
    Acta Physica Polonica A; 2009, 115, 1; 336-338
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermogravimetric Study of the Decomposition of BSA-Coated Magnetic Nanoparticles
    Autorzy:
    Csach, K.
    Juríková, A.
    Miškuf, J.
    Koneracká, M.
    Závišová, V.
    Kubovčíková, M.
    Kopčanský, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1429064.pdf
    Data publikacji:
    2012-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    47.65.Cb
    65.80.-g
    Opis:
    Magnetic nanoparticles used in biomedicine have to be biocompatible, which can be achieved by the modification of the magnetic particle surface with an appropriate biocompatible substance. In the work protein bovine serum albumin (BSA) was chosen to modify the surface of magnetic nanoparticles. The BSA-coated magnetic nanoparticles with different input weight ratios of BSA to the magnetite $Fe_3O_4$ were prepared and thermally characterized using thermogravimetric and differential scanning calorimetric analysis. The adsorption of BSA on the magnetic nanoparticles in wide range of concentration was confirmed. The activation energies of the thermal decomposition of the complex system were estimated.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 5-6; 1293-1295
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal Analysis of Magnetic Nanoparticles Modified with Dextran
    Autorzy:
    Juríková, A.
    Csach, K.
    Miškuf, J.
    Koneracká, M.
    Závišová, V.
    Kubovčíková, M.
    Kopčanský, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1429065.pdf
    Data publikacji:
    2012-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    47.65.Cb
    65.80.-g
    Opis:
    In the work the thermal behaviour of the magnetic nanoparticles modified with polysaccharide dextran of different weight ratios to the magnetite $Fe_3O_4$ was investigated using thermoanalytical methods - differential scanning calorimetry and thermogravimetric analysis. The adsorption of dextran on the magnetic nanoparticles was confirmed and the influence of the dextran amount in the modified magnetic fluid on the thermal decomposition of the complex system was studied. The results showed that magnetite catalyzed the thermal decomposition of dextran, the adsorbed dextran showed lower initial decomposition temperatures in comparison with the free one.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 5-6; 1296-1298
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Magnetic Field Induced Structural Transitions in 6CHBT-Based Ferronematics
    Autorzy:
    Tomašovičová, N.
    Timko, M.
    Koneracká, M.
    Závišová, V.
    Jadżyn, J.
    Beaugnon, E.
    Chaud, X.
    Kopčanský, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1428990.pdf
    Data publikacji:
    2012-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Mm
    61.30.Gd
    61.30.Hn
    Opis:
    Ferronematics are stable colloidal suspensions of magnetic particles in nematic liquid crystals. The presence of the magnetic particles enhances the magnetic susceptibility of ferronematics, in comparison with pure liquid crystals. In this work the thermotropic liquid crystal 4-(trans-4'-n-hexylcyclohexyl)-isothiocyanato-benzene (6CHBT) and 6CHBT dissolved in phenyl isothiocyanate were doped with spherical magnetic nanoparticles with aim to increase the sensitivity of the liquid crystal on an external magnetic field. The volume concentration of the magnetic particles was 5 × $10^{-4}$. The phase transition temperature from isotropic to nematic phase in the external magnetic field up to 12 T was monitored by precise capacitance measurements in the capacitance cells filled with nematic sample as well as with the prepared ferronematic sample. There was no observable shift in the transition temperature in the case of pure 6CHBT, 6CHBT doped with spherical particles and 6CHBT dissolved in phenyl isothiocyanate while in the case of 6CHBT dissolved in phenyl isothiocyanate doped with spherical magnetic particles the shift in the temperature about 9C of the phase transition from isotropic to droplet state at the external magnetic field 12 T was observed.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 5-6; 1276-1278
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Magnetic Properties of Magnetite Formed by Biomineralization and Chemical Synthesis
    Autorzy:
    Timko, M.
    Džarová, A.
    Kopčanský, P.
    Závišová, V.
    Koneracká, M.
    Kováč, J.
    Šprincová, A.
    Vaclavíková, M.
    Ivaničová, L.
    Vávra, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1813922.pdf
    Data publikacji:
    2008-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.75.+a
    47.65.Cb
    87.83.+a
    Opis:
    In this work, the magnetic properties of biologically produced magnetite (magnetosomes) by biomineralization process were compared to those of chemically synthesized $Fe_3O_4$. The coercivity of 185 Oe in magnetosomes is connected with the fact that the mean diameter is larger than critical size for transition from superparamagnetic to ferromagnetic behavior. A sharp magnetic transition at 105 K (Verwey transition) is clearly present in magnetosomes while in opposite, this transition is missing in $Fe_3O_4$.
    Źródło:
    Acta Physica Polonica A; 2008, 113, 1; 573-576
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Magnetic Properties of Biocompatible Magnetic Fluid after Electron Irradiation
    Autorzy:
    Tomašovičová, N.
    Haysak, I.
    Koneracká, M.
    Kováč, J.
    Timko, M.
    Závišová, V.
    Okunev, A.
    Parlag, A.
    Fradkin, A.
    Sakhno, V.
    Kopčanský, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1429089.pdf
    Data publikacji:
    2012-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Mm
    61.80.Fe
    61.82.Rx
    Opis:
    The magnetic particles in the water-based magnetic fluids were sterically stabilized by natrium oleate to prevent their agglomeration and consequently the adsorption of poly-ethylene-glycol (PEG) was carried out to improve the biocompatibility of the magnetic particles. Two sets of samples were prepared. The first set of the samples was with different molar weight of PEG (Mw = 400, 1000, 10000 and 20000) at the constant weight ratio of PEG/$Fe_3O_4$ = 0.25 and the second one was with different weight ratio of PEG/$Fe_3O_4$ and constant molar weight of PEG (Mw = 1000). The samples were irradiated with 20 Gy. The same reduction of saturated magnetization (about 10%) after electron irradiation with 20 Gy was observed for all prepared samples.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 5-6; 1302-1304
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Anchoring Energy of Liquid Crystal Molecules to Magnetic Particles in HAB-Based Ferronematics
    Autorzy:
    Tomašovičová, N.
    Koneracká, M.
    Kopčanský, P.
    Timko, M.
    Závišová, V.
    Vajda, A.
    Fodor-Csorba, K.
    Éber, N.
    Tóth-Katona, T.
    Jadzyn, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1813941.pdf
    Data publikacji:
    2008-01
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Mm
    61.30.Gd
    61.30.Hn
    Opis:
    In this work we describe the magnetic Freedericksz transition in HAB-based (4, 4'-di-n-heptylazoxybenzene) ferronematics. The ferronematic samples were prepared with two different volume concentrations of magnetic particles $φ_1 = 2×10^{-5}$ and $φ_2 = 2×10^{-4}$. The liquid crystal HAB is nematic at the temperatures from ≈53°C to 70°C and smectic A at the temperatures under 53°C. The anisotropy of dielectric permitivity of HAB liquid crystal is positive in nematic phase and negative in smectic A phase. The magnetic Fredericksz transition was studied in nematic phase at temperature 60°C.
    Źródło:
    Acta Physica Polonica A; 2008, 113, 1; 591-594
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Characterization of $Fe_3O_4$ Magnetic Nanoparticles Modified with Dextran and Investigation of Their Interaction with Protein Amyloid Aggregates
    Autorzy:
    Koneracká, M.
    Antošová, A.
    Závišová, V.
    Lancz, G.
    Gažová, Z.
    Šipošová, K.
    Juríková, A.
    Csach, K.
    Kováč, J.
    Tomašovičová, N.
    Fabián, M.
    Kopčanský, P.
    Powiązania:
    https://bibliotekanauki.pl/articles/1535048.pdf
    Data publikacji:
    2010-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Mm
    87.14.em
    87.19.xr
    Opis:
    Functionalised magnetic nanoparticles composed of $Fe_3O_4$ particles stabilised by sodium oleate and subsequently modified with dextran (MFDEX) were prepared by the co-precipitation method. Their morphology and particle size distribution were observed by scanning electron microscopy and photon cross correlation spectroscopy. In order to confirm the modification of magnetite surface with dextran physical techniques, including infrared spectroscopy, thermal analysis, and magnetic measurement, were used. Finally, the effect of MFDEX on amyloid fibrillar aggregates of human insulin and hen egg white lysozyme, typical amyloidogenic proteins, was investigated. In vitro interaction of MFDEX with protein amyloid fibrils resulted into destruction of amyloid aggregates. The anti-amyloid activity makes MFDEX of potential interest as therapeutic agent against amyloid-related diseases.
    Źródło:
    Acta Physica Polonica A; 2010, 118, 5; 983-985
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal Stability of Bent-Core Liquid Crystals Doped with Magnetic Nanoparticles
    Autorzy:
    Juríková, A.
    Csach, K.
    Miškuf, J.
    Tomašovičová, N.
    Mitróová, Z.
    Závišová, V.
    Koneracká, M.
    Kopčanský, P.
    Timko, M.
    Éber, N.
    Fodor-Csorba, K.
    Vajda, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1387994.pdf
    Data publikacji:
    2015-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.30.-v
    64.70.mj
    65.80.-g
    Opis:
    In the work phase transitions in bent-core liquid crystals were studied using differential scanning calorimetry. For the binary mixture of bent-core molecules with 50 wt% of rod-shaped compound, the nematic to smectic transition occured below 40°C and the crystallization temperature shifted to sub-ambient temperatures. The influence of doping of the bent-core liquid crystals with magnetic nanoparticles on the kinetics of observed phase transitions was studied. The phase transition temperatures were shifted depending on the nanoparticle type and changed with varying cooling rate for all studied liquid crystal samples.
    Źródło:
    Acta Physica Polonica A; 2015, 127, 2; 638-640
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Structural Phase Transition in Liquid Crystal Doped with Gold Nanoparticles
    Autorzy:
    Kopčanský, P.
    Tomašovičová, N.
    Koneracká, M.
    Timko, M.
    Mitróová, Z.
    Závišová, V.
    Éber, N.
    Fodor-Csorba, K.
    Tóth-Katona, T.
    Vajda, A.
    Jadzyn, J.
    Beaugnon, E.
    Chaud, X.
    Powiązania:
    https://bibliotekanauki.pl/articles/1535052.pdf
    Data publikacji:
    2010-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    75.50.Mm
    61.30.Gd
    61.30.Hn
    Opis:
    The influence of the inclusion of the dodecanethiol functionalized gold particles (with diameter 3-5 nm) on the structural transitions was investigated. The studied samples were based on the nematic liquid crystal 4-(trans-4'-n-hexylcyclohexyl)-isothiocyanatobenzene (6CHBT). The volume concentration of the gold particles was $ϕ_1 = 2 × 10^{-4}$ and $ϕ_2 = 10^{-3}$. The obtained results showed that the inclusion of the gold particles in the 6CHBT liquid crystal increases the sensitivity of such system on the external magnetic field.
    Źródło:
    Acta Physica Polonica A; 2010, 118, 5; 988-989
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-13 z 13

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