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Wyświetlanie 1-4 z 4
Tytuł:
Comparative Studies of Microstructure and Fatigue Life of Selected Lead-free Alloys
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Sobczak, N.
Wojciechowski, A.
Powiązania:
https://bibliotekanauki.pl/articles/379514.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lead free alloys
microstructure
mechanical properties
stopy bezołowiowe
mikrostruktura
właściwości mechaniczne
Opis:
Lead-free alloys containing various amounts of zinc (4.5%, 9%, 13%) and constant copper addition (1%) were discussed. The results of microstructure examinations carried out by light microscopy (qualitative and quantitative) and by SEM were presented. In the light microscopy, a combinatorial method was used for the quantitative evaluation of microstructure. In general, this method is based on the phase quanta theory according to which every microstructure can be treated as an arrangement of phases/structural components in the matrix material. Based on this method, selected geometrical parameters of the alloy microstructure were determined. SEM examinations were based on chemical analyses carried out in microregions by EDS technique. The aim of the analyses was to identify the intermetallic phases/compounds occurring in the examined alloys. In fatigue testing, a modified low cycle fatigue test method (MLCF) was used. Its undeniable advantage is the fact that each time, using one sample only, several mechanical parameters can be estimated. As a result of structure examinations, the effect of alloying elements on the formation of intermetallic phases and compounds identified in the examined lead-free alloys was determined. In turn, the results of mechanical tests showed the effect of intermetallic phases identified in the examined alloys on their fatigue life. Some concepts and advantages of the use of the combinatorial and MLCF methods in materials research were also presented.
Źródło:
Archives of Foundry Engineering; 2017, 17, 3; 111-116
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructural Aspects of Fatigue Parameters of Lead-Free Sn-Zn Solders with Various Zn Content
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Wojciechowski, A.
Sobczak, N.
Powiązania:
https://bibliotekanauki.pl/articles/379846.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lutowanie bezołowiowe
mikrostruktura
właściwości mechaniczne
lead-free solders
microstructure
mechanical properties
Opis:
The study includes the results of research conducted on selected lead-free binary solder alloys designed for operation at high temperatures. The results of qualitative and quantitative metallographic examinations of SnZn alloys with various Zn content are presented. The quantitative microstructure analysis was carried out using a combinatorial method based on phase quanta theory, according to which any microstructure can be treated as an array of elements disposed in the matrix material. Fatigue tests were also performed using the capabilities of a modified version of the LCF method hereinafter referred to in short as MLCF, which is particularly useful in the estimation of mechanical parameters when there are difficulties in obtaining a large number of samples normally required for the LCF test. The fatigue life of alloys was analyzed in the context of their microstructure. It has been shown that the mechanical properties are improved with the Zn content increasing in the alloy. However, the best properties were obtained in the alloy with a chemical composition close to the eutectic system, when the Zn-rich precipitates showed the most preferred morphological characteristics. At higher content of Zn, a strong structural notch was formed in the alloy as a consequence of the formation in the microstructure of a large amount of the needle-like Zn-rich precipitates deteriorating the mechanical characteristics. Thus, the results obtained during previous own studies, which in the field of mechanical testing were based on static tensile test only, have been confirmed. It is interesting to note that during fatigue testing, both significant strengthening and weakening of the examined material can be expected. The results of fatigue tests performed on SnZn alloys have proved that in this particular case the material was softened.
Źródło:
Archives of Foundry Engineering; 2017, 17, 1; 131-136
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructural Aspects of Fatigue Life of Sn-Zn Lead-free Solders with 1% of Ag Addition
Autorzy:
Pietrzak, K.
Klasik, A.
Maj, M.
Sobczak, N.
Wojciechowski, A.
Powiązania:
https://bibliotekanauki.pl/articles/382245.pdf
Data publikacji:
2018
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
lead-free solders
microstructure
mechanical properties
lutowanie bezołowiowe
mikrostruktura
właściwości mechaniczne
Opis:
The article presents the study results of Sn-Zn lead-free solders with the various Zn content. The results concern the hypoeutectic, eutectic and hypereutectic alloys containing respectively 4.5% Zn, 9% Zn and 13.5% Zn. Moreover, these alloys contain the constant Ag (1%) addition. The aim of the study was to determine the microstructural conditionings of their fatigue life. In particular it was focused on answer the question what meaning can be assigned to the Ag addition in the chemical composition of binary Sn-Zn alloys. The research includes a qualitative and quantitative assessments of the alloy microstructures, that have been carried out in the field of light microscopy (LM). In order to determine some geometrical parameters of the microstructure of alloys the combinatorial method based on the phase quanta theory was applied. Moreover, for the identification necessities the chemical analyses in the micro-areas by SEM/EDS technics were also performed. Based on the SEM/EDS results the phases and intermetallic compounds existing in the examined lead-free solders were identified. The mechanical characteristics were determined by means of the modified low cycle test (MLCF). Based on this method and on the results obtained every time from only one sample the dozen of essential mechanical parameters were evaluated. The research results were the basis of analyzes concerning the effects of microstructural geometrical parameters of lead-free alloys studied on their fatigue life at ambient temperature.
Źródło:
Archives of Foundry Engineering; 2018, 18, 1; 87-92
1897-3310
2299-2944
Pojawia się w:
Archives of Foundry Engineering
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Badania stabilności zawiesiny metalowo-ceramicznej po wielokrotnym przetopie kompozytu na bazie stopu aluminium A359 zbrojonego cząsteczkami Al2O3
Stability of metal-ceramic slurry after multiple re-melting of A359 aluminum alloy based composite reinforced with Al2O3 particles
Autorzy:
Pietrzak, K.
Sobczak, N.
Sobczak, J. J.
Klasik, A.
Kudyba, A.
Darłak, P.
Długosz, P.
Wojciechowski, A.
Sienicki, E.
Powiązania:
https://bibliotekanauki.pl/articles/391876.pdf
Data publikacji:
2017
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Odlewnictwa
Tematy:
kompozyty
recykling
wielokrotny przetop
stabilność zawiesiny metalowo-ceramicznej
metoda kropli leżącej
metal matrix composites
recycling
multiple re-melting
stability of metal-ceramic slurry
sessile drop method
Opis:
Metodę kropli leżącej zaadaptowano do badań wpływu wielokrotnego przetapiania i odlewania metalowych materiałów kompozytowych na strukturalną stabilność zawiesiny metalowo-ceramicznej. Do badań stosowano komercyjny kompozyt o osnowie stopu aluminium A359 (AlSiMg) firmy DURALCAN zawierający ok. 20% obj. cząsteczek tlenku glinu. Kompozyt poddano 10-krotnemu przetopieniu i odlewano, stosując dwa procesy znacznie różniące się czasem krzepnięcia zawiesiny metalowo-ceramicznej, tj. odlewanie grawitacyjne oraz prasowanie w stanie ciekłym (squeeze casting). Próbki kompozytu po każdorazowym cyklu przetopu i odlewania poddano badaniom wysokotemperaturowym na podłożu z tlenku glinu w próżni w temperaturze 850°C w ciągu 30 min. Zarówno bezpośrednia obserwacja zachowania próbek kompozytu podczas ich nagrzewania, jak i analiza strukturalna zakrzepłych próbek wykazała, że podczas topienia powstająca kropla zawiesiny metalowo-ceramicznej nie ulega rozwarstwianiu i zachowuje stabilność w badanym okresie czasowym, niezależnie od liczby przeprowadzonych przetopów i zastosowanego następnie sposobu odlewania kompozytu. Uzyskane wyniki potwierdzają dotychczasowe badania wskazujące na możliwość wielokrotnego przetapiania i ponownego odlewania kompozytów metalowych bez istotnej utraty ich właściwości użytkowych. Stwierdzona wysoka stabilność pierwotnej jednorodności zawiesiny metalowo- -ceramicznej upoważnia do zakwestionowania powszechnie akceptowanej tezy o nieprzydatności odlewanych kompozytów metalowych do recyklingu.
The sessile drop method was adopted to investigate the effect of multiple re-melting and casting of metal matrix composite on the structural stability of metal-ceramic slurry. Commercial aluminum matrix composite made of the A359Al alloy reinforced with about 20 vol. % Al2O3 particles was produced by DURALCAN and next re-melted and recast ten times using two casting methods, i.e. conventional gravity casting and squeeze casting. The samples taken from all composite ingots produced after every cycle of re-melting and re-casting were used for high temperature tests at a temperature of 850°C for 30 min, under vacuum conditions. Both direct observations of the behavior of composite samples placed on alumina substrates during their contact heating and at the test temperature as well as the detailed structural characterization of solidified droplets have shown high structural stability of the metalceramic slurry, irrespective of the number of re-melts and type of casting process used afterwards. The high stability of the originally obtained composite microstructure in each subsequent re-melting step in this study also entitles one to question the widely accepted opinion on the difficulties with re-melting of cast composites, and thus their unsuitability for recycling.
Źródło:
Prace Instytutu Odlewnictwa; 2017, 57, 2; 69-84
1899-2439
Pojawia się w:
Prace Instytutu Odlewnictwa
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-4 z 4

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