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Wyświetlanie 1-15 z 18
Tytuł:
FT-IR and NMR spectral LFER model analysis on some 3-(1-naphthyl)-1-substituted phenyl chalcones
Autorzy:
Sekar, K. G.
Janaki, P.
Muthuvel, I.
Sathiyendiran, V.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1031827.pdf
Data publikacji:
2020
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
1-Naphthyl styryl ketone
Aldol condensation
IR and NMR Spectra
LFER Model
Opis:
In this investigation, the authors predicted the effects of substituents on the functional groups of the titled chalcones using Linear Free Energy Relationship through Hammett equation with its constants and Swain-Lupton parameters. The LFER model statistical analysis was carried out using single and multi-linear regression analysis in MS Office 365 XL package. From the LFER analysis outcome, the influence of substituents on the spectroscopic functionality were discussed with their electronic effects such as, polar, inductive, resonance, field and conjugation. The titled compounds were prepared by solvent-free Aldol-Condensation method. The prepared compounds were characterised by their physical constants, micro analysis and spectroscopic data (FT-IR, NMR and Mass).
Źródło:
World Scientific News; 2020, 147; 88-103
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and spectral Hammett correlation analysis of some (E)-3-(5-bromothiophen-2-yl)-1-phenylprop-2-en-1-one compounds
Autorzy:
Christuraj, P.
Rajakumar, P. R.
Geetha, C.
Vanangamudi, G.
Arulkumran, R.
Manikandan, V.
Sundararajan, R.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1179576.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
(E)-3-(5-bromothiophen-2-yl)-1-phenylprop-2-en-1-ones
FT-IR and NMR spectra
Hammett correlation analysis
Substituent constants
Substituent effects
UV
Opis:
A series of substituted of (E)-3-(5-bromothiophen-2-yl)-1-phenylprop-2-en-1-one compounds by cross-aldol condensation reaction of 5-bromothiophene-2-carbaldehyde with various substituted acetaldehyde in the presence sodium hydroxide (base). The synthesized substituted (E)-3-(5-bromothiophen-2-yl)-1-phenylprop-2-en-1-one compounds was characterized by physical constants, UV, FT-IR, 1H & 13C-NMR spectral data. The group frequencies of infrared ʋ(cm-1) of CO s-cis and s-trans, CH in-plane and out of plane, CH=CH out of plane, >C=C< out of plane modes, NMR chemical shifts δ (ppm) of Hα, Hβ, CO, Cα and Cβ of these chalcones were correlated with Hammett substituent constants, F and R parameters using single and multi-regression analyses.
Źródło:
World Scientific News; 2017, 74; 15-35
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and effects of substituent on (E)-styryl-3-methyl-2-thienyl chalcones
Autorzy:
Christuraj, P.
Geetha, C.
Vanangamudi, G.
Arulkumaran, R.
Manikandan, V.
Rajakumar, P. R.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1161056.pdf
Data publikacji:
2018
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
(E)-3-(3-methylthiophen-2-yl)-1-phenylprop-2-en-1-ones
FT-IR & NMR spectra
Fly-ash:H3PO4 nanocatalyst
Hammett correlation analysis
Substituent effects
UV
solvent-free synthesis
Opis:
Series of eleven substituted of (E)-3-(3-methylthiophen-2-yl)-1-phenylprop-2-en-1-ones compounds by cross-aldol condensation reaction of 3-methylthiophene-2-carbaldehyde with various substituted acetaldehyde in the occurrence of Fly-Ash: H3PO4 catalyst. The effect of catalytic activity of this fly-ash:H3PO4 nanocatalyst was studied with the obtained yield of products under solvent-free conditions. The synthesized substituted (E)-3-(3-methylthiophen-2-yl)-1-phenylprop-2-en-1-one compounds was characterized by physical constants, UV, FT-IR, 1H & 13C-NMR spectral data. The infrared group frequencies of ʋ(cm-1) of COs-cis & s-trans, CHip and CHop, CH=CHop, >C=C
Źródło:
World Scientific News; 2018, 112; 55-73
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microwave assisted sulphated titania catalyzed aldol condensation: Synthesis of some (E) 3-(2-naphthyl)-1-(substituted phenyl)-2-propen-1-ones under solvent-free conditions
Autorzy:
Janaki, P.
Sekar, K. G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/411813.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
aldol condensation
sulphated titania
microwave irradiation
2-propen-1-ones
Opis:
A series of titled chalcones were synthesized by aldol condensation between 2-naphthaldehyde and various substituted acetophenones using solid acidic solid sulphated titania catalyst under microwave irradiation. The yields of these chalcones are more than 90 %. The synthesized chalcones are characterized by their physical constants, analytical and spectroscopic data.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 9; 16-22
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Insect antifeedant potent halogen substituted phenyl chalcones
Autorzy:
Sundararajan, R.
Arulkumaran, R.
Vijayakumar, S.
Kamalakkannan, D.
Suresh, R.
John, J. S.
Ranganathan, K.
Sakthinathan, S. P
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412081.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Substituted styryl 2′,3′,4′-trichlorophenyl ketones
sulfated Titania
IR and NMR spectra
Insect antifeedant activities
Opis:
Some 2′,3′,4′-trichlorophenyl chalcones [(E)-1-(2,3,4-trichlorophenyl)-3-(substituted phenyl)-2-propen-1-ones] have been synthesised using sulfated Titania catalyzed solvent-free aldol condensation between 2,3,4-trichloroacetophenone and substituted benzaldehydes. The purities of synthesised chalcones were checked by their analytical, physical and spectroscopic data reported in literature. The insect antifeedant activities of these chalcones have been studied using 4th instar larvae Achoea Janata L by castor leaf disc bio-assay method. The chloro substituted chalcones shows significant insect antifeedant activity.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 1; 67-73
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spectral correlations and antimicrobial activities of some (E)-N-Benzylidenepyridin-2-amines
Autorzy:
Sakthinathan, S. P.
Suresh, R.
Mala, V.
Sathiyamoorthi, K.
Kamalakkannan, D.
Ranganathan, K.
Arulkumaran, R.
Vijayakumar, S.
Sundararajan, R.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412108.pdf
Data publikacji:
2013
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Oxidative coupling Solvent-free synthesis
fly-ash
PTS
Aryl imines
IR and NMR spectra
Opis:
A series of aryl imines have been synthesized by Fly-ash: PTS catalyzed microwave assisted oxidative coupling of amines and aldehydes under solvent-free conditions. The yield of the imines has been found to be more than 90 %. The purity of all imines has been checked using their physical constants and spectral data as published earlier in literature. The UV ?maxC=N(nm), infrared ?C=N(cm-1), NMR ?(ppm) of CH=N and C=N spectral data have been correlated with Hammett substituent constants and F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the above spectral data has been studied. The antimicrobial activities of all imines have been studied using Bauer-Kirby method.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2013, 6; 77-90
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, spectral correlations and antimicrobial activities of some 2-hydroxyphenyl-styrylketone
Autorzy:
Sathiyamoorthi, K.
Mala, V.
Suresh, R.
Sakthinathan, S.P.
Kamalakkannan, D.
Ranganathan, K.
Arulkumaran, R.
Sundararajan, R.
Vijayakumar, S.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/411660.pdf
Data publikacji:
2013
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
solvent-free synthesis
SiO2-H3PO4
2’-hydroxyphenylchalcones
UV
IR
NMR spectra
Opis:
Some 2’-hydroxyphenylchalcones have been synthesized under microwave irradiation by Claisen-Schmidt condensation between substituted 2-hydroxyacetophenone and substituted benzaldehydes using catalytic amount of SiO2-H3PO4. These chalcones were established by their physical constants and spectroscopic data published earlier. The UV, IR, 1H NMR and 13C NMR spectral data of these chalcone have correlated with Hammett substituent constants, F and R parameters. All the compounds have been subjected to screened for antimicrobial activity.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2013, 7, 2; 102-119
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microwave assisted synthesis, spectral studies and antimicrobial activities of some 2′,4′-difluorophenyl chalcones
Autorzy:
Vijayakumar, S.
Arulkumaran, R.
Sundararajan, R.
Sakthinathan, S. P.
Suresh, R.
Kamalakkannan, D.
Ranganathan, K.
Sathiyamoorthy, K.
Mala, V.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412217.pdf
Data publikacji:
2013
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Microwave irradiation
Aldol condensation
Hydroxyapatite
Spectral correlations
Hammett σ constants
antimicrobial activities
Opis:
Some 2′,4′-difluorophenyl chalcones have been synthesized under microwave irradiation using aldol condensation between 2,4-difluoroacetophenone and substituted benzaldehydes using catalytic amount of hydroxyapatite. The yields of the chalcones are more than 85 %. The purities of these synthesized chalcones were examined by their physical constants and spectroscopic data. The UV absorption maxima (λmax, nm), infrared stretches (ν, cm-1) of CO, fingerprint region of CHip/op, CH=CHop, C=Cop modes, NMR chemical shifts (δ, ppm) of vinyl proton, carbon and carbonyl carbons have been assigned and correlated with Hammett substituent constants, F and R parameters using single and multi-regression analysis. From the statistical analysis the effect of substituent on the above spectral frequencies can be discussed. The antimicrobial activities of these synthesized chalcones have been screened using Bauer-Kirby method.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2013, 9, 1; 68-86
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis and spectral correlation studies of some substituted (E)-1-Benzylidene-2-(diphenylmethylene) hydrazines
Autorzy:
Arulkumaran, R.
Manikandan, V.
Christuraj, P.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/1182844.pdf
Data publikacji:
2017
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
(e)-1-benzylidene-2-(diphenylmethylene) hydrazine
ir and nmr spectra
hammett correlations
Opis:
About ten substituted (E)-1-Benzylidene-2-(diphenylmethylene) hydrazine compounds have been synthesized. They are characterized by their analytical, ultraviolet, infrared and NMR spectral data. From infrared spectra, the CN and N+N vibrational frequencies (cm-1) of the hydrazines have been assigned. From NMR spectra, the chemical shifts (, ppm) of CH proton and C(C6H5)2 carbons of the hydrazines have been assigned. These data are correlated with Hammett substituent constants, F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the spectral data have been discussed.
Źródło:
World Scientific News; 2017, 62; 93-110
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spectral correlation analysis and antimicrobial activities of some 2,4-dimethoxy phenyl chalcones
Autorzy:
Joseph, S. J.
Arulkumaran, R.
Kamalakkannan, D.
Sakthinathan, S. P.
Sundararajan, R.
Suresh, R.
Vijayakumar, S.
Ranganathan, K.
Kalyanasundaram, N.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412661.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
substituted styryl 2
4-dimethoxy phenyl ketones
UV spectra
IR spectra
NMR spectra
substituent effects
antimicrobial activities
Opis:
A series of 2,4-dimethoxy phenyl chalcones have been synthesized by Crossed-Aldol condensation of 2,4-dimethoxy phenyl and various substituted benzaldehydes. The purities of these chalcones have been checked by their physical constants, UV, IR, NMR and MASS spectral data. The spectral data of these chalcones have been correlated with Hammett sigma constants, F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effects of substituents on the spectral group frequencies have been discussed. The anti-microbial activities of these chalcones have been evaluated using Bauer-Kirby method.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 4; 48-65
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Assessment of substituent effects and antimicrobial activities of some 2ʹ,5ʹ-dimethyl phenyl chalcones
Autorzy:
Joseph, S. J.
Kamalakkannan, D.
Arulkumaran, R.
Sakthinathan, S. P.
Suresh, R.
Sundararajan, R.
Vijayakumar, S.
Ranganathan, K.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412597.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
substituted styryl 2
5ʹ-dimethyl phenyl chalcones
UV spectra
IR spectra
NMR spectra
substituent effects
antimicrobial activities
Opis:
Some 2ʹ,5ʹ-dimethyl phenyl chalcones have been synthesized by Crossed-Aldol condensation between 2,5-dimethyl acetophenone and various substituted benzaldehydes using catalytic amount of sodium hydroxide and ethanol. The yields of the chalcones are more than 93 %. The purities of these chalcones have been checked by their physical constants, UV, IR, NMR and MASS spectral data. The spectral data of these chalcones have been correlated with Hammett sigma constants, F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effects of substituents on the spectral group frequencies have been discussed. The anti-microbial activities of these chalcones have been evaluated using Bauer-Kirby method.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 5; 99-123
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Correlation analysis of substituted 2-((phenyl amino)methyl)-1,2-dihydro-5-(3-methoxyphenyl)-1-phenyl-1,2,4-triazole-3-thiones
Autorzy:
Thirunarayanan, G.
Kamalkkannan, D.
Suresh, R.
Sakthinathan, S. P.
Sundararajan, R.
Arulkumara, R.
Manikandan, R.
Vanangamudi, G.
Sathiyendiran, V.
Powiązania:
https://bibliotekanauki.pl/articles/1194047.pdf
Data publikacji:
2015
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
1-2-4-triazole
Hammett constants
IR spectral
NMR spectral
Swain-Lupton’s parameters
correlation
multi-regression analysis
Opis:
A series of substituted 2-((phenyl amino)methyl)-1,2-dihydro-5-(3-methoxyphenyl)-1-phenyl-1,2,4-triazole-3-thione compounds were synthesized and examined their purities as per the literature. The IR spectra of νC=N, νC=S, νNH and νCOC frequencies and NMR chemical shifts (ppm) of δNH, δOCH3, δCH2, δC=N, δC=S, δOCH3 and δCH2 are also assigned. The assigned IR and both 1H NMR and 13C NMR spectral data have been correlated with Hammett substituent constants and Swain-Lupton’s parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the above spectral data has been studied.
Źródło:
World Scientific News; 2015, 12; 24-43
2392-2192
Pojawia się w:
World Scientific News
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Synthesis, spectral correlations and biological activities of some (E)-[4-(substituted benzylidene amino)phenyl] (phenyl) methanones
Autorzy:
Mayavel, P.
Thirumurthy, K.
Dineshkumar, S.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412136.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
Schiff's bases
fly-ash
PTS
IR spectra
NMR spectra
Hammett correlation
Opis:
A series of Schiff’s bases have been synthesized by fly-ash:p-toluenesulfonic acid (fly-ash:PTS) catalyzed microwave assisted oxidative coupling of arylamines and substituted benzaldehydes under solvent-free condition. The synthesized Schiff’s bases are characterized by their physical constants, analytical and spectroscopic data. The group frequencies of imines such as IR (v, cm–1) and NMR (δ, ppm) spectral data was correlated with Hammett substituent constants, F and R parameters using single and multi-linear regression analysis. The antimicrobial activities of these Schiff’s bases have been studied using Bauer-Kirby method.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 20, 2; 145-159
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Electrochemical reduction potential correlation of some insect antifeedant potent 2-phenothiazinyl chalcones
Autorzy:
Ranganathan, K.
Suresh, R.
Kamalakkannan, D.
Arulkumaran, R.
Sundararajan, R.
Sakthinathan, S. P.
Vijayakumar, S.
Thirumurthy, K.
Mayavel, P.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/411842.pdf
Data publikacji:
2012
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
elektrochemia
potencjał redukcji
analiza korelacji
2-phenothiazenyl
chalkony
2-Phenothiazenyl chalcones
electrochemistry
reduction potential
correlation analysis
insect antifeedant activities
Opis:
A series containing twelve substituted styryl 2-phenothiazenyl ketones have been synthesized. The electrochemical potentials of carbonyl and vinyl groups were measured. These potentials are correlated with Hammett substituent constants, F and R parameters. From the results of statistical analyses, the effects of substituent on the group reduction potentials have been discussed. The insect antifeedant activities of these chalcones have been studied using 4th instar larvae Achoea Janata L with castor leaf discs.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2012, 4; 66-75
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Spectral correlation analysis of Hammett substituent constants and biological activities of some (E)-1-(4-phenoxyphenyl)-3-phenylprop-2-en-1-ones
Autorzy:
Kalyanasundaram, N.
Sakthinathan, S. P.
Suresh, R.
Kamalakkannan, D.
Joseph, S. J.
Vanangamudi, G.
Thirunarayanan, G.
Powiązania:
https://bibliotekanauki.pl/articles/412539.pdf
Data publikacji:
2014
Wydawca:
Przedsiębiorstwo Wydawnictw Naukowych Darwin / Scientific Publishing House DARWIN
Tematy:
substituted styryl 4-phenoxyphenylketones
UV-spectra
IR spectra
NMR spectra
Hammett constants
substituent effects
regression analysis and antimicrobial activities
Opis:
A series of aryl chalcones have been synthesized from 4-phenoxyacetophonone with various substituted benzaldehydes. The purity of all chalcones has been checked using their physical constants and spectral data. These spectral data have been correlated with Hammett substituent constants and F and R parameters using single and multi-linear regression analysis. From the results of statistical analysis, the effect of substituents on the above spectral data has been studied. The single parameter correlation with few Hammett constants and F and R parameters gave satisfactory correlation coefficients whereas all multiple correlations gave satisfactory correlation coefficients with Resonance, Field and Swain-Lupton’s parameters. The antimicrobial activities of all chalcones have been studied using Bauer-Kirby method.
Źródło:
International Letters of Chemistry, Physics and Astronomy; 2014, 9; 23-47
2299-3843
Pojawia się w:
International Letters of Chemistry, Physics and Astronomy
Dostawca treści:
Biblioteka Nauki
Artykuł
Wyświetlanie 1-15 z 18

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