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Wyświetlanie 1-3 z 3
Tytuł:
Defects in Ultra-Fine Grained Mg and Mg-Based Alloys Prepared by High Pressure Torsion Studied by Positron Annihilation
Autorzy:
Čížek, J.
Procházka, I.
Smola, B.
Stulíková, I.
Kužel, R.
Matěj, Z.
Cherkaska, V.
Islamgaliev, R.
Kulyasova, O.
Powiązania:
https://bibliotekanauki.pl/articles/2043304.pdf
Data publikacji:
2005-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
79.60.Jv
61.72.-y
Opis:
Despite the favourable strength and thermal stability, a disadvantage of the Mg-based alloys consists in a low ductility. Recently it has been demonstrated that ultra fine grained metals with grain size around 100 nm can be produced by high pressure torsion. A number of ultra fine grained metals exhibit favourable mechanical properties consisting in a combination of a very high strength and a significant ductility. For this reason, it is highly interesting to examine microstructure and physical properties of ultra fine grained Mg-based light alloys. Following this purpose, microstructure investigations and defect studies of ultra fine grained pure Mg and ultra fine grained Mg-10%Gd alloy prepared by high pressure torsion were performed in the present work using positron annihilation spectroscopy combined with X-ray diffraction, TEM observations, and microhardness measurements. Positrons are trapped at dislocations in Mg and Mg-10%Gd alloy deformed by high pressure torsion. A number of dislocations increases with the radial distance r from the centre to the margin of the sample. No microvoids (small vacancy clusters) were detected. Mg-10%Gd alloy deformed by high pressure torsion exhibits a homogeneous ultra fine grained structure with a grain size around 100 nm and high dislocations density. On the other hand, pure Mg deformed by high pressure torsion exhibits a binomial type of structure which consists of "deformed regions" with ultra fine grained structure and a high dislocation density and dislocation-free "recovered regions" with large grains. It indicates a dynamic recovery of microstructure during high pressure torsion processing.
Źródło:
Acta Physica Polonica A; 2005, 107, 5; 738-744
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Microstructure, Thermal and Mechanical Properties of Non-Isothermally Annealed Al-Sc-Zr and Al-Mn-Sc-Zr Alloys Prepared by Powder Metallurgy
Autorzy:
Vlach, M.
Stulíková, I.
Smola, B.
Císařová, H.
Piešová, J.
Daniš, S.
Gemma, R.
Tanprayoon, D.
Neubert, V.
Powiązania:
https://bibliotekanauki.pl/articles/1418427.pdf
Data publikacji:
2012-09
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
81.20.Ev
81.30.Mh
Opis:
This paper reports results of a study aimed at understanding the precipitation processes occurring during the annealing of two Al-Sc-Zr-based alloys with and without Mn prepared by powder metallurgy with subsequent hot extrusion at 350°C. Samples were isochronally annealed up to ≈ 570°C. Precipitation behaviour was studied by electrical resistometry and differential scanning calorimetry. Mechanical properties were monitored by microhardness HV1 measurements. Transmission electron microscopy examinations and X-ray diffraction of specimens quenched from temperatures of significant resistivity changes helped to identify the microstructural processes responsible for these changes. Fine (sub)grain structure develops and fine coherent $Al_3Sc$ and/or $Al_3(Sc,Zr)$ particles precipitate during extrusion in both alloys. The distinct changes in resistivity (at temperatures above ≈ 330°C) of the Al-Mn-Sc-Zr alloy are mainly caused by precipitation of Mn-containing particles. The easier diffusion of Mn atoms along the (sub)grain boundaries is responsible for the precipitation of the $Al_6Mn$ and/or $Al_6(Mn,Fe)$ particles at relatively lower temperatures compared to the temperature range of precipitation of these particles in the classical mould-cast Al-Mn-Sc-Zr alloys The apparent activation energy for precipitation of the $Al_3Sc$ and $Al_6Mn$ particles in the Al-Mn-Sc-Zr alloy was determined as (106 ± 10) kJ $mol^{-1}$ and (152 ± 33) kJ $mol^{-1}$, respectively.
Źródło:
Acta Physica Polonica A; 2012, 122, 3; 439-443
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
Ultra Fine-Grained Metals Prepared by Severe Plastic Deformation: A Positron Annihilation Study
Autorzy:
Čížek, J.
Procházka, I.
Kužel, R.
Matĕj, Z.
Cherkaska, V.
Cieslar, M.
Smola, B.
Stulíková, I.
Brauer, G.
Anwand, W.
Islamgaliev, R. K.
Kulyasova, O.
Powiązania:
https://bibliotekanauki.pl/articles/2043303.pdf
Data publikacji:
2005-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
78.70.Bj
79.60.Jv
Opis:
Recent investigations of ultra fine-grained metals (Cu, Fe, Ni) performed within a Prague-Rossendorf-Ufa collaboration will be reviewed. The specimens were prepared by severe plastic deformation: the high-pressure torsion and equal channel angular pressing. Positron annihilation spectroscopy was used as the main method including (i) the conventional lifetime and the Doppler broadening measurements with $\text{}^{22}$Na and (ii) the slow-positron implantation spectroscopy with the Doppler broadening measurement. Other methods were also involved: transmission electron microscopy, X-ray diffraction, and microhardness. First, the mean grain size was determined and defects were identified in the as-deformed materials. Defects concentration and spatial distribution were studied in detail. Dislocations situated in distorted regions along grain boundaries, and a few-vacancy clusters distributed homogeneously inside dislocations-free grains, were observed in the ultra fine-grained Cu, Fe, and Ni. Subsequently, the thermal evolution of the ultra fine-grained structures during isochronal annealing was studied.
Źródło:
Acta Physica Polonica A; 2005, 107, 5; 745-752
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-3 z 3

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