- Tytuł:
- Microstructure, Thermal and Mechanical Properties of Non-Isothermally Annealed Al-Sc-Zr and Al-Mn-Sc-Zr Alloys Prepared by Powder Metallurgy
- Autorzy:
-
Vlach, M.
Stulíková, I.
Smola, B.
Císařová, H.
Piešová, J.
Daniš, S.
Gemma, R.
Tanprayoon, D.
Neubert, V. - Powiązania:
- https://bibliotekanauki.pl/articles/1418427.pdf
- Data publikacji:
- 2012-09
- Wydawca:
- Polska Akademia Nauk. Instytut Fizyki PAN
- Tematy:
-
81.20.Ev
81.30.Mh - Opis:
- This paper reports results of a study aimed at understanding the precipitation processes occurring during the annealing of two Al-Sc-Zr-based alloys with and without Mn prepared by powder metallurgy with subsequent hot extrusion at 350°C. Samples were isochronally annealed up to ≈ 570°C. Precipitation behaviour was studied by electrical resistometry and differential scanning calorimetry. Mechanical properties were monitored by microhardness HV1 measurements. Transmission electron microscopy examinations and X-ray diffraction of specimens quenched from temperatures of significant resistivity changes helped to identify the microstructural processes responsible for these changes. Fine (sub)grain structure develops and fine coherent $Al_3Sc$ and/or $Al_3(Sc,Zr)$ particles precipitate during extrusion in both alloys. The distinct changes in resistivity (at temperatures above ≈ 330°C) of the Al-Mn-Sc-Zr alloy are mainly caused by precipitation of Mn-containing particles. The easier diffusion of Mn atoms along the (sub)grain boundaries is responsible for the precipitation of the $Al_6Mn$ and/or $Al_6(Mn,Fe)$ particles at relatively lower temperatures compared to the temperature range of precipitation of these particles in the classical mould-cast Al-Mn-Sc-Zr alloys The apparent activation energy for precipitation of the $Al_3Sc$ and $Al_6Mn$ particles in the Al-Mn-Sc-Zr alloy was determined as (106 ± 10) kJ $mol^{-1}$ and (152 ± 33) kJ $mol^{-1}$, respectively.
- Źródło:
-
Acta Physica Polonica A; 2012, 122, 3; 439-443
0587-4246
1898-794X - Pojawia się w:
- Acta Physica Polonica A
- Dostawca treści:
- Biblioteka Nauki
Artykuł