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    Wyświetlanie 1-8 z 8
    Tytuł:
    Hydrogen-Induced Defects in Palladium
    Autorzy:
    Melikhova, O.
    Čížek, J.
    Procházka, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1338026.pdf
    Data publikacji:
    2014-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.70.Bj
    61.72.-y
    Opis:
    In the present work positron annihilation spectroscopy was employed for investigation of hydrogen-induced defects in Pd. Well annealed Pd samples were electrochemically charged with hydrogen and development of defects with increasing hydrogen concentration $x_{H}$ was investigated. At low concentrations (α-phase, $x_{H}$ < 0.017 H/Pd) hydrogen loading introduced vacancies, since absorbed hydrogen segregating at vacancies lowers remarkably the vacancy formation energy. When hydrogen concentration exceeds 0.017 H/Pd, particles of palladium hydride (PdH) are formed. Stress induced by growing PdH particles leads to plastic deformation which generates dislocations and vacancies in the sample.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 3; 752-755
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Defects in Zirconia Nanomaterials Doped with Rare-Earth Oxides
    Autorzy:
    Prochazka, I.
    Cizek, J.
    Melikhova, O.
    Konstantinova, T.
    Danilenko, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1338541.pdf
    Data publikacji:
    2014-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.07.Wx
    61.46.Hk
    78.70.Bj
    Opis:
    Positron lifetime and coincidence Doppler broadening measurements on $ZrO_2$+3 mol.% $RE_2O_3$ (RE = Eu, Gd, Lu) nanopowders and ceramics obtained by sintering these nanopowders are reported. The initial nanopowders were prepared by a co-precipitation technique and exhibited a mean particle size of ≈ 15 nm. The nanopowders were calcined and pressure-compacted. All compacted nanopowders exhibited the prevailing tetragonal phase with at most 15% of the monoclinic admixture. Positrons in compacted nanopowders were found to annihilate almost exclusively at grain boundaries: (i) vacancy-like misfit defects along grain boundaries and (ii) larger defects situated at intersections of grain boundaries (triple points). In nanopowders, a small portion of positrons formed positronium in pores between crystallites. Sintering of nanopowders at 1500C caused a substantial grain growth and formation of ceramics. Sintering-induced grain growth led to a disappearance of the triple points and pores. The ceramics containing Eu and Gd dopants consist of mixture of the monoclinic and the tetragonal phase, while the ceramics with Lu dopant exhibits almost exclusively the tetragonal phase.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 3; 760-763
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Precipitation Effects in Mg-Zn Alloys Studied by Positron Annihilation and Hardness Testing
    Autorzy:
    Hruška, P.
    Čížek, J.
    Vlček, M.
    Melikhova, O.
    Procházka, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1196079.pdf
    Data publikacji:
    2014-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.70.Bj
    61.72.J-
    Opis:
    In the present work positron annihilation spectroscopy combined with Vickers hardness testing were employed in order to investigate precipitation effects in Mg-Zn alloys. It was found that incoherent precipitates of a metastable Zn-rich phase formed in the samples isochronally annealed above 200C cause hardening of the alloy.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 3; 718-721
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Investigation of Precipitation Effects in Mg-Tb and Mg-Tb-Nd Alloys
    Autorzy:
    Vlček, M.
    Čížek, J.
    Melikhova, O.
    Hruška, P.
    Procházka, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1196115.pdf
    Data publikacji:
    2014-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.70.Bj
    61.72.J-
    Opis:
    Investigation of precipitation effects in solution treated Mg-Tb and Mg-Tb-Nd alloy was performed. Solution treated alloys were compared with samples deformed by high pressure torsion to examine influence of deformation on precipitation effects. Dislocations present in samples processed by high pressure torsion can serve as diffusion channels for atoms and also as nucleation sites for precipitates. Therefore precipitation of some phases in high pressure torsion deformed samples was observed at lower temperatures than in solution treated ones.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 3; 744-747
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Defects Studies of ZnO Single Crystals Prepared by Various Techniques
    Autorzy:
    Lukáč, F.
    Čížek, J.
    Procházka, I.
    Melikhova, O.
    Anwand, W.
    Brauer, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1196118.pdf
    Data publikacji:
    2014-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.70.Bj
    61.72.J-
    Opis:
    The aim of the present work was a comparison of defects in ZnO crystals grown by various techniques available nowadays, namely hydrothermal growth, pressurized melt, Bridgman method growth and vapor phase growth. Positron annihilation spectroscopy was employed as a principal tool for characterization of defects in ZnO crystals grown by above mentioned various techniques. ZnO crystals can be divided into two groups: (i) hydrothermal grown crystals, which exhibit positron lifetime of 179-182 ps and (ii) ZnO crystals grown by the other techniques (pressurized melt, Bridgman method, vapor phase growth) which are characterized by the lower lifetimes falling in the range of 160-173 ps. Comparison of experimental data with ab initio theoretical calculations revealed that HT grown ZnO crystals contains Zn vacancies associated with hydrogen atom in a bond-centered site. On the other hand, ZnO crystals prepared by other techniques contain most probably stacking faults created by stresses induced by temperature gradients in the melt.
    Źródło:
    Acta Physica Polonica A; 2014, 125, 3; 748-751
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Positron Lifetimes in Zirconia-Based Nanomaterials
    Autorzy:
    Procházka, I.
    Čížek, J.
    Kuriplach, J.
    Melikhova, O.
    Konstantinova, T.
    Danilenko, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1812546.pdf
    Data publikacji:
    2008-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.70.Bj
    61.46.Hk
    81.05.Je
    81.07.Wx
    Opis:
    Positron lifetime spectroscopy is employed in a comparative study of several zirconia-based materials: (i) the pressure-compacted nanopowders of the three zirconia polymorphs - pure $ZrO_2$ (monoclinic), yttria-stabilized $ZrO_2$+3 mol.% $Y_2O_3$ (tetragonal) and yttria-stabilized $ZrO_2$+8 mol.% $Y_2O_3$ (cubic), (ii) ceramic materials obtained by sintering of the above two yttria-stabilized zirconia nanopowders and (iii) the tetragonal and cubic yttria-stabilized zirconia monocrystals. Positron lifetime data observed on the nanopowders suggest that the two shortest components, exhibiting lifetimes of ≈180 and ≈370 ps, arise from the annihilation of positrons trapped in defects associated with grain boundaries, presumably the vacancy-like defects and tripple points, respectively. Positron lifetime spectra observed on the ceramic materials resemble those found for the corresponding monocrystals, giving thus an additional support to the above interpretation of the nanopowders results.
    Źródło:
    Acta Physica Polonica A; 2008, 113, 5; 1495-1499
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Simulation of Positron Annihilation Response to Mechanical Deformation of Nanostructured AgCo
    Autorzy:
    Melikhova, O.
    Kuriplach, J.
    Čížek, J.
    Procházka, I.
    Hou, M.
    Pisov, S.
    Zhurkin, E.
    Powiązania:
    https://bibliotekanauki.pl/articles/1812541.pdf
    Data publikacji:
    2008-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.70.Bj
    71.15.Pd
    61.46.Hk
    Opis:
    Nanostructured materials attract nowadays a broad attention due to their specific properties. Defects play an essential role in material properties so their characterisation is very important. The evolution of the various open volume defects in AgCo nanowire modelled samples obtained using molecular dynamics was studied. Isothermal and isoenergetic deformation mechanisms are considered. General analyses of open volume defects concerning their size and their chemical environment were performed. Positron lifetimes, binding energies, and high momentum parts of the momentum distribution of annihilationγ-quanta were calculated for selected defects.
    Źródło:
    Acta Physica Polonica A; 2008, 113, 5; 1455-1464
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Positronium Probing of Pores in Zirconia Nanopowders
    Autorzy:
    Prochazka, I.
    Cizek, J.
    Lukac, F.
    Melikhova, O.
    Hruska, P.
    Anwand, W.
    Liedke, M.
    Konstantinova, T.
    Danilenko, I.
    Powiązania:
    https://bibliotekanauki.pl/articles/1033930.pdf
    Data publikacji:
    2017-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    81.07.Wx
    61.46.Hk
    78.70.Bj
    Opis:
    In the present paper, conventional positron lifetime measurements on selected zirconia-based nanopowders are reported. The nanopowders were doped with various metal cations (Y³⁺, Eu³⁺, Gd³⁺, Lu³⁺ and Mg²⁺). Lifetime experiments were conducted in air and supplemented with mass density measurements. In a range of lifetimes, from a few ns to ≈70 ns, up to two individual lifetime components could be identified. Such observations confirmed positronium (Ps) formation with subsequent ortho-Ps pick-off annihilation as well as the occurrence of pores of different size. Pore sizes were estimated using a shape-free model of the correlation between pore size and ortho-Ps lifetime. The origins of pores are discussed on the basis of the ortho-Ps data in combination with the results of mass density measurements.
    Źródło:
    Acta Physica Polonica A; 2017, 132, 5; 1564-1567
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-8 z 8

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