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    Wyświetlanie 1-4 z 4
    Tytuł:
    Thin SnO2 Films Manufactured Via the Sol-Gel and Electrospinning Methods
    Autorzy:
    Matysiak, W.
    Tański, T.
    Smok, W.
    Polishchuk, O.
    Powiązania:
    https://bibliotekanauki.pl/articles/351688.pdf
    Data publikacji:
    2020
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    thin films
    nanofibers
    tin oxide
    electrospinning
    optical properties
    Opis:
    The aim of this work was to produce a thin SnO2 film by a technique combining the sol-gel method and electrospinning from a solution based on polyvinylpyrrolidone and a tin chloride pentahydrate as a precursor. The spinning solution was subjected to an electrospinning process, and then the obtained nanofiber mats were calcined for 10 h at 500°C. Then, the scanning electron microscopy morphology analysis and chemical composition analysis by X-ray microanalysis of the manufactured thin film was performed. It was shown that an amorphous-crystalline layer formed by the SnO2 nanofiber network was obtained. Based on the UV-Vis spectrum, the width of the energy gap of the obtained layer was determined.
    Źródło:
    Archives of Metallurgy and Materials; 2020, 65, 2; 761-765
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Polyvinylpyrrolidone/Silicon Dioxide Composite Thin Films - Preparation and Analysis of Properties
    Autorzy:
    Tański, T.
    Matysiak, W.
    Zaborowska, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/355952.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    spin coating
    PVP/SiO2
    thin films
    composite coatings
    optical properties
    Opis:
    The purpose of this study was to produce composite thin films with polyvinylpyrrolidone (PVP) matrix with nanoparticles of silicon dioxide (SiO2 ) as the reinforcing phase (5 and 10%) using spin coating method and to investigate the influence of mass concentration of silica particles and process parameters on the morphology and optical properties of the obtained PVP/SiO2 nanocomposite coatings. The composite layer topography examination, made using atomic force microscope (AFM), showed the increase of roughness due to the increase of silica mass concentration in thin films. UV-Vis spectroscopy analysis showed that with the increase of SiO2 nanoparticles in polymer matrix and use of higher rotation speed, the absorbance level decrease. Besides, composite layers with 10% mass concentration relative to polymer concentration were characterized by wider energy band gap, so it can be concluded that obtained nanocomposite thin films can be used as protective layers against UV radiation, with zero absorption in the range of visible light wavelengths.
    Źródło:
    Archives of Metallurgy and Materials; 2018, 63, 1; 211-215
    1733-3490
    Pojawia się w:
    Archives of Metallurgy and Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Manufacturing process and characterization of electrospun PVP/ZnO NPs nanofibers
    Autorzy:
    Matysiak, W.
    Tański, T.
    Zaborowska, M.
    Powiązania:
    https://bibliotekanauki.pl/articles/201889.pdf
    Data publikacji:
    2019
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    electrospinning
    PVP
    ZnO
    nanofibers
    band gap
    nanocomposites
    optical properties
    elektrospining
    nanowłókna
    pasmo wzbronione
    nanokompozyty
    właściwości optyczne
    Opis:
    Constantly developing nanotechnology provides the possibility of manufacturing nanostructured composites with a polymer matrix doped with ceramic nanoparticles, including ZnO. A specific feature of polymers, i.e. ceramic composite materials, is an amelioration in physical properties for polymer matrix and reinforcement. The aim of the paper was to produce thin fibrous composite mats, reinforced with ZnO nanoparticles and a polyvinylpyrrolidone (PVP) matrix obtained by means of the electrospinning process and then examining the influence of the strength of the reinforcement on the morphology and optical properties of the composite nanofibers. The morphology and structure of the fibrous mats was examined by a scanning electron microscope (SEM) with an energy dispersive spectrometer (EDS) and Fourier-transform infrared spectroscopy (FTIR). UV –Vis spectroscopy allowed to examine the impact of zinc oxide on the optical properties of PVP/ZnO nanofibers and to investigate the width of the energy gap.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2019, 67, 2; 193-200
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Influence of calcination temperature on optical and structural properties of TiO2 thin films prepared by means of sol-gel and spin coating
    Autorzy:
    Tański, T.
    Matysiak, W.
    Kosmalska, D.
    Lubos, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/201456.pdf
    Data publikacji:
    2018
    Wydawca:
    Polska Akademia Nauk. Czytelnia Czasopism PAN
    Tematy:
    TiO2 thin films
    spin coating
    optical properties
    structural properties
    calcination
    sol-gel
    titanium dioxide
    Cienkie warstwy TiO2
    właściwości optyczne
    właściwości strukturalne
    kalcynacja
    zol-żel
    dwutlenek tytanu
    Opis:
    In this study, ceramic TiO2 thin films were prepared on glass substrates using sol-gel and spin-coating methods from the TNBT/ AcOH/ EtOH/ H2O solution. The obtained coatings were subjected to drying at room temperature and were then calcined in the air at different temperatures in a range of 400–600°C in order to obtain clean TiO2   layers. The surface morphology and chemical composition were characterized with the use of a scanning electron microscope (SEM) and an energy dispersive spectrometer (EDX). Research has shown the presence of elements in the TiO2   and the influence of temperatures on layer thickness. Analysis of optical properties and energy gap width of the prepared coatings was determined by means of spectra analysis of absorbance as a function of radiation energy obtained with the use of the UV-VIS spectrophotometer. The obtained spectra of the layers are characterized by a shift of absorption lines towards the visible light wavelengths and the obtained values of band gaps decrease as the calcination temperature rises. The obtained and developed results of TiO2   thin films testify to the wide application possibilities of the layers in elements which use photocatalytic processes such as self-cleaning surfaces, solar cells, pollution removing membranes and optoelectronic components.
    Źródło:
    Bulletin of the Polish Academy of Sciences. Technical Sciences; 2018, 66, 2; 151-156
    0239-7528
    Pojawia się w:
    Bulletin of the Polish Academy of Sciences. Technical Sciences
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-4 z 4

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