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    Tytuł:
    Framboidy pirytowe jako wskaźniki paleośrodowiska
    Pyrite framboids as paleoenvironmental indicators
    Autorzy:
    Zatoń, M.
    Rakociński, M.
    Marynowski, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/2074589.pdf
    Data publikacji:
    2008
    Wydawca:
    Państwowy Instytut Geologiczny – Państwowy Instytut Badawczy
    Tematy:
    framboidy pirytowe
    redoks
    warunki środowiskowe oksyczne
    warunki środowiskowe dysoksyczne
    warunki środowiskowe euksyniczne
    jura
    dewon
    Polska
    pyrite framboids
    redox
    euxinia
    anoxia
    dysoxia
    Jurassic
    Devonian
    Polska
    Opis:
    The problemof application of pyrite framboids in reconstructions of the redox conditions is presented. The characteristics of pyrite framboids, their origin and principles of application in paleoenvironmental interpretations are given. The pyrite framboid diameter distribution as indicators of redox conditions was presented on the examples of the Middle Jurassic (Upper Bajocian-Lower Bathonian) ore-bearing clays of the Polish Jura, and Upper Devonian (Middle and Upper Famennian) dark grey and black shales from Kowala (Holy Cross Mountains). It has been shown, that during the sedimentation of the ore-bearing clays, the pyrite framboids formed in the sediment, below the oxic water column; however, some episodic oscillation around the dysoxic conditions cannot be entirely excluded. During the sedimentation of the Middle Famennian dark grey shales, the redox conditions at the sea-floor oscillated around dysoxia. In both examples, the framboids are characterized by wide range of their diameters and the presence of large, >10 "my"m, framboids. On the contrary, the Upper Famennian black shales, representing the Hangenberg event, were deposited below the euxinic conditions in the water column. It is indicated by a high frequency of small-size framboids, far below 6 "my"m in diameter, and the lack of the large ones. The overlying shales, on the other hand, show the transition to more oxic conditions. The redox conditions interpreted above are in agreement with the independent biomarker analyses and paleontological observations.
    Źródło:
    Przegląd Geologiczny; 2008, 56, 2; 158-164
    0033-2151
    Pojawia się w:
    Przegląd Geologiczny
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Anomalous Upper Devonian mercury enrichments : comparison of Inductively Coupled Plasma – Mass Spectrometry (ICP-MS) and Atomic Absorption Spectrometry (AAS) analytical data
    Autorzy:
    Racki, G.
    Rakociński, M.
    Marynowski, L.
    Powiązania:
    https://bibliotekanauki.pl/articles/2060451.pdf
    Data publikacji:
    2018
    Wydawca:
    Państwowy Instytut Geologiczny – Państwowy Instytut Badawczy
    Tematy:
    Mercury anomalies
    analytical methods
    geochemistry
    Frasnian-Famennian boundary
    Devonian-Carboniferous boundary
    volcanism
    Opis:
    Mercury geochemistry is emerging recently as a hot topic in chemostratigraphical and facies research, owing to the diagnostic character of Hg enrichments as a proxy of volcanic activity (crucial in the context of assumed causal links between volcanic cataclysms and mass extinctions). Thus, as a prerequisite to such far-reaching interpretations, reliable analytical determinations of Hg concentrations are necessary. In conventionally performed analyses in sedimentary geochemistry, Inductively Coupled Plasma – Mass Spectrometry (ICP-MS) is usually applied, as an analytical standard for trace elements, including Hg. However, with a detection limit (DL) of 10 ppb, such measured values have been questioned as a conclusive geochemical indicator of Hg anomalies, and, instead, far more accurate techniques, such as Atomic Absorption Spectrometry (AAS; DL = 0.2 ppb), are requested. As a preliminary test of this view, we present comparative analysis of 91 samples from three sections encompassing the key Frasnian-Famennian and Famennian-Tournaisian boundary intervals in Morocco (Lahmida), Germany (Kahlleite) and Uzbekistan (Novchomok), for which Hg concentrations were determined by both methods in the same samples. Despite some differences, especially at low Hg concentrations, both analytical methods reveal the same 12 extraordinarily enriched samples in excess of 1 ppm (with one exception, the determination error is <20%), as well as similar overall chemostratigraphic patterns characterized by a few prominent Hg spikes, with a top value of 5.8 ppm. The Hg concentrations determined by ICP-MS and AAS are significantly correlated, as high as r = 0.98 (Novchomok), even if the first method reveals a general tendency toward slightly heightened values (by ~15 to 30% for medians). Therefore, ICP-MS results can conclusively be used in mercury chemostratigraphy in order to recognize extraordinary volcanic (or other) signals, at least in the Devonian geological record. False Hg anomalies were not generated by these conventional ICP-MS determinations.
    Źródło:
    Geological Quarterly; 2018, 62, 3; 487--495
    1641-7291
    Pojawia się w:
    Geological Quarterly
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
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