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Wyświetlanie 1-3 z 3
Tytuł:
Crystallization Process of $Fe_{75}Co_5Zr_{10}B_{10}$ Amorphous Alloy
Autorzy:
Sun, Y.
Zuo, B.
Wang, D.
Meng, X.
Liu, J.
Wang, L.
Hua, Z.
Powiązania:
https://bibliotekanauki.pl/articles/1399278.pdf
Data publikacji:
2013-10
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
61.43.Dq
64.60.My
Opis:
$Fe_{75}Co_5Zr_{10}B_{10}$ amorphous alloy prepared by melt-spinning was annealed at various temperatures. The thermal property and microstructures were investigated by differential thermal analysis, X-ray diffraction, and transmission electron microscopy. The crystallization process of $Fe_{75}Co_5Zr_{10}B_{10}$ amorphous alloy is complex. The α-Fe phase precipitates from the amorphous matrix in the initial stage of crystallization. The α-Mn type (χ) phase precipitates at 570°C, but transforms to α-Fe phase and the Laves C14(λ) phase at higher temperature. In the final stage of crystallization, $Fe_3Zr$, $Fe_2Zr$, and unknown phases are observed and the λ-phase disappears. The α-Fe phase preferentially nucleates after annealing at 530C for 10 min and the χ-phase preferentially nucleates after annealing at 600C for 10 min. The nucleation barrier of χ-phase is larger than that of α-Fe phase. The local structure of χ-phase is more similar to amorphous phase.
Źródło:
Acta Physica Polonica A; 2013, 124, 4; 685-687
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Effect of Nb Content on the Thermal, Structural, and Magnetic Properties of FeNbB Ribbons
Autorzy:
Hua, Z.
Zuo, B.
Li, M.
Wang, X.
Wang, L.
Liu, J.
Wang, D.
Dong, L.
Powiązania:
https://bibliotekanauki.pl/articles/1365063.pdf
Data publikacji:
2014-05
Wydawca:
Polska Akademia Nauk. Instytut Fizyki PAN
Tematy:
65.60.+a
61.43.Dq
Opis:
Amorphous $Fe_{80-x}Nb_{x}B_{20}$ (x = 5, 10, 15) ribbons were prepared by single-roller melt spinning method. The thermal, structural and magnetic properties of $Fe_{80-x}Nb_{x}B_{20}$ (x = 5, 10, 15) ribbons were investigated using differential thermal analysis, X-ray diffraction, and vibrating sample magnetometer. The thermal stability is the lowest for $Fe_{70}Nb_{10}B_{20}$ ribbon and the highest for $Fe_{65}Nb_{15}B_{20}$ ribbon. Along with the increase of Nb content, the supercooled liquid region Δ $T_{x}$ increases, indicating that the amorphous formation ability improves. The primary stages of crystallization of the three ribbons are different. The primary devitrification phases are $Fe_{23}B_6$ type for $Fe_{70}Nb_{10}B_{20}$ and $Fe_{75}Nb_5B_{20}$ ribbons, and α-Fe type for $Fe_{65}Nb_{15}B_{20}$ ribbon. $Fe_{80-x}Nb_{x}B_{20}$ (x = 5, 10) ribbons are ferromagnetic and the $Fe_{65}Nb_{15}B_{20}$ ribbon is paramagnetic. The saturation magnetization ($M_{s}$) decreases with increasing Nb content.
Źródło:
Acta Physica Polonica A; 2014, 125, 5; 1149-1151
0587-4246
1898-794X
Pojawia się w:
Acta Physica Polonica A
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The Microstructural Evolution in HMX Based Plastic-bonded Explosive During Heating and Cooling Process: an in situ Small-angle Scattering Study
Autorzy:
Yan, G.
Tian, Q.
Liu, J.
Fan, Z.
Sun, G.
Zhang, C.
Wang, Y.
Chen, B.
Gong, J.
Zhou, X.
Yang, Z.
Nie, F.
Li, J.
Li, X.
Powiązania:
https://bibliotekanauki.pl/articles/358618.pdf
Data publikacji:
2016
Wydawca:
Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
Tematy:
SANS
SAXS
HMX-PBX
thermal damages
phase transition
Opis:
The thermal damage in octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX) based plastic-bonded explosive (PBX) was investigated using in situ small-angle neutron and X-ray scattering techniques. The microstructural evolution was quantitatively characterized by the model fitting parameters of total interfacial surface area (Sv) and void volume distribution. The Sv of HMX-PBX decreased markedly above 100 °C, indicating the movement of binder into the voids. After subsequent cooling to room temperature, the scattering intensity increased significantly with increasing storage time, and a new population of voids with average diameter of 20 nm was observed, accompanied by the gradual phase transition of HMX from δ- to β-phase. The experimental results implied that serious damage within the HMX-PBX was developed during storage after heating.
Źródło:
Central European Journal of Energetic Materials; 2016, 13, 4; 916-926
1733-7178
Pojawia się w:
Central European Journal of Energetic Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-3 z 3

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