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    Wyświetlanie 1-5 z 5
    Tytuł:
    Preparation and Characterization of Ultrafine HMX/TATB Explosive Co-crystals
    Autorzy:
    An, C.
    Li, H.
    Zhang, Y.
    Ye, B.
    Xu, C.
    Wang, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/358105.pdf
    Data publikacji:
    2017
    Wydawca:
    Sieć Badawcza Łukasiewicz - Instytut Przemysłu Organicznego
    Tematy:
    HMX
    TATB
    ultrafine co-crystals
    ball milling
    mechanical sensitivity
    Opis:
    An explosive co-crystal of 1,3,5,7-tetranitro-1,3,5,7-tetraazacyclooctane (HMX) and 1,3,5-triamino-2,4,6-trinitrobenzene (TATB) was prepared by the ball milling method. The raw materials and co-crystals were characterized using scanning electron microscopy (SEM), X-ray diffraction (XRD), differential scanning calorimetry (DSC) and Raman spectroscopy. Impact and friction sensitivity of the co-crystals were tested and analyzed. The results showed that the HMX/TATB co-crystals are spherical in shape and 100-300 nm in size. The co-crystals are different from anintimate mixture of HMX/TATB and they exhibit a new co-crystal structure. HMX/TATB co-crystals are formed by N-O···H hydrogen bonding between −NO2 (HMX) and −NH2 (TATB). The drop height of ultrafine HMX/TATB explosive co-crystals is 12.7 cm higher than that of ultrafine HMX, whilst the explosion probability of friction is 20% lower than that of ultrafine HMX. Ultrafine HMX/TATB explosive co-crystals are difficult to initiate under impact and friction conditions.
    Źródło:
    Central European Journal of Energetic Materials; 2017, 14, 4; 876-887
    1733-7178
    Pojawia się w:
    Central European Journal of Energetic Materials
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Improved method for phase wraps reduction in profilometry
    Autorzy:
    Du, G.
    Wang, M.
    Zhou, C.
    Si, S.
    Li, H.
    Lei, Z.
    Li, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/173793.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    phase unwrapping
    zero-padding
    Fourier transform
    carrier-frequency
    profilometry
    Opis:
    In order to completely eliminate, or greatly reduce the number of phase wraps in 2D wrapped phase map, Gdeisat and co-workers proposed an algorithm, which uses shifting the spectrum towards the origin. But the spectrum can be shifted only by an integer number, meaning that the phase wraps reduction is often not optimal. In addition, Gdeisat’s method will take much time to make the Fourier transform, inverse Fourier transform, select and shift the spectral components. In view of the above problems, we proposed an improved method for phase wraps elimination or reduction. First, the wrapped phase map is padded with zeros, the carrier frequency of the projected fringe is determined by high resolution, which can be used as the moving distance of the spectrum. And then realize frequency shift in spatial domain. So it not only can enable the spectrum to be shifted by a rational number when the carrier frequency is not an integer number, but also reduce the execution time. Finally, the experimental results demonstrated that the proposed method is feasible.
    Źródło:
    Optica Applicata; 2017, 47, 2; 295-306
    0078-5466
    1899-7015
    Pojawia się w:
    Optica Applicata
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Preliminary results of spatial distribution of uranium and thorium in soil profi les near a uranium industrial site, Guangdong province, China
    Autorzy:
    Wang, J.
    Liu, J.
    Chen, Y.
    Song, G.
    Chen, D.
    Xiao, T.
    Li, H.
    Wang, C.
    Jiang, F.
    Powiązania:
    https://bibliotekanauki.pl/articles/146530.pdf
    Data publikacji:
    2016
    Wydawca:
    Instytut Chemii i Techniki Jądrowej
    Tematy:
    spatial distribution
    thorium
    uranium
    U/Th ratio
    Opis:
    Four soil profiles were collected from locations with different distances (5, 50, 250 and 1000 m) from a uranium mill tailings dam, Guangdong province, China, to investigate the pollution status of the soil in mining/ milling-related areas based on the contents of uranium (U) and thorium (Th), thus to understand the impacts of uranium industrial activities to the surroundings. The U and Th concentrations were determined by inductively coupled plasma mass spectrometry (ICP-MS) after conventional HF-HNO3-HClO4 digestion procedures. The results indicate that the soils within 50 m from uranium tailing were severely contaminated; those in 250 and 1000 m soil samples were observed to be with local background level even though these in 250 m had slightly higher U/Th ratios. Uranium concentrations varied from 5.50 ± 0.27 to 160.55 ± 8.03 mg/kg, with maximum values recorded in an intermediate layer of the 5-m distance soil profile. In comparison, the concentration of Th ranged from 6.02 ± 0.30 to 84.71 ± 4.24 mg/kg, with maximum values observed in the top layer of the 1000-m distance soil profile. The U/Th ratio varied from 0.15 to 11.99 compared with 0.20, 0.22 and 0.26 of the average for Guangdong province, national China and the world, respectively. The mean U/Th of four soil profiles showed a reduction with distance from the uranium mill tailing dam, suggesting the relatively large magnitude of uranium elevation in soils within limited distances.
    Źródło:
    Nukleonika; 2016, 61, 3; 367-371
    0029-5922
    1508-5791
    Pojawia się w:
    Nukleonika
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    One shot profilometry using iterative two-step temporal phase-unwrapping
    Autorzy:
    Du, G.
    Wang, M.
    Zhou, C.
    Si, S.
    Li, H.
    Lei, Z.
    Li, Y.
    Powiązania:
    https://bibliotekanauki.pl/articles/173912.pdf
    Data publikacji:
    2017
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    phase unwrapping
    composite fringe pattern
    Fourier transform
    two-step temporal phase-unwrapping
    Opis:
    This paper reviews two techniques that have been recently published for three-dimensional profilometry and proposes one shot profilometry using iterative two-step temporal phase-unwrapping by combining the composite fringe projection and the iterative two-step temporal phase unwrapping algorithm. In temporal phase unwrapping, many images with different frequency fringe pattern are needed to project, which would take much time. In order to solve this problem, Ochoa proposed a phase unwrapping algorithm based on phase partitions using a composite fringe. However, we found that the fringe order determined through the construction of phase partitions tended to be imprecise. Recently, we proposed an iterative two-step temporal phase unwrapping algorithm, which can achieve high sensitivity and high precision shape measurement. But it needs multiple frames of fringe images which would take much time. In order to take into account both the speed and accuracy of three-dimensional shape measurement, we get a new, and more accurate unwrapping method based on a composite fringe pattern by combining these two techniques. This method not only retains the speed advantage of Ochoa’s algorithm, but also greatly improves its measurement accuracy. Finally, the experimental evaluation is conducted to prove the validity of the proposed method.
    Źródło:
    Optica Applicata; 2017, 47, 1; 97-110
    0078-5466
    1899-7015
    Pojawia się w:
    Optica Applicata
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Comparison of float-sink and progressive release flotation of ground products of coal middlings
    Autorzy:
    Xie, W.
    He, Y.
    Luo, C.
    Zhang, X.
    Li, H.
    Yu, J.
    Wang, H.
    Shi, F.
    Powiązania:
    https://bibliotekanauki.pl/articles/109500.pdf
    Data publikacji:
    2015
    Wydawca:
    Politechnika Wrocławska. Oficyna Wydawnicza Politechniki Wrocławskiej
    Tematy:
    coal middlings
    float-sink
    progressive release flotation
    XPS
    EDX
    Opis:
    An additional recovery of coking coal middlings can be utilized for increasing of the concentrate yield of coking coal. A combined flow sheet of comminution and flotation can realize this target. To investigate the effect of grinding process on further flotation of ground products, progressive release flotation tests were used to compare with the float-sink tests, which were regarded as a criterion. Coal middlings were ground by wet-milling with iron balls to <0.5 mm. Curves of ash vs. cumulative yields of sized products indicated that the concentrate yield of coal separated by progressive release flotation was lower than that of coal benefited by the float-sink test, with the same ash for four size fractions (0.5-0.25 mm, 0.25-0.125 mm, 0.125-0.074 mm and <0.074 mm). Distributions of elements conducted by energy disperse spectroscopy (EDX) showed that associated kaolinite was liberated and exposed on the surface. It led to the shift of local surface property from hydrophobicity to hydrophilicity. Meanwhile, analyses of chemical property performed by an X-Ray photoelectron spectrometer (XPS) depicted that the hydrophilic mineral FeOOH, which generated in the grinding process, was adsorbed on the coal surface. Flotation of the ground products were worsened due to the increase of hydrophilicity of the coal surface.
    Źródło:
    Physicochemical Problems of Mineral Processing; 2015, 51, 2; 675-684
    1643-1049
    2084-4735
    Pojawia się w:
    Physicochemical Problems of Mineral Processing
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-5 z 5

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