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    Wyświetlanie 1-9 z 9
    Tytuł:
    Photoemission Electronic States of Thallium- and Bismuth-Based Superconductors
    Autorzy:
    Zalecki, R.
    Kołodziejczyk, A.
    König, J. W.
    Gritzner, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/2014372.pdf
    Data publikacji:
    2000-11
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    74.72.-h
    79.60.-i
    Opis:
    X-ray photoemission spectra the core-levels as well as the X-ray photoemission spectra and ultraviolet photoemission spectra from the valence bands of the (Tl$\text{}_{0.6}$Pb$\text{}_{0.5}$)(Sr$\text{}_{0.9}$Ba$\text{}_{0.1}$) Ca$\text{}_{2}$Cu$\text{}_{3}$O$\text{}_{y}$ and (Bi$\text{}_{1.75}$Pb$\text{}_{0.35}$)Sr$\text{}_{1.9}$Ca$\text{}_{2.05}$Cu$\text{}_{3.05}$O$\text{}_{y}$ superconductors were measured and analyzed. Special attention was paid to the valence band X-ray photoemission spectra and ultraviolet photoemission spectra, the Cu 2p core-level X-ray photoemission spectra and the Cu L$\text{}_{2,3}$-M$\text{}_{4,5}$M$\text{}_{4,5}$ and O K-L$\text{}_{2,3}$L$\text{}_{2,3}$ Auger spectra. Both Cu 2p$\text{}_{3}\text{}_{/}\text{}_{2}$ and Cu 2p$\text{}_{1}\text{}_{/}\text{}_{2}$ core-level lines consisted of two spin-orbit split main lines accompanied with the two satellite lines. The charge transfer energy Δ from the oxygen ligand to the copper 3d$\text{}^{9}$ states and the hopping integral t were estimated from the energy separation between the main line and the satellite line taking advantage of the local cluster model calculations and their extension to high-temperature superconductors. The Coulomb correlation on-site energy U$\text{}_{dd}$ of two electrons in the same copper orbital and U$\text{}_{pp}$ of two electrons in the oxygen orbital as well as the correlation energy U$\text{}_{cd}$ of the 2p core hole - 3d electron interaction have been estimated from the Auger electron spectra and the valence band spectra. They are: U$\text{}_{dd}$=6.0±0.5eV, of U$\text{}_{pp}$≅ 10±1eV and of U$\text{}_{cd}$≅ 8.0±0.5eV nearly the same for both the Tl- and Bi-compounds. We conclude that these compounds are the charge transfer strongly-correlated metals.
    Źródło:
    Acta Physica Polonica A; 2000, 98, 5; 513-524
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Photoemission Electronic States of (Mn$\text{}_{1-x}$Fe$\text{}_{x}$)$\text{}_{5}$Si$\text{}_{3}$
    Autorzy:
    Penc, B.
    Zalecki, R.
    Jezierski, A.
    Szytuła, A.
    Kołodziejczyk, A.
    Ivanov, V.
    Powiązania:
    https://bibliotekanauki.pl/articles/2043378.pdf
    Data publikacji:
    2005-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    79.60.-i
    71.20.Gj
    71.15.Ap
    Opis:
    The core-level and valence band electronic states studies of single crystalline transition metal silicides (Mn$\text{}_{1-x}$Fe$\text{}_{x}$)$\text{}_{5}$Si$\text{}_{3}$ (x=0 and 0.05) by the X-ray and ultraviolet photoemission spectroscopies are reported. The Mn 2p core-level spectra for both compounds were ascribed to the relevant Mn sites in their crystal structure. The valence band spectra were compared with the result of ab-initio band calculations using the tight-binding linear muffin-tin orbital method. It was concluded that the enhancement of the spectral density within the 2 eV binding energy region below the Fermi energy comes from the effect of strongly correlated Mn 3d electrons.
    Źródło:
    Acta Physica Polonica A; 2005, 107, 6; 967-976
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Electronic Band Structure and Photoemission States of $La_{2//3}Pb_{1//3}MnO_3$
    Autorzy:
    Tokarz, W.
    Kowalik, M.
    Zalecki, R.
    Kołodziejczyk, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1427488.pdf
    Data publikacji:
    2012-05
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    71.20.-b
    71.55.Ak
    72.80.Ga
    75.47.Lx
    79.60.-i
    Opis:
    We present the theoretical study of electronic and magnetic properties in a manganese perovskite $La_{2//3}Pb_{1//3}MnO_3$. The calculations were carried out in frame of the first-principles density functional theory with the general gradient approximation using the WIEN 2K package. The P3c1 crystal structure was taken from the detailed X-ray diffraction data for the perovskite. The exact exchange energy was utilized for Mn d electrons. Density of states was determined by the modified tetrahedron method. As a result we get a valence band for the spin up and down density of states with the gap for the latter of 1.85 eV. We noticed that conduction band is mainly dominated by d spin up manganese electrons and $Mn (d_{xz}, d_{yz})$ states have twice larger contribution than $(d_{x^2 - y^2}, d_{xy})$. We attribute this to $Mn-O_6$ octahedral tilting. From the same reason $d_{3z^2 - r^2}$ state has no contribution to the density of states at the Fermi energy $(E_{F})$. Comparison of total density of states with the ultraviolet photoemission spectroscopy measurements shows similar features especially as far as the lead spectral intensity from the 6s electrons at about - 10 eV is concerned. The calculated total magnetic moment per formula unit is 3.66 $μ_{B}$, the measured one 3.48 $μ_{B}$/f.u.
    Źródło:
    Acta Physica Polonica A; 2012, 121, 5-6; 1151-1153
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Electronic Band Structure of $La_{2//3}Pb_{1//3}Mn_{2//3}Fe_{1//3}O_3$
    Autorzy:
    Tokarz, W.
    Kowalik, M.
    Kołodziejczyk, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1431533.pdf
    Data publikacji:
    2012-04
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    71.20.-b
    71.55.Ak
    72.80.Ga
    75.47.lx
    79.60.-i
    Opis:
    We present theoretical studies of electric and magnetic properties in manganese perovskite $La_{2//3}Pb_{1//3}Mn_{2//3}Fe_{1//3}O_3$. The calculations were carried out by means of the first-principles density functional theory (DFT) with general gradient approximation GGA+U using Wien2K package. The P-3c1 crystal structure was chosen from the detailed X-ray diffraction data for the perovskite. For Mn and Fe d electrons exact exchange energy was utilized. Different orientation of magnetic moments on Mn and Fe atoms was considered. The computed density of states display band gap for both spin orientations in accord with our previous work, indicating that this compound should show an insulating ground state
    Źródło:
    Acta Physica Polonica A; 2012, 121, 4; 876-878
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Electronic Band Structures of $La_{2/3}Pb_{1/3}Mn_{2/3}(Fe,Co,Ni)_{1/3}O_{3}$
    Autorzy:
    Kowalik, M.
    Tokarz, W.
    Kołodziejczyk, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/1385092.pdf
    Data publikacji:
    2015-02
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    71.20.-b
    71.55.Ak
    72.80.Ga
    75.47.Lx
    79.60.-i
    Opis:
    We present calculations of the electronic band structures of $La_{2/3}Pb_{1/3}Mn_{2/3}(Fe,Co,Ni)_{1/3}O_{3}$ colossal magneto-resistance manganites. The calculations are based on first-principles density functional theory with general gradient approximation GGA+U using WIEN2k package. The calculations show that electronic structures of these compounds consist mainly of Mn 3d, O 2p, and (Fe,Co,Ni) 3d states, which are hybridized over whole valence bands. Substitution Mn ion by Fe, Co, or Ni ions reduces the Mn and O contributions to the valence bands and weakens the double exchange interaction. The results are in good agreement with available experimental data.
    Źródło:
    Acta Physica Polonica A; 2015, 127, 2; 251-253
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Electronic Band Structure and Photoemission States of $Bi_{1.96}Mg_{0.04}Se_3$
    Autorzy:
    Tokarz, W.
    Zalecki, R.
    Kowalik, M.
    Kołodziejczyk, A.
    Kozłowski, A.
    Miotkowski, J.
    Powiązania:
    https://bibliotekanauki.pl/articles/1374118.pdf
    Data publikacji:
    2014-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    71.20.-b
    71.55.Ak
    72.80.Ga
    75.47.Lx
    79.60.-i
    Opis:
    We present theoretical band structure calculations and ultraviolet electron photoemission spectroscopy of a topological insulator $Bi_{1.96}Mg_{0.04}Se_3$. Our calculations were based on the first-principles density functional theory with general gradient approximation using Wien2k package with the spin-orbit interaction included by a second-variation method. The R3̅m crystal structure was optimized. In consequence, 4% decrease of volume and 3% decrease of ratio c/a was obtained. This modified structure was multiplied three times in a and b direction in order to place proper amount of Mg. Final crystal structure P3m1 with 135 atoms was used for the calculations. As a result metallic band structure was obtained with conduction band extended from -5.6 eV up to 0.16 eV. It composes mostly from Se p states. Comparison of total DOS with ultraviolet photoemission spectrum shows similar features.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 4a; A-127-A-129
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Bismuth Valence in a $Tl_{0.7}Bi_{0.3}Sr_{1.6}Ba_{0.4}CaCu_{2}O_{y}$ Superconductor from X-Ray Photoemission Spectroscopy
    Autorzy:
    Zalecki, R.
    Woch, W.
    Kowalik, M.
    Kołodziejczyk, A.
    Gritzner, G.
    Powiązania:
    https://bibliotekanauki.pl/articles/1537186.pdf
    Data publikacji:
    2010-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    74.72.-h
    74.25.Jb
    79.60.-i
    Opis:
    The X-ray electron photoemission spectra of a $Tl_{0.7}Bi_{0.3}Sr_{1.6}Ba_{0.4}CaCu_2O_{y}$ superconductor were measured with $Al K_{α}$ and $Mg K_{α}$ radiation at room temperature. The Bi 4f spectrum was compared to the same spectra of $Bi_{1.75}Pb_{0.35}Sr_{1.9}Ca_{2.05}Cu_{3.05}O_{y}$ and $Tl_{0.6}Pb_{0.4}Sr_{1.6}Ba_{0.4}Ca_2Cu_3O_{y}$ superconductors. In Bi,Pb-based superconductor only one type of $Bi^{3+}$ ions is present. The Bi 4f spectrum in the Tl,Bi-superconductor consists of two contributions due to the different valences. The component from $Bi^{5+}$ lines is in higher binding energy than from $Bi^{3+}$. The ratio of trivalent $Bi^{3+}$ to pentavalent $Bi^{5+}$ bismuth ions was calculated from decomposition of the spin-orbit split spectrum of the Bi 4f photoelectrons. The conclusion is that Bi is present in trivalent and in pentavalent form and the ratio of $Bi^{3+}$ to $Bi^{5+}$ is 1.87 ± 0.02.
    Źródło:
    Acta Physica Polonica A; 2010, 118, 2; 393-395
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Izolacja i identyfikacja naturalnych substancji barwiących obecnych w próbkach farb artystycznych i tkaninach pochodzenia historycznego
    Isolation and identification of natural dyestuffs present in artistic paints and textiles of historical origin
    Autorzy:
    Otłowska, O.
    Śliwka-Kaszyńska, M.
    Kołodziejczyk, A.
    Powiązania:
    https://bibliotekanauki.pl/articles/172392.pdf
    Data publikacji:
    2016
    Wydawca:
    Polskie Towarzystwo Chemiczne
    Tematy:
    barwniki
    naturalne barwniki organiczne
    analiza LC-DAD-MS
    ekstrakcja
    historyczne farby artystyczne
    natural organic dyes
    analysis LC-DAD-MS
    extraction
    historical artistic paints
    Opis:
    Natural organic dyes are group of substances that belong to various types of chemical compounds. The most commonly used in paintings and dyeing textiles were naturally occurring dyestuffs from group of anthraquinones, flavones and indigoid dyes. Identification of coloring substances present in historical artistic paints provides relevant information for a wide range of specialists dealing with works of art and in the field of conservation science. This research presents a review of analytical techniques (mainly chromatographic and spectroscopic) used for identification of dyes. It also describes the methods of colorants isolation from historical artistic paints and textiles. Furthermore, the article presents a brief characteristics of fragmentation reactions of selected groups of dyestuffs, which is useful in their identification.
    Źródło:
    Wiadomości Chemiczne; 2016, 70, 3-4; 163-187
    0043-5104
    2300-0295
    Pojawia się w:
    Wiadomości Chemiczne
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-9 z 9

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