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Wyszukujesz frazę "Jędrzejewski, Ł." wg kryterium: Autor


Wyświetlanie 1-2 z 2
Tytuł:
Analysis of Thermal Stability of CrCN Coatings Deposited on Nitrided Substrates Using Modulated Temperature Thermodilatometry
Autorzy:
Mydłowska, K.
Myśliński, P.
Szparaga, Ł.
Ratajski, J.
Gilewicz, A.
Jędrzejewski, R.
Powiązania:
https://bibliotekanauki.pl/articles/352462.pdf
Data publikacji:
2017
Wydawca:
Polska Akademia Nauk. Czytelnia Czasopism PAN
Tematy:
antiwear coatings
nitriding
residual stress
thermal stability
thermodilatometry
Opis:
The aim of the research was to investigate the influence of nitriding of the substrate made of 42CrMo4 steel on thermal stability of the antiwear CrCN coating deposited on its surface using Cathodic Arc Evaporation method. Samples of non-nitrided and nitrided substrate/CrCN coating systems were tested with Modulated Temperature Thermodilatometry, which program included system annealing in 26 h, temperature of 290°C and argon atmosphere. Recorded during tests, changes in substrate elongation in response for changes of sample temperature, enabled qualitative determination of changes in stress states in the coatings as a result of samples annealing. Annealing of the system with nitrided substrate resulted in smaller change in residual stress in coating than for the system with non-nitrided substrate, which can indicate its better thermal stability. Values of residual stresses in coatings calculated by sin2ψ method before and after annealing on the basis of tests performed using X-Ray diffraction, agree with results of dilatometric tests.
Źródło:
Archives of Metallurgy and Materials; 2017, 62, 2A; 771-776
1733-3490
Pojawia się w:
Archives of Metallurgy and Materials
Dostawca treści:
Biblioteka Nauki
Artykuł
Tytuł:
The utilization of the mesoporous Ti-SBA-15 catalyst in the epoxidation of allyl alcohol to glycidol and diglycidyl ether in the water medium
Autorzy:
Wróblewska, A.
Makuch, E.
Dzięcioł, M.
Jędrzejewski, R.
Kochmański, P.
Kochmańska, A.
Kucharski, Ł.
Powiązania:
https://bibliotekanauki.pl/articles/777977.pdf
Data publikacji:
2015
Wydawca:
Zachodniopomorski Uniwersytet Technologiczny w Szczecinie. Wydawnictwo Uczelniane ZUT w Szczecinie
Tematy:
glycidol
diglycidyl ether
Ti-SBA-15 catalyst
allyl alcohol epoxidation
hydrogen peroxide
Opis:
This work presents the studies on the optimization the process of allyl alcohol epoxidation over the Ti-SBA-15 catalyst. The optimization was carried out in an aqueous medium, wherein water was introduced into the reaction medium with an oxidizing agent (30 wt% aqueous solution of hydrogen peroxide) and it was formed in the reaction medium during the processes. The main investigated technological parameters were: the temperature, the molar ratio of allyl alcohol/hydrogen peroxide, the catalyst content and the reaction time. The main functions the process were: the selectivity of transformation to glycidol in relation to allyl alcohol consumed, the selectivity of transformation to diglycidyl ether in relation to allyl alcohol consumed, the conversion of allyl alcohol and the selectivity of transformation to organic compounds in relation to hydrogen peroxide consumed. The analysis of the layer drawings showed that in water solution it is best to conduct allyl alcohol epoxidation in direction of glycidol (selectivity of glycidol 54 mol%) at: the temperature of 10–17°C, the molar ratio of reactants 0.5–1.9, the catalyst content 2.9–4.0 wt%, the reaction time 2.7–3.0 h and in direction of diglycidyl ether (selectivity of diglycidyl ether 16 mol%) at: the temperature of 18–33°C, the molar ratio of reactants 0.9–1.65, the catalyst content 2.0–3.4 wt%, the reaction time 1.7–2.6 h. The presented method allows to obtain two very valuable intermediates for the organic industry.
Źródło:
Polish Journal of Chemical Technology; 2015, 17, 4; 23-31
1509-8117
1899-4741
Pojawia się w:
Polish Journal of Chemical Technology
Dostawca treści:
Biblioteka Nauki
Artykuł
    Wyświetlanie 1-2 z 2

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