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    Wyświetlanie 1-6 z 6
    Tytuł:
    Effect of the Thermal Treatment on the Microstructure and Magnetic Property of $Fe_{68}Zr_{20}B_{12}$ Alloy Prepared by Mechanical Alloying
    Autorzy:
    Sun, Y.
    Yu, W.
    Hua, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/1505353.pdf
    Data publikacji:
    2011-03
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.37.Lp
    61.05.Qr
    Opis:
    $Fe_{68}Zr_{20}B_{12}$ amorphous alloy prepared by mechanical alloying technique of 60 h of duration was annealed at different temperatures (420-720°C) during 1 h. Microstructure and magnetic property of as-milled and annealed alloy were investigated by X-ray diffraction, transmission electron microscopy, the Mössbauer spectroscopy and vibrating sample magnetometer techniques. $Fe_{68}Zr_{20}B_{12}$ powders milled during 60 h exhibit amorphous character. After annealing at 420°C, α-Fe phase precipitates from amorphous matrix. Transmission electron microscopy analysis shows the nucleation and growth of α-Fe grains. The Mössbauer results of the annealed alloy at 670°C show that the $Fe_3B$ phase precipitates already and there is still remaining amorphous phase. Coercivity increases with increasing annealing temperature, which is closely related to the microstructures after annealing.
    Źródło:
    Acta Physica Polonica A; 2011, 119, 3; 374-377
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Effect of High Co Addition on the Properties of $Fe_{79}Zr_{9}B_{12}$ and $Fe_{76}Zr_{9}B_{15}$ Alloys
    Autorzy:
    Yu, W.
    Long, D.
    Liu, Y.
    Sun, Y.
    Hua, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/1401884.pdf
    Data publikacji:
    2015-09
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    65.60.+a
    61.43.Dq
    Opis:
    Thermal properties, microstructure and magnetic properties of $Fe_{79}Zr_{9}B_{12},$ $Fe_{76}Zr_{9}B_{15},$ $Fe_{39.5}Co_{39.5}Zr_{9}B_{12}$ and $Fe_{38}Co_{38}Zr_{9}B_{15}$ alloys were investigated by differential thermal analysis, X-ray diffraction and vibrating sample magnetometer. High Co addition has a significant impact on the properties of alloys. High Co addition increases the main crystallization peak temperature and the crystallization activation energy. Moreover, high Co addition changes the crystallization products and influences the crystallization processes of $Fe_{79}Zr_{9}B_{12}$ and $Fe_{76}Zr_{9}B_{15}$ alloys. The specific saturation magnetization $(M_{s})$ increases and coercivity $(H_{c})$ decreases by high Co additions.
    Źródło:
    Acta Physica Polonica A; 2015, 128, 3; 340-342
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Thermal Behavior and Crystallization of $Fe_{81 - x}Co_{x}Zr_7Nb_2B_{10}$ (x = 2, 4, 6) Alloys
    Autorzy:
    Yu, W.
    Sun, Y.
    Liu, L.
    Dong, L.
    Hua, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/1492773.pdf
    Data publikacji:
    2011-12
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    65.60.+a
    61.43.Dq
    Opis:
    Thermal behavior and microstructure of $Fe_{81 - x}Co_{x}Zr_7Nb_2B_{10}$ (x = 2, 4, 6) alloys were investigated by differential thermal analysis and X-ray diffraction. Both the supercooled liguid region Δ $T_{x}$ and the first crystallization peak temperature $T_{p1}$ are the lowest and the span Δ $T_{p}$ between $T_{p1}$ and $T_{p2}$ is the highest when 4 at.% Fe is substituted by Co. The crystallization activation energy $E_{p1}$ for $Fe_{75}Co_6Zr_7Nb_2B_{10}$ alloy is the minimum for the heating rates ν = 5-20 K/min. $E_{p1}$ for $Fe_{77}Co_4Zr_7Nb_2B_{10}$ alloy is the minimum for the heating rates ν = 20 - 50 K/min. The crystallization processes of $Fe_{81 - x}Co_{x}Zr_7Nb_2B_{10}$ (x = 2, 4, 6) amorphous alloys are similar on the whole, which is as follows: amorphous → amorphous + α-Fe(Co) → α-Fe(Co) + $Fe_3Zr$ + $Fe_2Nb_{0.4}Zr_{0.6}$.
    Źródło:
    Acta Physica Polonica A; 2011, 120, 6; 1034-1036
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Effect of Annealing Temperature and Ambient on Formation, Composition and Bandgap of $Cu_2ZnSnS_4$ Thin Films
    Autorzy:
    Sun, Y.
    Yao, B.
    Meng, X.
    Wang, D.
    Long, D.
    Hua, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/1205220.pdf
    Data publikacji:
    2014-08
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    68.55.-a
    Opis:
    Amorphous Cu-Zn-Sn-S precursor films were prepared by sol-gel and spin-coating with copper chloride, zinc chloride, tin chloride and thiourea solutions as starting materials. A $Cu_2ZnSnS_4$ film with kesterite structure and a small amount of chlorine formed when the precursor was annealed under Ar ambient at temperature above 200°C, but its atomic ratios of Cu:Zn:Sn:S far deviated from stoichiometric ratios of the $Cu_2ZnSnS_4$. However, when the precursor films were annealed with sulfur powder together at temperatures between 360 and 480°C, the CZTS film containing a very small amount of Cl formed, and its atomic ratio change little for Cu, Zn, and Sn, increases for S and decreases for Cl with increasing temperature. When the temperature is 480°C, a CZTS only has Cu, Zn, Sn, and S element is fabricated, and the atomic ratio of Cu:Zn:Sn:S is near the stoichiometric ratio. The bandgap of the CZTS decreases with increasing annealing temperature. The mechanisms of the formation and the properties of the CZTS are suggested in the present work.
    Źródło:
    Acta Physica Polonica A; 2014, 126, 3; 751-756
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    The Influence of Cycle Sputtering Deposition on the Properties of Cu₂ZnSnS₄ Thin Films
    Autorzy:
    Sun, Y.
    Yao, B.
    Long, D.
    Meng, X.
    Liu, L.
    Hua, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/1398930.pdf
    Data publikacji:
    2016-06
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    78.40.Fy
    Opis:
    Three kinds of precursor thin films with stacking orders of Cu/Sn/ZnS, Cu/Sn/ZnS/Cu/Sn/ZnS and Cu/Sn/ZnS/Cu/Sn/ZnS/Cu/Sn/ZnS were prepared by magnetron sputtering and annealed with sulfur powder. The microstructure, morphology and optical properties of thin films were investigated by X-ray diffraction, the Raman scattering, scanning electron microscopy and UV-visible spectrophotometer. The increase of cycle number decreases the sulfurizing temperature of the formation of Cu₂ZnSnS₄ phase. Chemical composition can be controlled by cycle sputtering deposition. After sulfurizing at 500°C, the particle size and the band gap increase with increasing cycle number.
    Źródło:
    Acta Physica Polonica A; 2016, 129, 6; 1169-1172
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
    Tytuł:
    Crystallization Process of $Fe_{75}Co_5Zr_{10}B_{10}$ Amorphous Alloy
    Autorzy:
    Sun, Y.
    Zuo, B.
    Wang, D.
    Meng, X.
    Liu, J.
    Wang, L.
    Hua, Z.
    Powiązania:
    https://bibliotekanauki.pl/articles/1399278.pdf
    Data publikacji:
    2013-10
    Wydawca:
    Polska Akademia Nauk. Instytut Fizyki PAN
    Tematy:
    61.43.Dq
    64.60.My
    Opis:
    $Fe_{75}Co_5Zr_{10}B_{10}$ amorphous alloy prepared by melt-spinning was annealed at various temperatures. The thermal property and microstructures were investigated by differential thermal analysis, X-ray diffraction, and transmission electron microscopy. The crystallization process of $Fe_{75}Co_5Zr_{10}B_{10}$ amorphous alloy is complex. The α-Fe phase precipitates from the amorphous matrix in the initial stage of crystallization. The α-Mn type (χ) phase precipitates at 570°C, but transforms to α-Fe phase and the Laves C14(λ) phase at higher temperature. In the final stage of crystallization, $Fe_3Zr$, $Fe_2Zr$, and unknown phases are observed and the λ-phase disappears. The α-Fe phase preferentially nucleates after annealing at 530C for 10 min and the χ-phase preferentially nucleates after annealing at 600C for 10 min. The nucleation barrier of χ-phase is larger than that of α-Fe phase. The local structure of χ-phase is more similar to amorphous phase.
    Źródło:
    Acta Physica Polonica A; 2013, 124, 4; 685-687
    0587-4246
    1898-794X
    Pojawia się w:
    Acta Physica Polonica A
    Dostawca treści:
    Biblioteka Nauki
    Artykuł
      Wyświetlanie 1-6 z 6

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