- Tytuł:
- Preparation of Nickel Nanoparticles Using Nickel Raffinate Separated by Solvent Extraction from The Spent FeCl3 Etching Solution
- Autorzy:
-
Park, Il-Jeong
Swain, Basudev
Kim, Dae-Weon
Kim, Geon-Hong
Han, Deok-Hyun
Jung, Hang-Chul - Powiązania:
- https://bibliotekanauki.pl/articles/354453.pdf
- Data publikacji:
- 2019
- Wydawca:
- Polska Akademia Nauk. Czytelnia Czasopism PAN
- Tematy:
-
nickel
recycling
solvent extraction
chemical reduction - Opis:
- FeCl3 bearing etching solution is mainly used for etching of metals used in shadow masks, PCBs and so on. Due course of Invar alloy etching process the FeCl3 bearing etching solution get contaminated with Ni2+ which affect adversely the etching efficiency. Hence, FeCl3 bearing etching solution discarded after several cycle of operation causes an environmental and economic problem. To address both the issues the etching solution was purified through solvent extraction and remained Ni2+ recovered by wet chemical reduction using hydrazine. For optimum Fe3+ extraction efficiency, various extraction parameter were optimized and size and morphology of the recovered pure Ni powder was analyzed. The reported process is a simple process to purify and recover Ni from industry etching solution.
- Źródło:
-
Archives of Metallurgy and Materials; 2019, 64, 2; 531-534
1733-3490 - Pojawia się w:
- Archives of Metallurgy and Materials
- Dostawca treści:
- Biblioteka Nauki